All the chemicals used in this study were of analytical reagent grade from regular sources and doubly distilled water (DDW) was used to prepare all the solutions. Sodium nitrate, sodium hydroxide, hydrochloric acid and ethanol were supplied by Merck. Nitrate reductase, 3-nitroaniline and 1-naphthylamine were purchased from Sigma. A stock 0.1 M solution of Sodium nitrate was prepared by exact weighing and dissolution of its solid powder in DDW and nitrate working solutions were prepared by diluting the stock solution to appropriate volumes. The Griess reagent including 3-nitroaniline (2.5 × 10−3 M), 1-naphthylamine (2.5 × 10−2 M) and hydrochloric acid (1.5 × 10−4 M) was prepared in DDW/ethanol mixture (50 : 50, v/v%).
1 naphthylamine
Manufactured by Merck Group
Sourced in China, United States, Germany, India
1-naphthylamine is a chemical compound used in laboratory settings. It serves as a starting material for the synthesis of various organic compounds. The core function of 1-naphthylamine is to provide a building block for further chemical reactions and transformations, as required in various research and analytical applications.
Automatically generated - may contain errors
Lab products found in correlation
2 naphthol, by Merck Group (2 mentions)
N n dimethylformamide (dmf), by Merck Group (2 mentions)
Hydrochloric acid (hcl), by Merck Group (2 mentions)
Ethanol, by Merck Group (2 mentions)
Aniline, by Merck Group (2 mentions)
Calcium nitrate trihydrate, by Merck Group (2 mentions)
Barbituric acid, by Merck Group (2 mentions)
Glucose, by Merck Group (2 mentions)
Tetraethyl orthosilicate, by Merck Group (2 mentions)
Nickel nitrate hexahydrate, by Merck Group (2 mentions)
Nitrate reductase, by Merck Group (1 mentions)
3 nitroaniline, by Merck Group (1 mentions)
Sodium hydroxide (naoh), by Merck Group (1 mentions)
Sodium nitrate, by Merck Group (1 mentions)
M dinitrobenzene, by Merck Group (1 mentions)
O dichlorobenzene, by J&K Scientific (1 mentions)
1 3 5 trimethylbenzene, by Maclin Biochemical Technology (1 mentions)
M xylene, by Merck Group (1 mentions)
P xylene, by Merck Group (1 mentions)
Naphthalene, by Merck Group (1 mentions)
11 protocols using 1 naphthylamine
1
Griess Reagent Preparation Protocol
2
Characterization of Aromatic Compounds and Graphene Derivatives
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The aromatic compounds used in this study included benzene (99.5%; Shanghai Lingfeng Chemical Reagent Co. Ltd., China), naphthalene (99%; Sigma-Aldrich), phenanthrene (98%; Sigma-Aldrich), 1-naphthylamine (98%; Sigma-Aldrich), 2-naphthol (99%; Sigma-Aldrich), chlorobenzene (99.0%; Shanghai Lingfeng Chemical Reagent Co. Ltd.), o-dichlorobenzene (99%; J&K Chemical, China), m-dichlorobenzene (97%; Sigma-Aldrich), p-dichlorobenzene (99.5%; Fluka, Switzerland), 1,2,4-trichlorobenzene (99.0%; Fluka), 1,3,5-trichlorobenzene (99%; Supelco, USA), p-chlorophenol (99%; Alfa Aesar, USA), p-chloroaniline (98%; Nanjing Chemical Reagent Co. Ltd., China), toluene (99.5%; Nanjing Chemical Reagent Co. Ltd), o-xylene (98.0%; Supelco), m-xylene (99.5%; Sigma-Aldrich), p-xylene (99.5%; Sigma-Aldrich), 1,3,5-trimethylbenzene (97%; Macklin, China), nitrobenzene (99.5%; Fluka), m-dinitrobenzene (97%; Sigma-Aldrich), and 1,3,5-trinitrobenzene (99.9%; Sigma-Aldrich). GO (99.0%) and RGO (98.9%) were purchased from XFNANO Materials Tech (China). GO was prepared by the modified Hammers method (18 (link), 23 ) and was mainly in the form of nanosheets with a diameter of 0.5 to 5 μm and thickness of 0.8 to 1.2 nm (according to the information provided by the manufacturer). RGO was prepared by the reduction of GO using l -ascorbic acid (48 ). All these materials were used without further purification.
3
Synthesis and Characterization of 3-(Naphthalen-1-ylimino)indolin-2-one
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Isatin (2,3-indolinedione, purity 97%), 1-naphthylamine (purity ≥ 99.0%), absolute ethanol, and acetic acid were supplied by Sigma Aldrich (St. Louis, MO, USA). “3-(Naphthalen-1-ylimino)indolin-2-one” was synthesized in the central laboratory, College of Pharmacy, King Saud University, (Riyadh, Saudi Arabia). High purity Milli-Q water was obtained through a Milli-Q Integral Water Purification System (Millipore, Bedford, MA, USA). The lipid-based self-nanoemulsifying formulation was developed in-house as a single oral dosage form to apply the method. Black seed oil (BSO) was obtained by cold press method from a local vendor. Imwitor 988 (I988) was kindly supplied by Sasol Germany GmbH (Werk Witten, Witten-Germany) and Kolliphor EL was purchased from BASF (Ludwigshafen, Germany). All other reagents were of analytical grade and used without further purification.
4
Plasmonic Microsphere Synthesis and Characterization
5
Synthesis and Characterization of Bis-Aldehydes
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Aniline, 1-naphthylamine, 2-aminoanthracene, 1-aminopyrene and N,N-dimethylformamide were purchased from Sigma-Aldrich Chemie GmbH (Germany) and used as received. α,ω-bis(4-formylphenoxy)-alcanes: (1,4-bis(4-formylphenoxy)-butane; 1,6-bis(4-formyl phenoxy)-sextane, 1,7-bis(4-formylphenoxy)-heptane, 1,8-bis(4-formylphenoxy)-octane, 1,9-bis(4-formylphenoxy)-nonane, 1,10-bis(4-formylphenoxy)-decane) were prepared and structurally characterized in our laboratory according to published procedures [51 (link),62 (link)].
6
Fabrication and Functionalization of ETAS Adsorbents
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Example 8
The following example describes the materials used in the fabrication and/or functionialization of the ETAS adsorbents. Pyrrole, chloroform, methanol, conductive multi-walled carbon nanotubes (diameter: 6-9 nm, purity: 95%), sodium perchlorate, tetrabutylammonium perchlorate, Sudan Orange G™ (SOG), 2,4-dichlorophenol, 2-naphthol, 1-naphthylamine, bisphenol A, bisphenol S, metolachlor, ethinyl estradiol, propranolol hydrochloride, methyl orange, and rhodamine B were purchased from Sigma Aldrich, and were used as received throughout the study, without further purification or chemical modification unless otherwise noted. Polyvinylferrocene with a molecular weight of 50,000 g/mol was obtained from Polysciences and used as received. A platinum wire auxiliary electrode and an Ag/AgCl (3 M NaCl) reference electrode were purchased from BASi and stored as instructed. Flexible carbon cloths were obtained from FuelCellStore and used as received without pretreatment prior to electrochemical functionalization by electroactive polymers.
7
Synthesis of Metal-Doped Silica Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Tetraethyl orthosilicate (TEOS, Merck), 1-naphthylamine (Sigma Aldrich), THF (Merck) and nitrate salts of the metal cations (Sigma Aldrich), Pluronic P123 (EO20PO70EO20, MW = ca. 5800, Sigma Aldrich) and 3-(isocyanatopropyl)trimethoxysilane. All of the above materials were used without any further purification. Deionized water was used in all procedures.
8
Synthesis of Functional Polymeric Materials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All materials and solvents
were commercially available and used as received unless otherwise
indicated. The following materials and solvents were used: methylmethacrylate
(MMA) (Merk, 99%), N-vinylpyrrolidone (VP) (Acros
Organic, 99%), 4-aminostyrene (SNH2) (Aldrich, 99%), 3-aminophenol
(Aldrich, 99%), methacrylic anhydride (Aldrich, 99%), hexane (Aldrich,
99%), hydrochloric acid (VWR-Prolabo, 37%), sodium hydroxide (VWR-Prolabo,
99%), sodium nitrite (Applichem Panreac, 99%), ethanol (Aldrich, 96%),
zinc acetate dihydrate (Aldrich, 99.5%), acetic acid glacial (Aldrich,
100%), potassium hexacyanoferrate (II) trihydrate (Aldrich, >98.5%),
sulfanilic acid (Aldrich, 99%), and 1-naphthylamine (Merck, 99%).
Azo-bis-isobutyronitrile (AIBN, Aldrich, 98%) was recrystallized twice
from methanol.
were commercially available and used as received unless otherwise
indicated. The following materials and solvents were used: methylmethacrylate
(MMA) (Merk, 99%), N-vinylpyrrolidone (VP) (Acros
Organic, 99%), 4-aminostyrene (SNH2) (Aldrich, 99%), 3-aminophenol
(Aldrich, 99%), methacrylic anhydride (Aldrich, 99%), hexane (Aldrich,
99%), hydrochloric acid (VWR-Prolabo, 37%), sodium hydroxide (VWR-Prolabo,
99%), sodium nitrite (Applichem Panreac, 99%), ethanol (Aldrich, 96%),
zinc acetate dihydrate (Aldrich, 99.5%), acetic acid glacial (Aldrich,
100%), potassium hexacyanoferrate (II) trihydrate (Aldrich, >98.5%),
sulfanilic acid (Aldrich, 99%), and 1-naphthylamine (Merck, 99%).
Azo-bis-isobutyronitrile (AIBN, Aldrich, 98%) was recrystallized twice
from methanol.
9
Synthesis and Characterization of Magnetic Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All chemicals and reagents, namely calcium nitrate trihydrate (99 %), nickel nitrate hexahydrate (99 %), iron nitrate nonahydrate (99 %), tetraethyl orthosilicate, glucose, barbituric acid, 1‐naphthylamine and the respective benzaldehyde derivatives, were purchased from Merck Chemical Company. 1H NMR spectra were taken with 400 MHz NMR spectrometer for solution NMR analysis. IR spectra were obtained with Shimadzu's instrument. Electrothermal Programmable Digital Melting Point Apparatus used to measure melting points. BGMN/Profex/AutoQuan software reported the results of the X‐Ray Diffraction study. nanoparticles were examined using a field emission scanning electron microscope (FE‐SEM), On the Zeiss, that ran at an accelerating voltage of 15 kV. The magnetic properties of nanostructure were measured by a vibrating sample magnetometer (VSM) with PPMS‐9 T at 300 K. The Brunauer‐Emmett‐Teller (BET) specific area and pore volume were measured via the nitrogen adsorption/desorption isotherms method using BELSORP MINI II. High Resolution Transmission Electron Microscopy (HR‐TEM) was prepared by a FEI TECNAI F20 at 200 kV instrument.
10
Electrochemical Synthesis of Aniline Polymer
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
o-Phenylenediamine
(SD Fine Chem. Pvt. Ltd., India), aniline (Merck, India), polyvinylidene
fluoride (PVDF), 1-naphthylamine (Merck, India), DMSO (Merck, India),
potassium dihydrogen phosphate (Merck, India), ferric chloride (Merck,
India), gelatin-B (GL-B) (Sigma-Aldrich), glutaraldehyde (Merk, India),
and metformin hydrochloride (MFH) were purchased from Franco-Indian
Pharmaceutical Pvt. Ltd., India.
(SD Fine Chem. Pvt. Ltd., India), aniline (Merck, India), polyvinylidene
fluoride (PVDF), 1-naphthylamine (Merck, India), DMSO (Merck, India),
potassium dihydrogen phosphate (Merck, India), ferric chloride (Merck,
India), gelatin-B (GL-B) (Sigma-Aldrich), glutaraldehyde (Merk, India),
and metformin hydrochloride (MFH) were purchased from Franco-Indian
Pharmaceutical Pvt. Ltd., India.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!