All starting materials and reagents were obtained from commercial suppliers and were used without further purification. Air- and moisture-sensitive reactions were performed under an argon atmosphere. Flash column chromatography was performed using silica gel 60 (230–400 mesh, Merck KGaA, Darmstadt, Germany) with the indicated solvents. Thin-layer chromatography was performed using 0.25 mm silica gel plates (Merck KGaA). 1H- and 13C-NMR spectra were recorded on a Bruker 600 MHz spectrometer as solutions in deuteriochloroform (CDCl3) or methanol-d4 (Cambridge Isotope Laboratory, Andover, MA, USA). 1H-NMR data were reported in the order of chemical shift, multiplicity (s, singlet; d, doublet, t, triplet; m, multiplet; and/or multiple resonances), number of protons, and coupling constant (J) in hertz (Hz). High-resolution mass spectra (HRMS) were recorded on a JEOL JMS-700 (EI) (JEOL Ltd., Tokyo, Japan) and an Agilent 6530 Q-TOF LC/MS/MS system (ESI) (Agilent Technologies, Inc., Santa Clara, CA, USA).
Agilent 6530 q tof lc ms ms system esi
Manufactured by Agilent Technologies
Sourced in Japan
The Agilent 6530 Q-TOF LC/MS/MS system (ESI) is a high-resolution mass spectrometry instrument capable of performing liquid chromatography-mass spectrometry (LC-MS/MS) analysis. It utilizes electrospray ionization (ESI) to ionize samples for mass analysis.
Automatically generated - may contain errors
3 protocols using agilent 6530 q tof lc ms ms system esi
1
Synthesis and Characterization of Organic Compounds
2
Synthesis and Characterization of Novel Compounds
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All starting materials and reagents were obtained from commercial suppliers and were used without further purification. Air- and moisture-sensitive reactions were performed under an argon atmosphere. Flash column chromatography was performed with silica gel 60 (230–400 mesh, Merck KGaA, Darmstadt, Germany) and the indicated solvents. Thin-layer chromatography was performed using 0.25 mm silica gel plates (Merck KGaA). 1H- and 13C-NMR spectra were recorded on a Bruker 600 MHz spectrometer with solutions of deuteriochloroform (CDCl3) or methanol-d4 (Cambridge Isotope Laboratory, Andover, MA). 1H-NMR data were reported as the order of chemical shift, multiplicity (s, singlet; d, doublet; t, triplet; m, multiplet; and/or multiple resonances), number of protons, and coupling constant (J) in hertz (Hz). High-resolution mass spectra (HRMS) were recorded on a JEOL JMS-700 (EI) (JEOL Ltd., Tokyo, Japan) and Agilent 6530 Q-TOF LC/MS/MS system (ESI) (Agilent Technologies, Inc., Santa Clara, CA).
3
Purification and Characterization of Organic Compounds
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All starting materials and reagents were obtained from commercial suppliers and were used without further purification. Air- and moisture-sensitive reactions were performed under an argon atmosphere. Flash column chromatography was performed using silica gel 60 (230–400 mesh, Merck KGaA, Darmstadt, Germany) with the indicated solvents. Thin-layer chromatography was performed using 0.25 mm silica gel plates (Merck KGaA). 1H- and 13C-NMR spectra were recorded on a Bruker 600 MHz spectrometer as solutions in deuteriochloroform (CDCl3) or methanol-d4 (Cambridge Isotope Laboratory, Andover, MA, USA). 1H-NMR data were reported in the order of chemical shift, multiplicity (s, singlet; d, doublet; t, triplet; m, multiplet; and/or multiple resonances), number of protons, and coupling constant (J) in hertz (Hz). High-resolution mass spectra (HRMS) were recorded on a JEOL JMS-700 (EI) (JEOL Ltd., Tokyo, Japan) and an Agilent 6530 Q-TOF LC/MS/MS system (ESI) (Agilent Technologies, Inc., Santa Clara, CA, USA).
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