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Fp900

Manufactured by Mettler Toledo
Sourced in Switzerland

The FP900 is a thermal analysis instrument designed for laboratory use. It is capable of performing differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA) measurements. The FP900 provides accurate and precise thermal analysis data for a variety of sample types.

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2 protocols using fp900

1

Thermal Analysis of BZ and PCL/BZ Blend

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TOA analyses of BZ and a physical blend of PCL/BZ (1:1.33) were performed using Mettler Toledo FP900 equipment, with an FP90 processor and FP82 hot stage (Mettler-Toledo, Schwerzenbach, Switzerland). Images were captured by Leica DM4000B optical microscope (Wetzlar, Germany) at 100×. Pure BZ samples were analyzed in the temperature range of 175 to 215 °C, at a heating rate of 2 °C/min. The physical blends of PCL and BZ samples were analyzed in the temperature range of 55 to 75 °C for PCL and 180 to 205 °C for BZ at a heating rate of 2 °C/min.
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2

SAXS Characterization of Samples

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SAXS experiments were conducted on BL10C in the Photon Factory, KEK, Japan, where PILATUS 2M (DECTRIS Ltd, Baden, Switzerland) detector and an incident X-ray with a wavelength of 1.5 Å were used. The measured q range was 0.013 Å−1 to 0.83 Å−1 at a sample-to-detector distance of 1.1 m. A silver behenate standard was used to calibrate sample-to-detector distances. A polyimide tube containing a sample was held in a hot stage (FP900, Mettler-Toledo Inc., Columbus, OH) and all the samples were subjected to measurements at T = 54 °C. Data reduction was performed using Nika45 and background correction was made by subtracting the SAXS profile of H2O.
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