All of the reagents and precursors, including cadmium perchlorate hydrate (Sigma-Aldrich, St. Louis, MO, USA, Cd(ClO4)2 · 6H2O), sodium sulphide (Synth, Diadema, Brazil, >98%, Na2S · 9H2O), and hydrochloric acid (Sigma-Aldrich, St. Louis, MO, USA, 36.5% to 38%, HCl) were used as received. Glycol Chitosan (G-CHI; Sigma-Aldrich, St. Louis, MO, USA, PN# G7753; degree of polymerization ≥400, lot supplied = 2,000 (Mw ~ 410 kDa); degree of deacetylation DD ≥60%, lot supplied = 76.2%) was used as the ligand. Chitosan (Aldrich Chemical, St. Louis, MO, USA, catalogue#419419; high molecular weight, Mw = 310 to >395 kDa; degree of deacetylation DD ≥75.0%; viscosity 800 to 2,000 cPoise, 1 wt.% in 1% acetic acid) was used as the reference polysaccharide ligand. Unless otherwise indicated, deionised water (DI water; Millipore Simplicity™, Millipore, Billerica, MA, USA) with a resistivity of 18 MΩ · cm was used to prepare the solutions, and the procedures were conducted at room temperature (RT; 23°C ± 2°C).
Cadmium perchlorate hydrate
Manufactured by Merck Group
Sourced in United States, Ireland
Cadmium perchlorate hydrate is a chemical compound used in various laboratory applications. It is a crystalline solid with the formula Cd(ClO4)2·xH2O, where x represents the number of water molecules. The core function of this product is to serve as a source of cadmium and perchlorate ions for experimental and analytical purposes.
Automatically generated - may contain errors
Lab products found in correlation
Chitosan, by Merck Group (1 mentions)
Hydrochloric acid (hcl), by Merck Group (1 mentions)
Sulfuric acid, by Thermo Fisher Scientific (1 mentions)
2 propanol, by Merck Group (1 mentions)
Cysteamine, by Merck Group (1 mentions)
Thiourea, by Merck Group (1 mentions)
Acetonitrile, by Fujifilm (1 mentions)
Diethyl ether, by Fujifilm (1 mentions)
Dichloromethane dcm, by Fujifilm (1 mentions)
Tetrachloroauric acid, by Merck Group (1 mentions)
Copper 2 chloride, by Merck Group (1 mentions)
Nickel 2 chloride, by Merck Group (1 mentions)
Silver nitrate, by Merck Group (1 mentions)
Sodium borohydride, by Merck Group (1 mentions)
Cetyltrimethylammonium bromide ctab, by Merck Group (1 mentions)
3 aminopropyltrimethoxysilane aptes, by Merck Group (1 mentions)
Manganese 2 chloride, by Merck Group (1 mentions)
Mercury 2 chloride, by Merck Group (1 mentions)
Ascorbic acid, by Merck Group (1 mentions)
Lead 2 chloride, by Merck Group (1 mentions)
4 protocols using cadmium perchlorate hydrate
1
Synthesis and Characterization of Cadmium Sulfide Nanoparticles
2
Peptide Synthesis and Explosive Detection
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All chemicals studied were analytical grade. TentaGel Resin (capacity: 0.25 mmol g -1 ) was purchased from Intavis AG (Cologne, Germany). N-Fluorenyl-9-methoxycarbonyl (Fmoc) protected L-amino acids, O-benzotriazole-N,N,N',N'-tetra-methyl-uronium-hexafluoro-phosphate (HBTU), diisopropylethylamine (DIEA), trifluoroacetic acid (TFA), triisopropylsilane (TIPS), N,N-dimethylformamide (DMF) and 20% piperidine solution in DMF were obtained from Watanabe Chemical Ind., Ltd. (Hiroshima, Japan). Dichloromethane (DCM), ethanol, diethyl ether, acetonitrile, 1-methyl-2-pyrrolidone (NMP), toluene and acetonitrile were purchased from FUJIFILM Wako Pure Chemical Corp. (Osaka, Japan). TNT solution solution (1mg mL -1 in acetonitrile), 2-propanol, sodium hydrate, cadmium perchlorate hydrate, cysteamine and thiourea were purchased from Sigma-Aldrich (St. Louis, USA). Aluminum telluride were provided from ABSCO Limited (Haverhill, UK) and stored under N2 atmosphere. Sulfuric acid was purchased from Fisher Scientific (Loughborough, UK). 1,2-Ethanedithiol (EDT), thioanisole, 2,4-Dinitrotoluene (2,4-DNT), 2,6-dinitrotoluene (2,6-DNT), 2-nitrotoluene (2-NT) and amyl nitrate were purchased from Tokyo Chemical Industry Co., Ltd. (Tokyo, Japan). All aqueous solutions were prepared with MilliQ grade deionized water.
3
Synthesis of Metal Nanoparticles
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Tetrachloroauric acid, sodium borohydride, ascorbic acid, silver nitrate, cetyltrimethyl-ammoniumbromide (CTAB), mercury(II) chloride, cadmium perchlorate hydrate, lead(II) chloride, nickel(II) chloride, manganese(II) chloride and copper(II) chloride and (3-aminopropyl)trimethoxysilane (APTES) were obtained from Sigma-Aldrich (Ireland). All glassware was cleaned with piranha solution prior to nanorod synthesis. Milli-Q water (resistivity > 18 MΩ cm−1) was used for all the experiments.
4
Fabrication and Sensing of Metal Ions
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All reagents used for device fabrication and sensing were utilized without further pre-treatment. ARS, a commercially available river sample with trace elements in river water (Elevated Level, NMIJ CRM 7202-c, Supplementary Table S1 ), and iron(III) nitrate enneahydrate (Fe3+) were obtained from FUJIFILM Wako Pure Chemical Co., Ltd. The target metal ions including cobalt(II) perchlorate hexahydrate (Co2+), calcium perchlorate tetrahydrate (Ca2+), lead(II) perchlorate trihydrate (Pb2+), cadmium perchlorate hydrate (Cd2+), nickel(II) perchlorate hexahydrate (Ni2+), copper(II) perchlorate hexahydrate (Cu2+), magnesium perchlorate hexahydrate (Mg2+), aluminum perchlorate non-ahydrate (Al3+), mercury(II) perchlorate hydrate (Hg2+), and zinc perchlorate hexahydrate (Zn2+) were purchased from Sigma-Aldrich. The building blocks of the chemosensors purchased from Tokyo Chemical Industry Co., Ltd. were 3-NPBA, BPR, PR, and PV. A buffer material purchased from DOJINDO was 4-(2-hydroxyethyl)-1-piperazineethanesulfonic acid (HEPES). All aqueous solutions were prepared using Milli-Q water (18.2 Ω cm).
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!