Methyl methacrylate (MMA, Alfa Aesar, Warsaw, Poland) and [2-(methacryloyl-oxy)ethyl]trimethylammonium chloride (TMAMA, 80% aq. solution, Sigma-Aldrich, Poznan, Poland) were dried using molecular sieves or under vacuum, respectively. Copper(I) chloride (CuCl, Fluka, 98%, Steinheim, Germany) was purged according to procedures described previously [39 (link)]. Methanol was obtained from Chempur (Piekary Śląskie, Poland). Rifampicin (RIF, 97%) and sodium fusidate (FUS, 98.8%) were purchased from Alfa Aesar (Warsaw, Poland) and used without prior purification. Phosphate-buffered saline (PBS), 2,2′-bipyridine (bpy), and tetrahydrofuran (THF) were obtained from Sigma-Aldrich (Poznań, Poland).
2 2 bipyridine bpy
Manufactured by Merck Group
Sourced in Poland, United States, United Kingdom
2,2'-bipyridine (bpy) is a heterocyclic organic compound with the molecular formula C₁₀H₈N₂. It is a colorless solid that is commonly used as a ligand in coordination chemistry and as a building block in the synthesis of various organic compounds.
Automatically generated - may contain errors
Lab products found in correlation
Sodium fusidate, by Thermo Fisher Scientific (1 mentions)
Methanol, by Chempur (1 mentions)
Methyl methacrylate mma, by Thermo Fisher Scientific (1 mentions)
Rifampicin, by Thermo Fisher Scientific (1 mentions)
Tetrahydrofuran thf, by Merck Group (1 mentions)
Phosphate buffered saline (pbs), by Merck Group (1 mentions)
2 hydroxy 5 nitrobenzaldehyde, by Merck Group (1 mentions)
Methyl methacrylate mma, by Merck Group (1 mentions)
Copper 1 bromide cubr, by Merck Group (1 mentions)
Benzoyl peroxide bpo, by Merck Group (1 mentions)
Tetrahydrofuran, by Avantor (1 mentions)
Methanol, by Avantor (1 mentions)
Toluene, by Avantor (1 mentions)
1 propanol, by Merck Group (1 mentions)
1 4 dioxane, by Merck Group (1 mentions)
Mesitylene, by Merck Group (1 mentions)
Nafion, by Merck Group (1 mentions)
Glacial acetic acid, by Merck Group (1 mentions)
4 7 diphenyl 1 10 phenanthroline, by Merck Group (1 mentions)
Anhydrous methanol, by Merck Group (1 mentions)
5 protocols using 2 2 bipyridine bpy
1
Controlled Radical Polymerization for Bioactive Coatings
2
Photoinitiated ATRP of Methyl Methacrylate
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Chemicals were used without further purification and were of analytical grade. Methyl methacrylate (MMA) (Mw: 100.1 g mol−1; 99%, Sigma-Aldrich, St. Louis, MO, USA), Benzoyl peroxide (BPO, Mw: 242.2 g mol−1; 99.98%, Sigma-Aldrich); Copper (I) bromide (CuBr, Mw: 143.45 g mol−1, 99.99%, Sigma-Aldrich); 2,2′-Bipyridine (Bpy, Mw: 156.1 g mol−1; ≥99%, Sigma-Aldrich); 1,3,3-Trimethyl-2-methylen-indoline (Mw: 173.2 g mol−1, 97%, Sigma-Aldrich); 2-hydroxy-5-nitrobenzaldehyde (Mw: 167.12 g mol−1, 98% Sigma-Aldrich). 2-bromoethanol (C2H5BrO, Sigma-Aldrich) and 2-butanone (C2H5COCH3, 99.0%, Sigma-Aldrich).
3
Synthesis of Rhenium-Bipyridine Complexes
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5,5′-diamino-2,2′-bipyridine (95%, Yuhao Chemical), pentacarbonylchlororhenium (98%, Sigma-Aldrich), 2,2′-bipyridine (Bpy) (≥99%, Sigma-Aldrich), triformylphloroglucinol (Tp) (95%, Yuhao Chemical), mesitylene (98%, Sigma-Aldrich), 1,4-dioxane (anhydrous, 99.8%, Sigma-Aldrich), glacial acetic acid (ACS reagent, Aldrich), Nafion (10 wt% in H2O), 1-propanol (for HPLC, ≥99.9%, Sigma-Aldrich), toluene (for HPLC, VWR Chemicals), methanol (for HPLC, VWR Chemicals), tetrahydrofuran (for HPLC, VWR Chemicals).
4
Synthesis and Characterization of Ruthenium Complexes
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All solvents were of analytical grade and were used without further purification. Reagents were purchased from Sigma-Aldrich. 2,2′-bipyridine (bpy) and 4,7-diphenyl-1,10-phenanthroline (dip) were purchased from Sigma-Aldrich. The following complexes [Ru(dip)2(bpy)]Cl2,[Ru(dip)2(bpy-SC)]Cl2 and [Ru(bpy)2bpy-NitroIm]Cl2 were prepared according to the published procedures [42 (link),43 (link),44 (link)]. The purity and identity were confirmed by HPLC by comparison to published results as well as 1H NMR or HRMS analysis (data available in Supplementary Materials ).
5
Synthesis and Characterization of MPC Monomer
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2-(Methacryloyloxy)ethyl phosphorylcholine monomer (MPC; 99.9% purity) was donated by Biocompatibles UK Ltd. Anhydrous ethanol (99%), anhydrous methanol (≥99.8%), 2-(diisopropylamino)ethyl methacrylate (DPA), copper(I) bromide [Cu(I)Br; 99.999%], 2,2′-bipyridine (bpy; 99%), tris(2-carboxyethyl)phosphine hydrochloride (TCEP; ≥98.0%), dry triethylamine, and PTA were purchased from Sigma Aldrich UK. The silica gel 60 (0.063 to 0.200 μm) used to remove the spent atom transfer radical polymerization (ATRP) catalyst CuBr was purchased from E. Merck. High-performance liquid chromatography–grade dichloromethane and methanol were purchased from Fisher Scientific. All of the above were used as received. Phosphate-buffered saline (PBS) was prepared from tablets obtained from Oxoid. Semipermeable cellulose dialysis tubing (Spectra/Por 6 MWCO 1000) was purchased from Fisher Scientific.
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