acid (8 wt %), ethylene glycol,
polypropylene, polystyrene (pellets, Mw 35000), and polystyrene-block-polybutadiene were
purchased from Sigma-Aldrich. Low-density polyethylene
(powder, 300 μm), poly(ethylene terepththalate) (powder, 300
μm), poly(lactic acid) (pellets, 3 mm), and polyurethane (foam,
10 × 100 × 100 mm3, density 0.08 g cm–3) were obtained from Goodfellow Cambridge Ltd. polypropylene, polystyrene,
polystyrene-block-polybutadiene, poly(lactic acid),
and polyurethane were frozen with liquid N2 and then ground
in a coffee grinder to powders prior to use. NaOD (40 wt % in D2O), KOH (semiconductor grade), KSCN, maleic acid, nickel(II)
chloride hexahydrate, sodium hypophosphite monohydrate, soybean oil,
and terephthalic acid were purchased from Fischer Scientific. D2O (99.96 atom % D) was obtained from Euriso-Top, and TiO2 nanoparticles (P25, 10–30 nm) were purchased from
SkySpring Nanomaterials, Inc. A plastic water bottle (still Scottish
mountain water) was purchased from Marks and Spencer Simply Food,
dried, and ground by using a coffee grinder into pieces ≤0.5
cm2. Polyester microfibers (Homescapes Super Microfibre)
were used as received.