X-ray thermodiffractometry was performed for compound 1 under a 5 L h−1 nitrogen flow in an Anton Paar HTK1200N of a D8 Advance Bruker diffractometer (θ–θ mode, CuKα radiation) equipped with a Vantec1 linear position sensitive detector (PSD). Each powder pattern was recorded in the range 5–50° (2θ) (at intervals of 20 °C between RT and 800 °C) with a 1 s per step scan, corresponding to an approximate duration of 37 min. The temperature ramps between two patterns were 5 °C min−1.
Htk1200n
Manufactured by Bruker
Sourced in Germany
The HTK1200N is a high-temperature chamber from Bruker. It is designed for x-ray diffraction measurements at high temperatures up to 1200°C.
Automatically generated - may contain errors
4 protocols using htk1200n
1
Thermal X-Ray Diffraction of Compound 1
2
In-situ and Operando X-ray Analysis of P2 Phase Synthesis
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
To determine the best synthesis
condition for the desired P2 phase, in situ X-ray
diffraction (XRD) for synthesis was performed using an HTK1200N temperature
chamber installed on a Bruker D8 Advance diffractometer. At each designed
temperature, the temperature was held for 1 h for the XRD pattern
collection. Operando XRD of the samples was performed
on the Bruker D8 Advance diffractometer equipped with a molybdenum
source (λ = 0.709 Å). The in situ cell
was charged/discharged within a voltage domain of 1.5–4.5 V
at a rate of C/30. Each scan covered a 2θ range of 6.5–23°
in a time duration of 5000 s. The electrochemical cell used for the operando XRD measurement is similar to those used in our
previous publication.28 (link) Selected powder
samples were also tested using the synchrotron radiation source (λ
= 0.4539 Å) at beamline 17-BM at the Advanced Photon Source (APS)
at Argonne National Laboratory (ANL). Some additional synchrotron
experiments were also performed using 28-ID-2 beamline of the National
Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory
and the 7-2 beamline of Stanford Synchrotron Radiation Lightsource
(SSRL). Morphological investigation and energy-dispersive X-ray spectroscopy
(EDS) mapping analysis of the samples was conducted using a field
emission scanning electron microscopy (FE-SEM, Zeiss, Ultra60).
condition for the desired P2 phase, in situ X-ray
diffraction (XRD) for synthesis was performed using an HTK1200N temperature
chamber installed on a Bruker D8 Advance diffractometer. At each designed
temperature, the temperature was held for 1 h for the XRD pattern
collection. Operando XRD of the samples was performed
on the Bruker D8 Advance diffractometer equipped with a molybdenum
source (λ = 0.709 Å). The in situ cell
was charged/discharged within a voltage domain of 1.5–4.5 V
at a rate of C/30. Each scan covered a 2θ range of 6.5–23°
in a time duration of 5000 s. The electrochemical cell used for the operando XRD measurement is similar to those used in our
previous publication.28 (link) Selected powder
samples were also tested using the synchrotron radiation source (λ
= 0.4539 Å) at beamline 17-BM at the Advanced Photon Source (APS)
at Argonne National Laboratory (ANL). Some additional synchrotron
experiments were also performed using 28-ID-2 beamline of the National
Synchrotron Light Source II (NSLS-II) at Brookhaven National Laboratory
and the 7-2 beamline of Stanford Synchrotron Radiation Lightsource
(SSRL). Morphological investigation and energy-dispersive X-ray spectroscopy
(EDS) mapping analysis of the samples was conducted using a field
emission scanning electron microscopy (FE-SEM, Zeiss, Ultra60).
3
Thermal Analysis of Material Composition
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Thermogravimetric analysis was performed on a thermoanalyzer 92 SETARAM TGA up to 800 °C, in air, with a heating rate of 5 °C.min -1 .
X-ray thermodiffractometry was performed under 5l.h -1 air flow in an Anton Paar HTK1200N of a D8 Advance Bruker diffractometer (- mode, CuKα radiation) equipped with a Vantec1 linear position sensitive detector (PSD). Each powder pattern was recorded in the range 5-60° (2) (at intervals of 20°C up to 800°C) with a 0.5 s/step scan, corresponding to an approximate duration of 30 mn.
X-ray thermodiffractometry was performed under 5l.h -1 air flow in an Anton Paar HTK1200N of a D8 Advance Bruker diffractometer (- mode, CuKα radiation) equipped with a Vantec1 linear position sensitive detector (PSD). Each powder pattern was recorded in the range 5-60° (2) (at intervals of 20°C up to 800°C) with a 0.5 s/step scan, corresponding to an approximate duration of 30 mn.
4
Structural and Morphological Characterization
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The structural and phase purity was studied employing a high-temperature powder X-ray diffractometer (HT-XRD) equipped with an HTK 1200N—Bruker D8 Advance, Leipzig, Germany. Additionally, small changes in the structural morphology and disorder of the carbon nanomaterials were detected using micro–laser Raman instruments (Seiki, Japan). Furthermore, the morphologies of the sample were examined through the utilization of a CAREL ZEISS EVO 18, Oberkochen, Germany scanning electron microscope and a JEOL-2100+ high-resolution transmission electron microscope, Tokyo, Japan. The composition and chemical state of the Ni-MgO/CNT were examined employing a PHI-VERSAPROBE III—X-ray photoelectron spectrometer, (ULVAC, Chigasaki, Japan). An electrochemical study was conducted employing a Biologic SP-150 instrument, Seyssinet-Pariset, France to investigate the electrochemical properties of the system under study.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!