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Nitric acid 65

Manufactured by Thermo Fisher Scientific

Nitric acid 65 is a highly concentrated solution of nitric acid in water. It is a strong oxidizing agent and a corrosive chemical. The core function of Nitric acid 65 is to serve as a reagent in various laboratory and industrial applications.

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2 protocols using nitric acid 65

1

Rhenium Quantification Protocol

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The ICP-OES was used to estimate the rhenium amount in the sample. The film was digested for four hours in 4 ml of nitric acid (Nitric acid 65%, Fisher Scientific), and the small probe was diluted ten times with Milli-Q water containing 5% HNO3 and filtered with 0.2-μm syringe filters (Whatman) before measurement. Avio 200 Scott/Cross-Flow Configuration was used for ICP measurements. A calibration curve was formed for the measurements using a Rhenium Calibration Standard (Merk). Concentrations of 0, 0.1, 1 and 10 ppm of the Re were used to create a four-point linear regression. All measured values are within a relative standard deviation (RSD) of 2%.
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2

Cobalt Content Determination by ICP-OES

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The ICP-OES was used to estimate the cobalt amount in the sample. The film was digested in 4 mL of nitric acid (FisherScientific, nitric acid 65%) for several hours. Before measurement, the small probe was diluted 10 times with Milli-Q water containing 2% HNO3 and filtered with 0.2 μm syringe filters (Whatman). Avio 200 Scott/Cross-Flow Configuration was used for ICP measurements. A calibration curve was formed for the measurements using a Cobalt Calibration Standard (CPAchem). Concentrations of 0, 0.1, 1 and 10 ppm of the Co were used to create a 4-point linear regression. All measured values are within a relative standard deviation (RSD) of 2%.
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