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2 protocols using methyl caprate

1

Volatile Compounds Analysis Protocol

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2-Pentanone, diacetyl, acetoin, 2-undecanone, butyl acetate, methyl hexanoate, methyl caprate, ethyl caprate, ethyl butyrate, ethyl hexanoate, 3-methylbutanal, benzaldehyde, pentanal, nonanal, octanal, acetic acid, propionic acid, isobutyric acid, butyric acid, isovaleric acid, hexanoic acid, octanoic acid, decanoic acid, valeric acid, δ-dodecalactone, (Z)-dairy lactone, δ-caprinolactone, γ-dodecalactone, dichloromethane and n-alkane standards (C6–C30) were purchased from Sigma-Aldrich (St. Louis, MO, USA). 2-Octanol (internal standard, IS) was purchased from Dr Ehrenstorfer GmbH, Augsburg, Germany. All of the chemicals were of chromatographic grade and had a purity>98 %.
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2

Characterization of Pharmaceutical Compounds

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Capric acid (CA) and methyl caprate (MC) were purchased from Sigma-Aldrich. Droperidol (Drp) and Aripiprazole (Arp) were kindly provided as gifts from Jordanian Pharmaceutical Manufacturing Company (JPM), Amman, Jordan. All chemicals were used as such without further purification. Full characterisation of the drugs was performed using NMR techniques to demonstrate their purity. Deuterated solvents for NMR were purchased from Cambridge Isotope Laboratories and Sigma-Aldrich.
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