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Iron 3 acetylacetonate

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Iron(III) acetylacetonate is a coordination complex compound commonly used as a precursor in various chemical reactions and processes. It serves as a source of iron ions in organic synthesis and materials chemistry applications.

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Lab products found in correlation

Oleic acid, by Merck Group (36 mentions) Oleylamine, by Merck Group (31 mentions) Benzyl ether, by Merck Group (18 mentions) 1 2 hexadecanediol, by Merck Group (17 mentions) 1 octadecene, by Merck Group (9 mentions) Dimethyl sulfoxide (dmso), by Merck Group (8 mentions) Chloroform, by Merck Group (8 mentions) Dibenzyl ether, by Merck Group (5 mentions) Toluene, by Merck Group (5 mentions) Dopamine hydrochloride, by Merck Group (5 mentions) Manganese 2 acetylacetonate, by Merck Group (5 mentions) Manganese 2 chloride, by Merck Group (4 mentions) Fetal bovine serum (fbs), by Thermo Fisher Scientific (4 mentions) N hexane, by Merck Group (4 mentions) Cobalt 2 acetylacetonate, by Merck Group (4 mentions) Hexane, by Thermo Fisher Scientific (3 mentions) Rpmi 1640 medium, by Thermo Fisher Scientific (3 mentions) Osmium tetroxide, by Merck Group (3 mentions) Acryloyl chloride, by Thermo Fisher Scientific (3 mentions) N boc ethylenediamine, by Thermo Fisher Scientific (3 mentions)

Close spelling variants of this product

Iron acetylacetonate (18 citations) Iron(III) acetylacetonate (Fe(acac)3) (17 citations) Iron acetylacetonate Fe(acac)3 (3 citations) Iron III (2 citations) Iron (III) acetylacetonate (FeAA) catalyst (2 citations) Iron(III) acetylacetonate (Fe(acac)3 ≥97%) (2 citations)

80 protocols using iron 3 acetylacetonate

1

Synthesis of Multifunctional Nanoparticles

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All chemicals and materials used were commercially available and applied without further purification. Iron (III) acetylacetonate (98%), oleic acid (90%), dibenzyl ether were purchased from Sigma-Aldrich Co. (St. Louis, MO, USA). Platinum (II) acetylacetonate (97%), oleylamine (80–90%), oleyl alcohol, diphenyl ether, N-(3-dimethylaminopropyl)-N′-ethylcarbodiimide hydrochloride, N-hydroxysuccinimide, N, N’-dicyclohexylcarbodiimide, dopamine hydrochloride, 2-(N-morpholino) ethanesulfonic acid (MES) buffer and rhodamine B isothiocyanate (RITC) were purchased from Aladdin Industrial Inc. (Shanghai, China). Ethanol, hexane, diethyl ether, chloroform, dimethylformamide and sodium carbonate were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China). α,ω-dicarboxyl poly(ethylene glycol) (molecular weight = 2000) was acquired from Ponsure Biological Co. (Shanghai, China). Cyclic arginyl–glycyl-aspartic acid (RGD) peptide (cRGDyK) was obtained from GL Biochem (Shanghai) Ltd. Foetal bovine serum (FBS) was purchased from Sijiqing Biologic Co., Ltd. (Hangzhou, China). Dulbecco’s modified eagle medium (DMEM) and trypsin-EDTA solution (0.5% trypsin, 5.3 mM EDTA tetrasodium) were purchased from Jinuo Biomedical Technology Co., Ltd. (Hangzhou, China). Distilled water was prepared by Milli-Q (Millipore, USA).
Liang Z., Wang Q., Liao H., Zhao M., Lee J., Yang C., Li F, & Ling D. (2021). Artificially engineered antiferromagnetic nanoprobes for ultra-sensitive histopathological level magnetic resonance imaging. Nature Communications, 12, 3840.
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2

TEOS-Fe Nanoparticle Synthesis Protocol

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Tetraethyl orthosilicate (TEOS 99.999%, Sigma Aldrich) and iron (III) acetylacetonate (99.9% trace metals grade, Sigma Aldrich) were utilized as Si and Fe precursors. Toluene (99.99%, Sigma Aldrich) was used as a solvent for these chemicals within the atomizer. Teflon filters collected the excess particles that were characterized using offline analysis.
Reed N., Fang J., Chavalmane S, & Biswas P. (2016). Real-time measurement of size-resolved elemental composition ratio for flame synthesized composite nanoparticle aggregates using a tandem SMPS-ICP-OES. Aerosol science and technology : the journal of the American Association for Aerosol Research, 51(3), 311-316.
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3

Synthesis of Cobalt-Doped Superparamagnetic Iron Oxide Nanoparticles

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To enhance the magnetic properties of the SPION-loaded micelles, cobalt-doped superparamagnetic iron oxide nanoparticles (SPIONs) were synthesized, as previously described.58 (link) The 10 nm cobalt-doped SPIONs could be readily synthesized in one step (i.e., vs. sequential seed growth) and efficiently loaded into the micelles. Briefly, 1 mmol cobalt chloride (Alfa Aesar), 2 mmol iron (III) acetylacetonate (Sigma), 2 mmol oleic acid (Chem-Impex International), 6 mmol oleylamine (Sigma), and 5 mmol 1, 2-hexadecanediol (Sigma) were reacted in 20 mL benzyl ether (Sigma) in a two-neck flask while stirred under nitrogen. The reaction was heated to 200°C for 30 minutes, followed by heating to reflux for 75 minutes. The product was cooled to room temperature and washed with 100% ethanol by centrifugation at 5,500 g × 15 minutes. The pellet was resuspended in toluene and large aggregates were removed by centrifugation at 3,000 g × 15 minutes.
Liu J.F., Lan Z., Ferrari C., Stein J.M., Higbee-Dempsey E., Yan L., Amirshaghaghi A., Cheng Z., Issadore D, & Tsourkas A. (2019). Use of Oppositely-Polarized External Magnets to Improve the Accumulation and Penetration of Magnetic Nanocarriers into Solid Tumors. ACS nano, 14(1), 142-152.
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4

Functionalized Nanoparticles for Targeted Drug Delivery

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Iron (III) acetylacetonate (97%), Dibenzyl ether (>98%) and Dopamine hydrochloride (DA) were purchased from Sigma. Zinc acetylacetonate hydrate (97%), morpholineethanesulfonic acid (MES), 1-(3-dimethylaminopropyl)-3-ethyl carbodiimide hydrochloride (EDC, > 98.0%), N-hydroxy succinimide (NHS, 98%) and N,N-Dimethylformamide (DMF) were purchased from Aladdin. Phosphate buffer saline (PBS), Dulbecco's Modified Eagle's medium (DMEM), penicillin/streptomycin and fetal bovine serum (FBS) were purchased from Hyclone. mPEG-NH2 (MW=2000) was purchased from SINOPEG Biotech Co. Ltd (Xiamen China). Poly (acrylic acid) (PAA) (MW=2000) was purchased from Macklin Shanghai China. Epidermal Growth Factor (EGF) peptide was purchased from GL Biochem Ltd. (Shanghai). The CCK-8 kit and Propidium Iodide (PI) stain were purchased from Beijing Zoman Biotechnology Co., Ltd. Calcein, Fluo-4 AM and LDH cytotoxicity Assay Kit were purchased from Thermo Fisher Scientific, Shanghai, China. Ultra-pure water was used throughout all experiments. Matrigel was purchased from Corning, USA.
Shen Y., Wu C., Uyeda T.Q., Plaza G.R., Liu B., Han Y., Lesniak M.S, & Cheng Y. (2017). Elongated Nanoparticle Aggregates in Cancer Cells for Mechanical Destruction with Low Frequency Rotating Magnetic Field. Theranostics, 7(6), 1735-1748.
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5

Synthesis and Characterization of Metal Nanoparticles

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Copper (II) acetylacetonate (Cu(acac)2, 97%), iron (III) acetylacetonate (Fe(acac)3, ≥99.9%), 1-dodecanethiol (DDT, ≥ 98%), oleic acid (OA, technical grade, 90%), oleylamine (Olam, technical grade, 70%), toluene (anhydrous), nitric acid (70%, TraceMetal grade), and tetrachloroethylene (TCE, ≥ 99.9%) were purchased from Sigma-Aldrich. Hexanes (Optima for HPLC, ≥ 99.9%), isopropyl alcohol (99.5%), ethanol (anhydrous, histological), and cobaltocene (98%) were purchased from Fisher Scientific, while sulfur (refined, 99.5%) was procured from ACROS Organics. Quartz glass cuvettes were sourced from Starna Cells Inc. Gold nanorods (10 nm × 67 nm), citrate-coated, were purchased from Nanopartz, and 1,2-distearoyl-sn-glycero-3-phosphoethanolamine-N-[methoxy-(polyethylene glycol)-2000] (ammonium salt) was purchased from Avanti Lipids. All air-sensitive materials were stored and handled in a glovebox under an argon atmosphere.
Kays J.C., Conti CR I.I.I., Margaronis A., Kuszynski J.E., Strouse G.F, & Dennis A.M. (2021). Controlled Synthesis and Exploration of CuxFeS4 Bornite Nanocrystals. Chemistry of materials : a publication of the American Chemical Society, 33(18), 7408-7416.
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6

Synthesis of Functionalized Nanoparticles

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Iron (III) acetylacetonate (99%), oleic acid (technical grade 90%), benzyl ether (98%), and BSA (98%) were purchased from Sigma-Aldrich (St. Louis, MO, USA) and used as received; 4-biphenylcarboxylic acid (99%, Acros Organics, Belgium, WI, USA), acetone (99.5%), hexanes (98.5%), sodium bicarbonate (99.7%), nitric acid (70%), and hydrogen peroxide (30%) were purchased from Fisher Scientific (Waltham, MA, USA). The BSA Cy5.5 conjugate (BSA Cy5.5, 10 mg·mL‒1 in saline) was purchased from Protein Mods (Burlington, ON, Canada).
Cho M., Cervadoro A., Ramirez M.R., Stigliano C., Brazdeikis A., Colvin V.L., Civera P., Key J, & Decuzzi P. (2017). Assembly of Iron Oxide Nanocubes for Enhanced Cancer Hyperthermia and Magnetic Resonance Imaging. Nanomaterials, 7(4), 72.
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7

Synthesis of Magnetic Nanoparticles

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Iron (III) acetylacetonate (97%), 1,2-hexadecanediol (90%), benzyl ether (98%), oleic acid (OA, 70%) and oleylamine (OAm, 70%) were purchased from Sigma-Aldrich Corporation. Diethylenetriaminepentaacetic dianhydride (98%) was purchased from TCI Chemical Industry Development Corporation. NH2-PEG-dopamine (Mw 1 k and 2 k) were purchased from Shanghai Ponsure Biotech, Inc. (Shanghai, China). Gadolinium (III) chloride (GdCl3) and ethylenediaminetetraacetic acid disodium salt (EDTA2Na) were purchased from Aladdin Industrial Corporation. All other chemicals and solvents were of analytical grade and used without further purification.
Yang L., Fu S., Cai Z., Liu L., Xia C., Gong Q., Song B, & Ai H. (2021). Integration of PEG-conjugated gadolinium complex and superparamagnetic iron oxide nanoparticles as T1–T2 dual-mode magnetic resonance imaging probes. Regenerative Biomaterials, 8(6), rbab064.
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8

Synthesis of Graphene-Based Nanomaterials

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Ammonium molybdate tetrahydrate, thiourea, ethanol, cobalt(iii) acetylacetonate, iron(iii) acetylacetonate, oleylamine, and pure graphite powder (99.99%) were purchased from Sigma Aldrich. HNO3, H2SO4, and KClO3 were procured from Fisher Scientific. All chemicals were reagent grade and were used as received without further purification. High purity deionized (DI) water was used in this work as a solvent and for purification.
Prasad J., Singh A.K., Haldar K.K., Tomar M., Gupta V, & Singh K. (2019). CoFe2O4 nanoparticles decorated MoS2-reduced graphene oxide nanocomposite for improved microwave absorption and shielding performance. RSC Advances, 9(38), 21881-21892.
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9

Synthesis of Monodisperse Nanoparticles

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In this study was used: iron (III) acetylacetonate (99%) from Sigma Aldrich (St. Louis, MO, USA), oleic acid (90%) from Panreac (Barcelona, Spain), benzyl ether (99%) from Sigma Aldrich (Madrid, Spain), 4-biphenylcarboxylic acid (99%) from Sigma Aldrich (Madrid, Spain), toluene (99.8%) from Panreac (Barcelona, Spain), hexane (99%) from Panreac (Barcelona, Spain), chloroform (99.9%) from Panreac (Barcelona, Spain), and nitrogen (99%) from Air Liquide (Paris, France). All solutions were made with distilled water.
Sánchez O.S., Castelo-Grande T., Augusto P.A., Compaña J.M, & Barbosa D. (2021). Cubic Nanoparticles for Magnetic Hyperthermia: Process Optimization and Potential Industrial Implementation. Nanomaterials, 11(7), 1652.
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10

Synthesis of Magnetic Nanoparticles

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Lithium carbonate, iron(iii)-acetylacetonate, oleylamine (technical grade, 70%), oleic acid (technical grade, 90%), phosphoric acid 85 wt% in H2O (H3PO4) and tetraethyleneglycol (TEG) were purchased from Sigma-Aldrich and used without purification. Acetone and hexane were purchased from Samchun Chemical (Korea) and used as received.
Yang C., Lee D.J., Kim H., Kim K., Joo J., Kim W.B., Song Y.B., Jung Y.S, & Park J. (2019). Synthesis of nano-sized urchin-shaped LiFePO4 for lithium ion batteries. RSC Advances, 9(24), 13714-13721.
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