Log In Sign up
The largest database of trusted experimental protocols

Hexachlorocyclotriphosphazene

Manufactured by Merck Group
Visit Supplier
Sourced in Canada, United States, Germany

Hexachlorocyclotriphosphazene is a chemical compound with the formula (NPCl2)3. It is a colorless, crystalline solid used as a precursor in the synthesis of various phosphorus-containing compounds. The product serves as a building block for the development of advanced materials and specialized applications, though its specific uses are not detailed here.

Automatically generated - may contain errors

Lab products found in correlation

Aluminum trichloride, by Merck Group (1 mentions) Trimethylamine, by Thermo Fisher Scientific (1 mentions) Anhydrous tetrahydrofuran, by Merck Group (1 mentions) Anhydrous acetonitrile, by Thermo Fisher Scientific (1 mentions) Anhydrous dimethyl sulfoxide, by Thermo Fisher Scientific (1 mentions) 2 methoxyethylamine, by Merck Group (1 mentions) P phenylenediamine, by Merck Group (1 mentions) 1 4 dioxane, by Merck Group (1 mentions) Ethanol, by Merck Group (1 mentions) Cyclohexane, by Merck Group (1 mentions) 1 3 5 trihydroxybenzene, by Merck Group (1 mentions) Dimethyl sulfoxide (dmso), by Merck Group (1 mentions) Potassium hydroxide, by Merck Group (1 mentions) Glutaric anhydride, by Thermo Fisher Scientific (1 mentions) Methoxy poly ethylene glycol, by Merck Group (1 mentions) 4 dimethylaminopyridine dmap, by Thermo Fisher Scientific (1 mentions) Histamine dihydrochloride, by Merck Group (1 mentions) Docetaxel, by Merck Group (1 mentions)

5 protocols using hexachlorocyclotriphosphazene

1

Synthesis of Phosphazene-Containing Polymers

Check if the same lab product or an alternative is used in the 5 most similar protocols
PEO (average Mv = 600,000; Sigma-Aldrich) was dried at 50 °C for 24 h under
vacuum before use. Hexachlorocyclotriphosphazene (HCCP, 99%), aluminum
trichloride (AlCl3, 99.9%), 2-methoxyethylamine (99%),
3-methoxypropylamine (99%), n-butyllithium (2.5 M
in hexanes), and anhydrous tetrahydrofuran (THF; 99.9%) were purchased
from Sigma-Aldrich and used without further purification. 2,2,2-Trifluoroethylamine
(98%), Li foil (99.9%), trimethylamine (TEA, 99%), anhydrous acetonitrile
(ACN; 99.8%), and anhydrous dimethyl sulfoxide (DMSO; 99.8%) were
purchased from Fisher Scientific and used as received. LiFePO4 (LFP, 99.5%; Gelon) and Super C45 Carbon Black were dried
at 60 °C before use. All synthesis procedures were carried out
on a Schlenk line under N2, and all other air- and/or moisture-sensitive
procedures were carried out in an Ar-filled glovebox (H2O and O2 less than 1 ppm).
Johnson B.R., Sankara Raman A., Narla A., Jhulki S., Chen L., Marder S.R., Ramprasad R., Turcheniuk K, & Yushin G. (2024). Polyphosphazene-Based Anion-Anchored Polymer Electrolytes For All-Solid-State Lithium Metal Batteries. ACS Omega, 9(13), 15410-15420.
+ Open protocol
+ Expand
2

Synthesis of Phosphazene Derivative

Check if the same lab product or an alternative is used in the 5 most similar protocols
Hexachlorocyclotriphosphazene, p-phenylenediamine,
1.4-dioxane, ethanol, acetone, and triethylamine
were purchased from Sigma-Aldrich (Oakville, ON, Canada). Deionized
(DI) water was produced by a water purification machine (Milli-Q Reference).
1.4-dioxane was dried using 4 Å molecular sieves before being
used.
Rhili K., Chergui S., Samih ElDouhaibi A., Mazzah A, & Siaj M. (2023). One-Pot Synthesis of Cyclomatrix-Type Polyphosphazene Microspheres and Their High Thermal Stability. ACS Omega, 8(10), 9137-9144.
+ Open protocol
+ Expand
3

Hexachlorocyclotriphosphazene-Based Porous Ceramics

Check if the same lab product or an alternative is used in the 5 most similar protocols
Hexachlorocyclotriphosphazene
(HCCP, 99%), 1,3,5-trihydroxybenzene (THB or phloroglucinol, ≥99%), m-dihydroxybenzene (MDHB, ≥99.9%), p-dihydroxybenzene (PDHB, ≥99.9%), and dimethylsulfoxide (DMSO,
anhydrous, ≥99.9%) were obtained from Sigma-Aldrich. Cyclohexane
(EMSURE for analysis) and potassium hydroxide (KOH, pellets extra
pure) were supplied from Merck. All chemicals and solvents were used
as received. Macroporous α-alumina disks with a diameter of
39 mm, a thickness of 2 mm, and a pore size of 80 nm were obtained
from Pervatech B.V. and used as the support.
Radmanesh F., Tena A., Sudhölter E.J., Hempenius M.A, & Benes N.E. (2023). Nonaqueous Interfacial Polymerization-Derived Polyphosphazene Films for Sieving or Blocking Hydrogen Gas. ACS Applied Polymer Materials, 5(3), 1955-1964.
+ Open protocol
+ Expand
4

Synthesis of Amphiphilic Poly(organophosphazene) Conjugates

Check if the same lab product or an alternative is used in the 5 most similar protocols
Hexachlorocyclotriphosphazene was purchased from Sigma-Aldrich (USA) and purified by sublimation at 55 °C under vacuum (about 0.1 mmHg). Poly(dichlorophosphazene) was prepared as described previously [42 (link)]. Methoxy poly(ethylene glycol) with molecular weight of 750 Da (Sigma-Aldrich, USA) was substituted to α-amino-ω-Methoxy poly(ethylene glycol) (AMPEG) to substitute to the poly(organophosphazene) backbone as described in our previous work. The l-Isoleucine ethyl ester hydrochloride (IleOEt•HCl)(A&Z food additives, HangZhou, china, aminoethanol (Sigma-Aldrich, USA), glutaric anhydride (Alfa Aesar, USA), and 4-(dimethylamino) pyridine (DMAP)(Alfa Aesar, USA) were purchased. Tetrahydrofuran (THF) and trimethylamine (TEA) were dried by reflux over sodium metal and barium oxide respectively under dry nitrogen. Triamcinolone acetonide (TCA) was purchased from TCI (Japan). All other reagents were purchased from commercial suppliers.
Seo B.B., Kwon Y., Kim J., Hong K.H., Kim S.E., Song H.R., Kim Y.M, & Song S.C. (2021). Injectable polymeric nanoparticle hydrogel system for long-term anti-inflammatory effect to treat osteoarthritis. Bioactive Materials, 7, 14-25.
+ Open protocol
+ Expand
5

Synthesis and Characterization of PEGylated Docetaxel Conjugates

Check if the same lab product or an alternative is used in the 5 most similar protocols
Hexachlorocyclotriphosphazene (99.95%) was purchased from Sigma-Aldrich (Steinheim, Germany) and purified by sublimation at 80–90 °C before use. Aluminum chloride (AlCl3, Reagent Plus, 99%), methoxypolyethylene glycol amine (PEG–NH2, molecular weight 2000, extent of labeling: ≥ 0.4 mmol/g NH2 loading), histamine dihydrochloride (Hys, ≥99.0% (AT)), methyl-p-aminobenzoate (MAB, 98%) and Docetaxel (purum, ≥97.0% (HPLC)) were acquired from Sigma-Aldrich (Steinheim, Germany) and used without further purification. All other reagents were purchased from commercially available sources and used without further purification. Adriamycin-resistant MCF-7 human breast cancer cell line was acquired from the European Collection of Cell Cultures (ECACC).
Serbezeanu D., Vlad-Bubulac T., Macsim A.M, & Bǎlan V. (2023). Design and Synthesis of Amphiphilic Graft Polyphosphazene Micelles for Docetaxel Delivery. Pharmaceutics, 15(5), 1564.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!