1,4-Butanediamine, di-tert-butyl di-carbonate, chloroform, dichloromethane, triethylamine, sodium hydroxide, ethanol, diethyl ether, sodium chloride, N,N-dimethylformamide (DMF), hydrochloric acid, dimethyl sulfoxide (DMSO), and N-(2-Aminoethyl)maleimide trifluoroacetate salt were purchased from FUJIFILM Wako Pure Chemical Corporation (Osaka, Japan) and used as received. Cinnamoyl chloride was purchased from Tokyo Chemical Industry Co., Ltd. (Tokyo, Japan) and used as received. Succinimidyl-tetra-PEG (pentaerythritol tetra (succinimidyloxyglutaryl) polyoxyethylene), maleimide-tetra-PEG (N-(2-aminoethyl)maleimide trifluoroacetate salt, and Pentaerythritol tetra {[3-(3-maleimido-1-oxopropyl)amino]propyl} polyoxyethylene) were purchased from NOF Corporation (Tokyo, Japan) and used as received. All aqueous solutions were prepared with ultrapure water (Milli-Q, 18.2 MΩ·cm). Other solvents and reagents of analytical grade were obtained from commercial sources and were used without further purification.
Cinnamoyl chloride
Manufactured by Tokyo Chemical Industry
Sourced in Japan
Cinnamoyl chloride is a colorless to pale yellow liquid organic compound used as a laboratory reagent. It is primarily employed in the synthesis of various chemical compounds, particularly in the pharmaceutical and agrochemical industries.
Automatically generated - may contain errors
Lab products found in correlation
Chloroform, by Fujifilm (1 mentions)
Sodium chloride (nacl), by Fujifilm (1 mentions)
Triethylamine, by Fujifilm (1 mentions)
Sodium hydroxide (naoh), by Fujifilm (1 mentions)
1 4 butanediamine, by Fujifilm (1 mentions)
Ethanol, by Fujifilm (1 mentions)
Dimethyl sulfoxide (dmso), by Fujifilm (1 mentions)
N n dimethylformamide (dmf), by Fujifilm (1 mentions)
Triethylamine, by Tokyo Chemical Industry (1 mentions)
2 protocols using cinnamoyl chloride
1
Bioconjugation Reagents for Protein Modification
2
Synthesis of Compound 128 via Cinnamoyl Chloride
Check if the same lab product or an alternative is used in the 5 most similar protocols
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Example 26
To 146 parts of methylene chloride, 5.0 parts of the compound of the formula [57-2] were added, and the mixture was stirred. Subsequently, 3.9 parts of cinnamoyl chloride (manufactured by Tokyo Chemical Industry Co., Ltd.) were added dropwise thereto at room temperature, then 2.3 parts of triethylamine (manufactured by Tokyo Chemical Industry Co., Ltd.) were added dropwise thereto at the same temperature as above, and the mixture was stirred for 1 hour. After the completion of the reaction, deposits were filtered off, and n-hexane was added to the filtrate. The resulting yellow oil substance was isolated, and ethyl acetate was added thereto. The resulting white solid was filtered off, washed with water, and dried in vacuum to obtain compound 128 as a white solid (1.5 parts).
MS(ESI): [M−H]−: cal.: 356.1, found: 356.1.
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