The largest database of trusted experimental protocols

Frontier fourier transform infrared spectrometer

Manufactured by PerkinElmer

The Frontier Fourier transform infrared (FTIR) spectrometer is a versatile analytical instrument used to identify and quantify a wide range of chemical compounds. It measures the interaction between infrared light and the chemical bonds within a sample, generating a unique spectrum that can be used to detect and analyze the composition of the sample.

Automatically generated - may contain errors

5 protocols using frontier fourier transform infrared spectrometer

1

Comprehensive Characterization of Material Samples

Check if the same lab product or an alternative is used in the 5 most similar protocols
Transmission electron
microscopy (TEM)
and high-resolution transmission electron microscopy (HR-TEM) images
were collected using a JEM-2100 transmission electron microscope (JEOL,
Ltd., Tokyo, Japan). Proton nuclear magnetic resonance (1H NMR) spectra were measured in dimethyl sulfoxide (DMSO) using an
AVANCE III HD 500 MHz spectrometer (BrukerCorp, Karlsruhe, Germany).
X-ray photoelectron spectroscopy (XPS) was carried out using an Escalab
250Xi X-ray photoelectron spectrometer (Thermo Fisher Scientific Co.,
Ltd., Shanghai, China). The FTIR spectra were collected using a frontier
Fourier transform infrared spectrometer (PerkinElmer Co., Ltd., Waltham,
MA). The UV–vis absorption spectra were recorded using a TU-1950
ultraviolet–visible spectrofluorometer (Persee General Instrument
Co., Ltd., Beijing, China). Photoluminescence (PL) measurements were
carried out using an LS55 fluorescence spectrometer (PerkinElmer Co.,
Ltd.). Fluorescence decay curves were measured using a DeltaFlex modular
fluorescence lifetime instrument (Horiba Jobin Yvon IBH Ltd., Glasgow,
U.K.). PL quantum yields were measured using an FLS1000 fluorescence
spectrometer (Edinburgh Instruments, Ltd., Edinburgh, U.K.). Fluorescence
images were captured using a DMI4000 B inverted fluorescence microscope
(Leica Microsystems Inc., Wetzlar, Germany).
+ Open protocol
+ Expand
2

Elemental Composition and IR Spectroscopy of HA-LIG and HA-CYN

Check if the same lab product or an alternative is used in the 5 most similar protocols
The elemental composition of HA-LIG and HA-CYN was determined with a Fison EA 1108 Elemental Analyzer. Infrared (IR) spectra were recorded on a Perkin–Elmer Frontier Fourier transform infrared spectrometer using an attenuated total reflection (ATR) device equipped with a diamond/ZnSe crystal. About 2 mg of finely ground powder was inserted in the crystal device and the contact was obtained applying on sample a strength of about 150 N. Each spectrum was subjected to 32 scans with the resolution of 4 cm−1 in the 4000–400 cm−1 region.
+ Open protocol
+ Expand
3

FTIR Analysis of Dried Films

Check if the same lab product or an alternative is used in the 5 most similar protocols
A PerkinElmer frontier Fourier transform infrared spectrometer
(PerkinElmer) was used to record the spectra of the dried films and
individual film components. The spectral resolution was 4 cm–1, and 32 scans were acquired for each spectrum (4000–400 cm–1). The FTIR spectra of the samples were acquired directly.
+ Open protocol
+ Expand
4

Detailed Characterization of Porous Carbon

Check if the same lab product or an alternative is used in the 5 most similar protocols
N2 adsorption–desorption analysis was performed at 77 K using a TriStar (Micromeritics Instrument Corp.; Norcross, GA, USA), equipped with automated surface area and pore size analyser. Before analysis, samples were degassed at 200 °C for 24 h. CO2 adsorption isotherms were acquired at 273 K using a Quantachrome Autosorb-1. Before analysis, samples were allowed to outgas at 200 °C under turbomolecular vacuum pumping for a minimum of 15 h. For TEM and STEM characterization, samples were dispersed in ethanol using an ultrasonic bath. The final suspensions were transferred to TEM grids and dried in ambient air before electron microscopy analysis. The material morphology was visualized using STEM-HAADF images and electron energy loss spectroscopy on a Nion UltraSTEM 200 microscope operated at 200 kV. Powder X-ray diffraction (XRD) and SAXS were measured on a Bruker D8 diffractometer equipped with scintillation counter. The Zn and Ni contents were measured by inductively coupled plasma-atomic emission spectroscopy. All gas chromatography experiments were carried out and recorded by Agilent Technology 7890A. Fourier transform infrared spectrum was collected by PerkinElmer Frontier Fourier transform infrared spectrometer. Mimosa tannin from SILVACHIMICA S.r.l. (Italy) was used as the carbon precursor.
+ Open protocol
+ Expand
5

Structural Elucidation of Organic Compounds

Check if the same lab product or an alternative is used in the 5 most similar protocols
General information: Solvents and reagents were purchased from commercial suppliers TCI Chemicals (Tokyo, Japan), Sigma-Aldrich (Bangalore, India), and Fluka (Dorset, UK). Structure determination was conducted by analyzing the 1H, 13C, and 19F NMR spectra (Bruker 300 apparatus) and the infrared (IR) spectrum was determined using PerkinElmer Frontier Fourier-transform infrared spectrometer. Melting point was conducted using Stuart SMP2 melting point apparatus and high-resolution mass spectroscopy was analyzed by Thermo scientific, Orbitrap Q Exactive Focus.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!