Acrylated epoxidized soybean oil (AESO) containing 4000 ppm monomethyl ether hydroquinone and tert-butyl peroxybenzoate (TBPB) were purchased from Sigma-Aldrich (St. Louis, MO, USA). The UPE used in this study was propylene glycol–isophthalic acid–maleic anhydride (PG-IPA-MA) plastic and the styrene–(PG-IPA-MA) resin, which were obtained from Ashland Inc. (Dublin, OH, USA).
Acrylated epoxidized soybean oil aeso
Manufactured by Merck Group
Sourced in United States, Germany
Acrylated epoxidized soybean oil (AESO) is a versatile chemical compound used in various industrial applications. It is a modified vegetable oil derived from soybean oil. AESO possesses reactive functional groups that can be utilized in various chemical processes and formulations.
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4 protocols using acrylated epoxidized soybean oil aeso
1
Synthesis of Acrylated Epoxidized Soybean Oil
2
Synthesis of Acrylated Epoxidized Soybean Oil
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Acrylated epoxidized soybean oil (AESO, an average number of acryloyl groups per molecule calculated from the 1H-NMR spectrum is 2.7 and 0.3 of epoxide groups) was purchased from Sigma-Aldrich (Darmstadt, Germany). Vanillin dimethacrylate (VDM) and vanillin diacrylate (VDA) were purchased from Specific Polymers. Chloroform was purchased from Chempur (Karlsruhe, Germany). All materials were used without further purification.
3
Biobased Hybrid Polymer Synthesis
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Microcrystalline cellulose (MCC, average particle size: 50 µm) was obtained from Thermo Fisher Scientific (Waltham, MA, USA). Acrylated epoxidized soybean oil (AESO, average molecular weight: 1200 g/mol; viscosity (25 °C): 18,000–32,000 mPa·s; acid value: ≤10 mg KOH/g; inhibitor: 3500–4500 ppm monomethyl ether hydroquinone), tert-butyl peroxybenzoate (TBPB, 98%), and acetone (≥99.9%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). All the chemicals were used as received.
4
Thiol-Epoxy Photocurable Hybrid Polymers
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Acrylated epoxidized soybean oil (AESO, an average number of acryloyl groups per molecule 2.7 and 0.3 of epoxide groups), benzene-1,3-dithiol (1,3BDT), pentaerythritol tetra(3-mercaptopropionate) (PETMP), 1-methylimidazole (1MI), and 4-methyl-2-pentanone were purchased from Sigma-Aldrich (Darmstadt, Germany). Epoxidized linseed oil (ELO, having an average number of 6 epoxy groups per molecule) was purchased from Chemical Point (Oberhaching, Germany). Photoinitiator ethyl(2,4,6-thimethylbenzoyl) phenyl phosphinate (TPOL) was purchased from Fluorochem (Hadfield, Derbyshire, UK). All materials were used as received.
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