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2 protocols using stainless steel mesh

1

Synthesis of Electrode Materials for Li-ion Batteries

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Synthetic graphite (<45 µm, 99.99%), LiPF6 (battery grade, ≥99.99%), DMC (anhydrous, ≥99%), and alginic acid sodium salt (Alg, medium viscosity) were purchased from Sigma Aldrich. Super P, Li foil (~250 μm in thickness), and stainless steel mesh were bought from Alfa Aesar. Li(CF3SO2NSO2CF3)2 (LiTFSI, 99.5%) and Li(FSO2NSO2F)2 (LiFSI, 99.5%) were purchased from Solvionic. 5,10,15,20-(tetra-4-aminophenyl) porphyrin, 1,4-phenylene-4,4’-bis (2,6-diphenyl-4-pyrylium tetrafluoroborate), sodium oleyl sulfate (SOS) and solvents (e.g., chloroform) were purchased from PorphyChem and Sigma-Aldrich, and used directly without further purification. Water was purified using a Milli-Q purification system (Merck KGaA). All the reactions were carried out under an ambient atmosphere. Substrates (e.g., 300 nm SiO2/Si wafer, quartz glass and copper grids) were obtained from Microchemicals and Plano GmbH.
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2

Carbon Cloth Electrode Synthesis

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The chemicals and materials were purchased from Sigma-Aldrich, unless otherwise specified. The carbon cloth was purchased from Fuel Cell Earth, and the stainless-steel mesh was purchased from Alfa Aesar. The 1H NMR standard sodium 3-(trimethylsilyl) propionate 2,2,3,3-D4 (TSP-D4) and deuterium oxide (purity > 99.9%) were obtained from Cambridge Isotope Laboratories, Inc. Methanol, acetonitrile, ammonium acetate, ammonium hydroxide, and acetic acid were purchased from Fisher Scientific.
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