1 2 dichlorobenzene dcb

Manufactured by Merck Group

Sourced in United States

1,2-dichlorobenzene (DCB) is a colorless liquid chemical compound. It has a characteristic aromatic odor. DCB is commonly used as a laboratory solvent and as an intermediate in the production of other chemicals.

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Dichlorobenzene (DCB;

6 protocols using 1 2 dichlorobenzene dcb

Carbohydrate-Functionalized Carbon Nanotube Bioconjugates

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The SWNTs were obtained from Unidym (HiPco, Lot# P2150). Methyl pentafluorobenzoate, D-(+)-mannose, β-D-(+)-galactose pentaacetate, 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid (HEPES), sodium metabisulfide (Na₂S₂O₅) and palladium (10% on carbon) were purchased from Alfa Aesar. Boron trifluoride ethyl etherate (BF₃·Et₂O), N-hydroxysuccinimide (NHS), N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride (EDAC·HCl), 1, 2-dichlorobenzene (DCB), and bovine serum albumin (BSA) were obtained from Sigma-Aldrich. Sodium azide (NaN₃) and sodium methoxide (CH₃ONa) were acquired from Fluka. 2-[2-(2-Chloroethoxy)-ethoxy]ethanol was obtained from TCI Japan. Concanavalin A (fluorescein conjugate, lectin from Jack bean) was purchased from Molecular Probes (Eugene, Oregon). All chemicals were used as received without purification. Water used was from a Milli-Q ultrapure water purification system. PFPA-NHS was synthesized following previously reported procedures.^{40 (link), 41 (link)} Man-EG₂-NH₂ and Gal-EG₂-NH₂ were synthesized following previously established procedures (see Supporting Information for detailed synthesis and characterization).^{42 (link)–44}

Kong N., Shimpi M.R., Park J.H., Ramström O, & Yan M. (2014). Carbohydrate Conjugation through Microwave-Assisted Functionalization of Single-Walled Carbon Nanotubes Using Perfluorophenyl Azides. Carbohydrate research, 405, 33-38.

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Organic Photovoltaic Materials Fabrication

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PEDOT:PSS (Clevios P VP AI. 4083) was purchased from Baytron, H.C. Starck, Inc. P3HT (molecular weight (M_W) = 4,500) and PC₆₁BM (M_W = 910.88) were obtained from Luminescence Technology Corp., Taiwan. 1,2-dichlorobenzene (DCB) (anhydrous, 99%) was purchased from Sigma–Aldrich and DOH was purchased from Tokyo Chemical Industry Co., Ltd. and used as received.

Xu B., Gopalan S.A., Gopalan A.I., Muthuchamy N., Lee K.P., Lee J.S., Jiang Y., Lee S.W., Kim S.W., Kim J.S., Jeong H.M., Kwon J.B., Bae J.H, & Kang S.W. (2017). Functional solid additive modified PEDOT:PSS as an anode buffer layer for enhanced photovoltaic performance and stability in polymer solar cells. Scientific Reports, 7, 45079.

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Organic Photovoltaic Materials Synthesis

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The polymers poly[N-9″-heptadecanyl-2,7-carbazole-alt-5,5-(4′,7′-di-2-thienyl-2′,1′,3′-benzothiadiazole)
(PCDTBT) and poly[4,8-bis[(2-ethylhexyl)oxy]benzo[1,2-b:4,5-b′]dithiaphene-2,6-diyl][3-fluro-2-[(2-ethylhexyl)cabonyl]thieno[3,4-b]thiophenyldiyl]] (PTB7) and acceptor phenyl-C₇₁-butyric acid methyl ester (PC₇₁BM) were purchased from
Ossila Limited, United Kingdom. Copper bromide (CuBr) and solvents
such as 1,2-dichlorobenzene (DCB), chlorobenzene (CB), diiodooctane
(DIO), MeCN, DMSO, and DMF were purchased from Sigma Aldrich. All
these commercially available chemicals were used without further purification.

Bhargav R., Chaudhary N., Rathi S., S.h.a.h.j.a.d., Bhardwaj D., Gupta S, & Patra A. (2019). Copper Bromide as an Efficient Solution-Processable Hole Transport Layer for Organic Solar Cells: Effect of Solvents. ACS Omega, 4(3), 6028-6034.

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Tetraphenylporphyrin Synthesis and Characterization

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5,10,15,20-Tetrakis(4-aminophenyl)-21H,23H-porphyrin (Tph) and 4-ethylpyridine
(epy) were purchased from TCI (Tokyo, Japan). Acetic acid was purchased
from Nacalai Tesque (Kyoto, Japan). Cytochrome c from
bovine heart, TMB, 1,2-dichlorobenzene (DCB), and 2,5-dimethoxy-1,4-dibenzaldehyde
were purchased from Sigma-Aldrich (Missouri, USA). Other reagents
were purchased from FUJIFILM Wako (Tokyo, Japan). All chemicals were
used without further purification.

Li X., Nomura K., Guedes A., Goto T., Sekino T., Fujitsuka M, & Osakada Y. (2022). Enhanced Photocatalytic Activity of Porphyrin Nanodisks Prepared by Exfoliation of Metalloporphyrin-Based Covalent Organic Frameworks. ACS Omega, 7(8), 7172-7178.

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Synthesis of Perovskite and Titanate Heterostructures

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Hombikat UV100 (UV100, Venator, Wynyard, UK), sodium hydroxide (NaOH, Fisher Scientific, Hampton, NH, USA), hydrochloric acid (HCl, 37%, Fisher Scientific) and deionized water (DI) were used to synthesize pristine hydrogen titanate. Bismuth bromide (BiBr₃, Sigma-Aldrich, St. Louis, MO, USA), cesium bromide (CsBr, Sigma-Aldrich), dimethyl sulfoxide (DMSO, Sigma-Aldrich) and isopropanol (IPA, Sigma-Aldrich) was used to synthesize pristine Cs₃Bi₂Br₉ and Cs₃Bi₂Br₉/Hydrogen Titanate heterostructures. benzyl alcohol (BnOH, Sigma-Aldrich), Acetonitrile (MeCN, Sigma-Aldrich) and 1,2-dichlorobenzene (DCB, Sigma-Aldrich) were used for benzyl alcohol oxidation experiments. Potassium iodide (KI, Sigma-Aldrich), silver nitrate (AgNO₃, Sigma-Aldrich), p-benzoquinone (p-BQ, Sigma-Aldrich) and tert-butyl alcohol (TBA, Sigma-Aldrich) were used for scavenger tests to identify the main reactive oxygen species (ROSs) responsible for BnOH conversion. All chemical reagents were used in purities >99% as received without any further purification.

Awang H., Hezam A., Peppel T, & Strunk J. (2024). Enhancing the Photocatalytic Activity of Halide Perovskite Cesium Bismuth Bromide/Hydrogen Titanate Heterostructures for Benzyl Alcohol Oxidation. Nanomaterials, 14(9), 752.

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Regioregular P3HT Polymer Purification

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The regioregular poly (3-hexyl-thiophene-2,5-diyl) (rr-P3HT) was purchased from American Dye Source, Inc. and used without further purification. Cyclohexanone (CHN) was purchased from AKS, Atabay Pharmaceutical Products Inc., Turkey and used as a poor solvent while 1,2-dichlorobenzene (DCB) was purchased from Sigma-Aldrich, USA and used as a main solvent for rr-P3HT polymer.

Kiymaz D., Yagmurcukardes M., Tomak A., Sahin H., Senger R.T., Peeters F.M., Zareie H.M, & Zafer C. (2016). Controlled growth mechanism of poly (3-hexylthiophene) nanowires. Nanotechnology, 27(45).

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