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Ascend 850 nmr spectrometer

Manufactured by Agilent Technologies

The Ascend® 850 NMR spectrometer is a high-performance nuclear magnetic resonance (NMR) instrument designed for advanced analytical applications. It features a superconducting magnet that generates a powerful magnetic field, enabling precise and sensitive detection of molecular structures and compositions.

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2 protocols using ascend 850 nmr spectrometer

1

NMR and Mass Spectrometry Analysis of Compound 10

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HR-ESI-MS spectra were recorded on a Bruker microTOF II ESI-TOF-MS spectrometer. MSn analysis was carried out on a LTQ Velos dual-pressure ion trap mass spectrometer (Thermo Fisher Scientific)32 for compound 10. 1H, 13C, 1H-1H COSY, 1H-1H TOCSY, 1H-1H NOESY, 1H-13C HSQC, 1H-13C HMBC and 1H-15N HSQC NMR spectra for compound 10 were recorded on a Bruker Ascend® 850 NMR spectrometer (850 MHz for 1H and 212.5 MHz for 13C) or a 600 MHz Varian NMR spectrometer (Topspin 2.1.6 software, Bruker) with a 1.7 mm cryoprobe, respectively, using DMSO-d6 as solvent. 1H, 13C, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC spectra for compounds 6, 13, and 14 were all performed on a Bruker Ascend® 600 NMR spectrometer (600 MHz for 1H and 150 MHz for 13C) using DMSO-d6. Data were collected and reported as follows: chemical shift, integration multiplicity (s = singlet, d = doublet, t = triplet, m = multiplet), coupling constant. Chemical shifts were reported using the DMSO-d6 resonance as internal standard for 1H-NMR DMSO-d6: δ = 2.50 ppm and 13C-NMR DMSO-d6: δ = 39.6 ppm.
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2

NMR and Mass Spectrometry Analysis of Compound 10

Check if the same lab product or an alternative is used in the 5 most similar protocols
HR-ESI-MS spectra were recorded on a Bruker microTOF II ESI-TOF-MS spectrometer. MSn analysis was carried out on a LTQ Velos dual-pressure ion trap mass spectrometer (Thermo Fisher Scientific)32 for compound 10. 1H, 13C, 1H-1H COSY, 1H-1H TOCSY, 1H-1H NOESY, 1H-13C HSQC, 1H-13C HMBC and 1H-15N HSQC NMR spectra for compound 10 were recorded on a Bruker Ascend® 850 NMR spectrometer (850 MHz for 1H and 212.5 MHz for 13C) or a 600 MHz Varian NMR spectrometer (Topspin 2.1.6 software, Bruker) with a 1.7 mm cryoprobe, respectively, using DMSO-d6 as solvent. 1H, 13C, 1H-1H COSY, 1H-1H NOESY, 1H-13C HSQC and 1H-13C HMBC spectra for compounds 6, 13, and 14 were all performed on a Bruker Ascend® 600 NMR spectrometer (600 MHz for 1H and 150 MHz for 13C) using DMSO-d6. Data were collected and reported as follows: chemical shift, integration multiplicity (s = singlet, d = doublet, t = triplet, m = multiplet), coupling constant. Chemical shifts were reported using the DMSO-d6 resonance as internal standard for 1H-NMR DMSO-d6: δ = 2.50 ppm and 13C-NMR DMSO-d6: δ = 39.6 ppm.
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