2-aminoethane, 5,5′-dithio-bis-(2-nitrobenzoic acid) (Ellman’s reagent), adipoyl chloride, cystamine dihydrochloride, dialysis tubing cellulose membrane (MWCO 12,000 Da), dimethylsulfoxide (DMSO), dimethylsulfoxide-d6 (DMSO-d6), pancreatin, pepsin polyvinyl alcohol (PVA), sodium nitroprusside, triethylsilane (TES), trifluoroacetic acid (TFA), trimesoyl chloride, triphenylmethanol, Tween 80, and zinc dust were purchased from Sigma Chemicals (St. Loius, Missouri, US). Ammonium bicarbonate, calcium chloride (CaCl2), dichloromethane (DCM), diethyl ether (Et2O), disodium hydrogen phosphate (Na2HPO4.2H2O), hydrochloric acid (HCl), monopotassium phosphate (KH2PO4), sodium bicarbonate (NaHCO3), sodium chloride (NaCl), sodium hydroxide (NaOH), and sulfuric acid (H2SO4) were purchased from R&M Chemicals (London, UK). Silica gel (0.035–0.070 mm) was purchased from Acros Organics (Geel, Belgium) and used for column chromatography. Acetic acid and methanol were purchased from Qrec Chemical (Chonburi, Thailand). Lactobacillus was provided by the Department of Biological Science and Technology, China Medical University, Taichung, Taiwan.
Adipoyl chloride
Manufactured by Merck Group
Sourced in United States, Germany
Adipoyl chloride is a chemical compound used in various industrial processes. It is a colorless, pungent liquid that is primarily used as a raw material in the production of other chemicals.
Automatically generated - may contain errors
Lab products found in correlation
Trimesoyl chloride, by Merck Group (2 mentions)
Terephthaloyl chloride, by Merck Group (2 mentions)
N n dimethylformamide (dmf), by Merck Group (2 mentions)
Glutaryl chloride, by Merck Group (2 mentions)
Malonyl chloride, by Merck Group (2 mentions)
Succinyl chloride, by Merck Group (2 mentions)
Chloroform, by Merck Group (2 mentions)
Hexamethylenediamine, by Merck Group (2 mentions)
5 5 dithiobis 2 nitrobenzoic acid, by Merck Group (1 mentions)
Cystamine dihydrochloride, by Merck Group (1 mentions)
Tween 80, by Merck Group (1 mentions)
Trifluoroacetic acid tfa, by Merck Group (1 mentions)
Sodium nitroprusside, by Merck Group (1 mentions)
Triphenylmethanol, by Merck Group (1 mentions)
Zinc dust, by Merck Group (1 mentions)
Sebacoyl chloride, by Merck Group (1 mentions)
4 dimethylaminopyridine, by Thermo Fisher Scientific (1 mentions)
Standard laboratory solvents, by Biosolve (1 mentions)
1 3 cyclopentanediol, by Merck Group (1 mentions)
1 4 cyclo hexanediol, by Thermo Fisher Scientific (1 mentions)
8 protocols using adipoyl chloride
1
Enzyme-Responsive Polymer Synthesis
2
Synthesis of Furan-Based Polyesters
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1,3-Cyclopentanediol (15/85 cis/trans), 1,4-cyclohexanedimethanol (38/62 cis/trans), adipoyl chloride, sebacoyl chloride, terephthaloyl chloride, tin(ii ) 2-ethyl-hexanoate, and anhydrous chloroform, DMF, THF, and toluene were obtained from Sigma Aldrich. Magnesium(iv ) sulfate, 4-dimethylaminopyridine and pyridine were obtained from ACROS. 2,5-Furan-dicarboxylic acid was obtained from ABCR. 1,4-Cyclohexanediol (46/54 cis/trans) was obtained from Alfa Aesar. Ethylene glycol was obtained from TCI. Standard laboratory solvents were obtained from Biosolve. Deuterated solvents were obtained from Buchem BV (Netherlands). The purchased compounds were used directly without further purification, unless otherwise specified.
3
Organic Synthesis of Enantiopure Compounds
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Chemicals and reagents. Levoglucosenone was graciously provided by Circa group. Citronellol (Sigma Aldrich, Saint-Louis, MO, USA), diisobutylaluminum hydride (DIBAL-H) (Acros, Geel, Belgium), malonyl chloride 97% (Sigma Aldrich), succinyl chloride 95% (Sigma Aldrich), adipoyl chloride 98% (Sigma Aldrich), glutaryl chloride 97% (Sigma Aldrich), Lipopan® 50 BG (Novozymes, Bagsværd, Denmark) a purified lipase from Thermomyces lanuginosus expressed in Aspergillus oryzae, were used as received. NMR solvents, including CDCl3 and DMSO-d6, were purchased from Cambridge Isotopes Laboratories. HPLC grade solvents were purchased from Thermofisher Scientific, Waltham, MA, USA, and used as received. Ultra-pure laboratory-grade water was obtained from MilliQ, 18.2 megaOhms. TLC analyses were performed on an aluminum strip coated with Silica Gel 60 F254 from Merck, revealed under UV-light (254 nm), then in the presence of potassium permanganate staining solution. All manipulations with air-sensitive chemicals and reagents were performed using standard Schlenk techniques on a dual-manifold line, on a high-vacuum line.
4
Synthesis and Characterization of Functional Polymers
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Trimethylolpropane allyl ether (98%), adipoyl chloride (98%), pyridine (99.5%), 3-mercaptopropionic acid (≥99%), thioglycolic acid (98%), 3-(trimethoxysilyl)propyl methacrylate (98%), 2,2-dimethoxy-2-phenyl-acetophenone (99%), chloroform (≥99.8%), methanol (≥99.8%), dimethylformamide (≥99.8%), and Hellmanex III were purchased from Sigma-Aldrich (Steinheim, Germany). Ethanol (≥99.8%) was obtained from Honeywell (Seetze, Germany) and toluene (≥99.8%) from Fisher Scientific (Loughborough, UK). Dichloromethane (analytical grade), n-hexane (96%), and diethyl ether (99.8%) were purchased from Scharlau (Sentmenat, Spain). Dichloromethane was dried over calcium hydride and distilled under a nitrogen atmosphere prior to use. All the other solvents and chemicals were used without further purification.
Trypsin/EDTA (0.25%), phosphate buffer saline (PBS), Amphotericin-B (fungizone), penicillin/streptomycin (P/S), were all purchased from Gibco ThermoFisher Scientific (Waltham, MA, USA), Roswell Park Memorial Institute 1640 medium (RPMI) with stable glutamine and fetal bovine serum (FBS) from PAN-Biotech (Aidenbach, Germany) and PrestoBlueTM reagent for cell viability from Invitrogen Life Technologies (Carlsbad, CA, USA). The L929 fibroblastic cell line was purchased from the German collection of microorganisms and cell cultures (DSMZ GmbH, Braunschweig, Germany).
Trypsin/EDTA (0.25%), phosphate buffer saline (PBS), Amphotericin-B (fungizone), penicillin/streptomycin (P/S), were all purchased from Gibco ThermoFisher Scientific (Waltham, MA, USA), Roswell Park Memorial Institute 1640 medium (RPMI) with stable glutamine and fetal bovine serum (FBS) from PAN-Biotech (Aidenbach, Germany) and PrestoBlueTM reagent for cell viability from Invitrogen Life Technologies (Carlsbad, CA, USA). The L929 fibroblastic cell line was purchased from the German collection of microorganisms and cell cultures (DSMZ GmbH, Braunschweig, Germany).
5
Oxidation and Cyclization of Levoglucosenone
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Levoglucosenone was graciously provided by the Circa Group. Potassium carbonate 99% (Acros), hydrogen peroxide 30% (Fischer), diethyl succinate 98% (Alpha Aesar), malonyl chloride 97% (Sigma Aldrich), succinyl chloride 95% (Sigma Aldrich), adipoyl chloride 98% (Sigma Aldrich), glutaryl chloride 97% (Sigma Aldrich), terephthaloyl chloride >99% flakes (Sigma Aldrich) were used without further purification unless mentioned. NMR solvents including deuterated chloroform, deuterated methanol, and deuterated dimethyl sulfoxide were purchased from Cambridge Isotopes Laboratories.
6
Synthesis of PEG-based Polyurethanes
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Hexamethylene diisocyanate (purum, ≥98.0%; Sigma) (Sigma-Aldrich Israel Ltd., an affiliate of Merck KGaA, Darmstadt, Germany); PEG MW = 200 (PEG200) (Sigma); PEG MW = 400 (PEG400) (Sigma); Methoxypolyethylene glycol (PEG monomethyl ether) MW = 350 (PEG350M) (Sigma); Ethyl stannous hexanoate (Tin (II) 2-ethylhexanoate 92.5–100%) (Sigma); Adipoyl chloride (98%; Sigma); Hexamethylenediamine (98%; Sigma); Cyclohexane (99.5%; Sigma); KBr powder for FTIR analysis (FTIR grade, ≥99%; Sigma).
7
Fabrication of Microporous PES Membranes
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Microporous PES (0.45 µm, Millipore Express) and n-hexane were purchased from MERCK (Darmstadt, Germany). Trimesoyl chloride (TMC), hexamethylenediamine (HMD), adipoyl chloride (ADC), piperazine (PIP), and 17β-Estradiol (E2) were obtained from Sigma Aldrich (St. Louis, MO, USA). Ethanol and toluene were purchased from VWR (Radnor, PA, USA). Deionized water in Millipore® quality was used for all steps. All materials were used as they were received from suppliers.
8
Synthesis of Diacyl Chloride Derivatives
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Diacyl chlorides, adipoyl chloride (AC, Sigma Aldrich), suberoyl chloride (SC, Sigma Aldrich), sebacoyl chloride (SeC, TCI chemicals, India), and dodecanedioyl chloride (DC, Sigma Aldrich) were used. Acetic anhydride (AAn) was procured from Sigma Aldrich. Salicylic acid (SA) was obtained from SD Fine Chemicals, India. Solvents used at various stages of the study include ethyl acetate (EtoAc), chloroform, dichloromethane (DCM), dimethylsulfoxide (DMSO), N,N-dimethylformamide (DMF), and acetone (all from Merck, India).
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