Ftir spectrometer spectrum two model

Intensity data for CCPEHP were collected using the ω–θ2 scan technique on an Agilent SuperNova, (Single source at offset and Eos CCD detector) diffractometer with a SuperNova (Mo) X-ray Source (Mo-Kα, k = 0.71073 Å). The CRYSALISPRO software program was used for cell refinement, data collection and reduction [20] . The FTIR spectrum of the CCPEHP compound was obtained by the Perkin Elmer FTIR-Spectrometer Spectrum Two Model between 400 and 4000 cm⁻¹. Mass spectrum (ESI) was recorded on TSQ Fortis™ Triple Quadrupole Mass Spectrometer LC-MS/MS model device. The FTRaman spectrum was obtained in the region 100–4000 cm⁻¹ with a Thermo Fisher Scientific model DXR™ 3xi Raman Imaging Microscope with 1064 nm Nd: YAG laser source with a resolution of 3 cm⁻¹. The melting point of the crystallized material was determined by the Stuart SMP10 device. The absorption spectrum was recorded using a Shimadzu UV-1800 spectrophotometer between 240 and 800 nm. 3‑chloro-2-hydrazinopyridine, 4′-chloroacetophenone, ethanol, acetonitrile were bought from Sigma Aldrich company.