Zinc nitrate hexahydrate (Zn(NO 3 ) 2 •6H 2 O), zinc oxide (ZnO), 2-methylimidazole (mIm), cobalt nitrate hexahydrate (Co (NO 3 ) 2 •6H 2 O), 2,5-dihydroxyterephthalic acid, cobalt(II) oxide (CoO, ca. 325 mesh), benzimidazole (bIm), imidazole (Im), ammonium nitrate (NH 4 NO 3 ), ruthenium(IV) oxide (RuO 2 ) were obtained from Sigma-Aldrich. N,N-Dimethylformamide (DMF), potassium hydroxide (KOH), ethanol and methanol were supplied by Merck. Carbon cloth (CC) was supplied by Fuel Cell Store. Polyvinylidene fluoride membrane (PVDF) was supplied by MilliporeSigma. Titanium foil was supplied by Goodfellow. Fluorine doped tin oxide coated glass slides (FTO) were supplied by Aopi Weite New Energy Technology Co., Ltd, Yangzhou, China. Matrimid® 5218 was supplied by Huntsman Advanced Materials Americas, Inc. All the chemicals were used without further purification. All gases were supplied by Coregas Pty Ltd.
2 methylimidazole mim
Manufactured by Merck Group
Sourced in Finland, United States
2-methylimidazole (mIm) is a heterocyclic organic compound. It is a colorless, crystalline solid that serves as a key intermediate in the synthesis of various pharmaceutical and industrial products.
Automatically generated - may contain errors
Lab products found in correlation
Cobalt nitrate hexahydrate, by Merck Group (1 mentions)
Zinc nitrate hexahydrate, by Merck Group (1 mentions)
Ammonium nitrate, by Merck Group (1 mentions)
Cobalt 2 oxide, by Merck Group (1 mentions)
2 5 dihydroxyterephthalic acid, by Merck Group (1 mentions)
Ruthenium 4 oxide, by Merck Group (1 mentions)
N hydroxysuccinimide nhs, by Thermo Fisher Scientific (1 mentions)
Ethylenediamine, by Thermo Fisher Scientific (1 mentions)
Zn no3 2 6h2o, by Merck Group (1 mentions)
4 dimethylaminopyridine dmap, by Thermo Fisher Scientific (1 mentions)
N 3 dimethylamino propyl n ethylcarbodiimidehydrochloride edc hcl, by Thermo Fisher Scientific (1 mentions)
Milli q, by Merck Group (1 mentions)
N 3 dimethylaminopropyl n ethylcarbodiimide hydrochloride edc hcl, by Merck Group (1 mentions)
Zinc acetate dihydrate, by Avantor (1 mentions)
Ethylenediamine eda, by Merck Group (1 mentions)
N n dimethylformamide (dmf), by Merck Group (1 mentions)
5 protocols using 2 methylimidazole mim
1
Synthesis of Metal-Organic Frameworks
2
Doxorubicin-Folic Acid Conjugate Synthesis
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Doxorubicin (DOX·HCl) and folic acid
(FA) were purchased from Arisun ChemPharm Co., Ltd. (China). cis-Aconitic anhydride (CAA), ethylenediamine, 4-dimethylaminopyridine
(DMAP), N-hydroxy succinimide (NHS), and N-(3-(dimethylamino)propyl)-N-ethylcarbodiimide
hydrochloride (EDC·HCl) were purchased from Alfa Aesar (Finland).
2-Methylimidazole (MIM), Zn (NO3)2·6H2O, N,N-dimethylformamide (DMF), triethylamine
(TEA), dichloromethane (DCM), and menthol (MeOH) were purchased from
Sigma-Aldrich (Finland).
(FA) were purchased from Arisun ChemPharm Co., Ltd. (China). cis-Aconitic anhydride (CAA), ethylenediamine, 4-dimethylaminopyridine
(DMAP), N-hydroxy succinimide (NHS), and N-(3-(dimethylamino)propyl)-N-ethylcarbodiimide
hydrochloride (EDC·HCl) were purchased from Alfa Aesar (Finland).
2-Methylimidazole (MIM), Zn (NO3)2·6H2O, N,N-dimethylformamide (DMF), triethylamine
(TEA), dichloromethane (DCM), and menthol (MeOH) were purchased from
Sigma-Aldrich (Finland).
3
Protein Purification and Modification Protocol
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All proteins were purchased from Sigma-Aldrich unless otherwise stated (Table S1† ). Each of the proteins tested were lyophilised powders and were used without further purification. 2-Methyl imidazole (mIM) and N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (EDC·HCl) were purchased from Sigma-Aldrich, zinc acetate dihydrate from VWR Chemicals, succinic anhydride from BDH, acetic anhydride from Chem Supply, and ethylene diamine (EDA) from Merck. The water used was ultra pure Milli-Q (MQ) with resistivity of 18 MΩ cm–1 (Merck Millipore purification system). All other buffers and solvents were purchased from commercial sources and used without further purification.
4
Synthesis of Magnetite-Zeolitic Imidazolate Frameworks
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Magnetite (Fe3O4, daverage = 8 nm, 99.9% purity, US Research Nanomaterials, Houston, TX, USA), 2-methylimidazole (mIm, 99% purity, Sigma-Aldrich, Zwijndrecht, The Netherlands), poly(ethylene glycol) (PEG, 1 kDa, Sigma-Aldrich, Zwijndrecht, The Netherlands), N,N-dimethylformamide (DMF, ≥99.9% purity, Sigma-Aldrich, Zwijndrecht, The Netherlands), zinc nitrate hexahydrate (Zn(NO3)2 · 6 H2O, 98% purity, Thermofischer Acros Organic, Geel, Belgium), Matrimid® 5218 (Matrimid, kindly provided by Huntsman, Basel, Switzerland), ultrapure water (PURELAB Option demineralizer, Veolia Water Solutions and Technologies, Ede, The Netherlands), helium (5.0 grade, Linde gas, Schiedam, The Netherlands), nitrogen (4.5 grade, Linde gas, Schiedam, The Netherlands) and carbon dioxide (4.5 grade, Linde gas, Schiedam, The Netherlands) were used as received without further purification.
5
Synthesis of ZIF-8 Nanocrystals
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
ZIF-8 nanocrystals
were synthesized by dissolving 4.5 mmol of zinc nitrate hexahydrate
[Zn(NO3)2·6H2O; 98%, Sigma-Aldrich]
and 13.5 mmol of 2-methylimidazole (mIm; 98%, Sigma-Aldrich) in 60
mL of methanol, respectively. After the two clear solutions were combined,
the white colloidal solution was rigorously stirred for 1 min and
then left to form the nanocrystals. Immediately, some material was
removed, diluted in fresh methanol, and washed three times. Each washing
step encompassed centrifugation at 8000 rpm for 5 min, followed by
solvent exchange with fresh methanol, and sonication for 30 s. The
same procedure was repeated after 3, 5, and 60 min: after these time
intervals, some material was removed and thoroughly washed to stop
the growth process.
were synthesized by dissolving 4.5 mmol of zinc nitrate hexahydrate
[Zn(NO3)2·6H2O; 98%, Sigma-Aldrich]
and 13.5 mmol of 2-methylimidazole (mIm; 98%, Sigma-Aldrich) in 60
mL of methanol, respectively. After the two clear solutions were combined,
the white colloidal solution was rigorously stirred for 1 min and
then left to form the nanocrystals. Immediately, some material was
removed, diluted in fresh methanol, and washed three times. Each washing
step encompassed centrifugation at 8000 rpm for 5 min, followed by
solvent exchange with fresh methanol, and sonication for 30 s. The
same procedure was repeated after 3, 5, and 60 min: after these time
intervals, some material was removed and thoroughly washed to stop
the growth process.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!