All the solvents and reagents used for synthesis were of analytical grade that were purchased from Oakwood Chemicals and Sigma Aldrich. The reaction was carried out under standard conditions using oven-dried round bottom flask. Progress of the reaction was monitored by TLC using silica-gel based thin layers in a solvent ratio 1 : 3 (ethyl acetate: petroleum ether). All the ions such as fluoride (F−), bromide (Br−), acetate (AcO−), chloride (Cl−), cyanide (CN−), perchlorate, and bisulfate in the form of tetra butyl ammonium salts were purchased from Sigma Aldrich. The structure of synthesized chemosensors IF-1 and 1F-2 were confirmed using 1H-NMR, HRMS and UV-visible characterization techniques. Solvents used for analysis were of spectroscopic grade. 1H-NMR and 13C NMR spectra were obtained at frequencies 300 MHz and 100 MHz respectively in DMSO-d6 solvent where TMS was used as internal standard. The absorption and transmission studies of light (UV-vis spectroscopy) were recorded using Shimadzu UV-1800 spectrophotometer.
Bisulfate
Manufactured by Merck Group
Bisulfate is a laboratory chemical compound used as a reagent in various analytical and synthetic processes. It serves as a source of sulfite ions and can be used to adjust the pH of solutions. Bisulfate is commonly employed in applications that require controlled sulfur-based chemistry, though its specific use cases may vary depending on the application and research field.
Automatically generated - may contain errors
Lab products found in correlation
Tetrabutyl ammonium salts, by Merck Group (1 mentions)
Uv 1800 spectrophotometer, by Shimadzu (1 mentions)
Periodate, by Merck Group (1 mentions)
Potassium dichromate, by Merck Group (1 mentions)
Rosmarinic acid, by Merck Group (1 mentions)
Agarose, by Merck Group (1 mentions)
Hepes buffer, by Merck Group (1 mentions)
Agno3, by SD Fine Chemicals (1 mentions)
Sodium borohydride, by Merck Group (1 mentions)
Ascorbic acid, by Merck Group (1 mentions)
Sodium phosphate monobasic, by Merck Group (1 mentions)
2 protocols using bisulfate
1
Synthesis and Characterization of Chemosensors
2
Spectrophotometric Analysis of Anionic Salts
Check if the same lab product or an alternative is used in the 5 most similar protocols
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Rosmarinic acid, sodium borohydride, ascorbic
acid, HEPES buffer, sodium phosphate monobasic, and agarose (low melting
point) were purchased from Sigma-Aldrich. AgNO3 was purchased
from S. D. Fine Chemicals. Tetrabutylammonium (TBA+) salts
of fluoride, bromide, chloride, iodide, periodate, cyanide, dihydrogen
phosphate, acetate, nitrate, and bisulfate were purchased from Sigma
Aldrich. Potassium dichromate was purchased from Merck Ltd. Solutions
of all the chemicals were prepared in Milli-Q water.
acid, HEPES buffer, sodium phosphate monobasic, and agarose (low melting
point) were purchased from Sigma-Aldrich. AgNO3 was purchased
from S. D. Fine Chemicals. Tetrabutylammonium (TBA+) salts
of fluoride, bromide, chloride, iodide, periodate, cyanide, dihydrogen
phosphate, acetate, nitrate, and bisulfate were purchased from Sigma
Aldrich. Potassium dichromate was purchased from Merck Ltd. Solutions
of all the chemicals were prepared in Milli-Q water.
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