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Thermo nicolet is5

Manufactured by Thermo Fisher Scientific
Sourced in United States

The Thermo Nicolet iS5 is a compact and versatile Fourier Transform Infrared (FTIR) spectrometer designed for routine analysis. It provides reliable performance and easy-to-use operation for a wide range of applications.

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3 protocols using thermo nicolet is5

1

Characterization of Activated Carbon Surface

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The surface morphologies of the AC samples were characterized using scanning electron microscopy (SEM; EM-30 Plus, COXEM, Daejeon, Korea). For better observation, the samples were sprayed with gold before testing to increase their surface conductivities.
The AC surface functional groups were identified via Fourier transform infrared spectroscopy (FTIR, Thermo Nicolet iS5, Thermo Fisher Scientific, Waltham, MA, USA). The samples were characterized in the infrared region using the potassium bromide sheet method at 25 °C with wavenumbers ranging from 4000 to 600 cm−1, 32 scans and 4 cm−1 resolution. The sample profiles were retrieved and analyzed using an infrared atlas database.
The nitrogen adsorption–desorption isotherms and other pore properties were determined at a pretreatment temperature of 200 °C and time of 6 h using a surface-area pore analyzer (ASAP 2460, Mac, Atlanta, GA, USA). The Brunauer–Emmett–Teller (BET) method was used to calculate the specific surface area.
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2

Infrared Spectroscopic Analysis of MSNN Compounds

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The infrared (IR) spectra of MSNN, MIT, MTX, MSNN+MTX, MSNN−MTX, MSNN−MIT, and MSNN−MTX/MIT were recorded using a FT-IR spectrometer (Thermo Nicolet IS5, Thermo Fisher Scientific, Waltham, MA, USA). Approximately 1 mg sample of MSNN or MIT or MTX or MSNN+MTX or MSNN−MTX or MSNN−MIT or MSNN−MTX/MIT was measured using the KBr pellet method at room temperature.
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3

Analytical Techniques for WPCB Characterization

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Atomic
absorption spectrophotometers (PerkinElmer, Pin AAcle 900F, USA) are
used to determine the concentration of copper ions in solutions. Scanning
electron microscopy (SEM, HITACHI, Regulus8100, Japan) and energy-dispersive
spectroscopy were used to analyze the morphology and elemental distribution
of WPCB particles before and after microwave pretreatment. A Fourier
transform infrared (FT-IR) spectrometer (Thermo Fisher, Thermo Nicolet
iS5, USA) was used to measure changes in chemical bond types before
and after WPCB pretreatment; X-ray fluorescence (XRF, PANalytical,
Axios, Netherland) spectrometry is used to measure elements and content
in WPCB; and analytical balances (METTLER TOLEDO, AL-104, China) are
used to measure the mass of WPCB in different particle size intervals.
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