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Inova 400 mhz nmr

Manufactured by Agilent Technologies

The Inova 400 MHz NMR is a nuclear magnetic resonance spectrometer designed for high-resolution analysis of chemical samples. It operates at a frequency of 400 MHz and is capable of performing a variety of NMR experiments to study the structure and properties of organic and inorganic compounds.

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2 protocols using inova 400 mhz nmr

1

Analytical Techniques for Complex Samples

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The following instruments were used for spectroscopic analyses:
USB-2000 fiber optic spectrometer (Ocean Optics, Inc.) with DT-Mini-B lamp source for UV-visible absorbance spectroscopy, Agilent 1260 and 1050 systems with attached vacuum degasser, auto-autosampler and diode array detector for chromatography, ABI-Q-Trap 3200 for mass spectrometry, and Varian Inova 400 MHz NMR.
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2

Hyperpolarization of Cesium-133 Ions

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Hyperpolarization of 133Cs+ was achieved in a 3.35 T HyperSense polarizer (Oxford Instruments, Oxford, UK) with the sample at 1.2 K and irradiated at the optimum microwave frequency using a 94 GHz source. Equilibrium of polarization occurred after ~1 h, following a bi-exponential build up and was typically around 50%, similar to the previously obtained values7 (link).
133Cs NMR spectra were recorded at 52.5 MHz on a Varian Inova 400 MHz NMR spectrometer, with a shielded, vertical, narrow-bore 9.4 T, AS 400, magnet from Oxford Instruments (2006). A Varian 10-mm broad-band probe with thermal regulation was used. Spectra, including peak integrals, were extracted using MNova software (MestreLab Research S. L., Santiago de Compostela, Spain).
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