The largest database of trusted experimental protocols

2 protocols using graphite powder

1

Electrochemical Sensor for Paracetamol Analysis

Check if the same lab product or an alternative is used in the 5 most similar protocols
All materials were applied without additional purification. Sodium hydroxide (NaOH, 99%), tetraethyl orthosilicate (TEOS, 98%), nickel(II) acetate tetrahydrate (Ni(CH3COO)2, 98%), cobalt(II) acetate tetrahydrate (Co(CH3COO)2, 98%), ethylenediamine (99%), salicylaldehyde (98%), potassium chloride (KCl, 99.5%), potassium hexacyanoferrate (III) (K3Fe(CN)6, 99%) and potassium hexacyanoferrate (IV) (K4Fe(CN)6, 99%), phosphoric acid (H3PO4, 85%), potassium dihydrogen phosphate (KH2PO4, ≥ 99.5%), potassium hydrogen phosphate (K2HPO4, ≥ 99.5%), ascorbic acid (> 99%) and paracetamol (> 99%) were obtained from Merck company (Germany) with analytical reagent grade. Graphite powder (99.5%), diethyl ether (99%), paraffin oil (d = 0.88 g cm−3, 99%) and sodium aluminate (98%) were acquired from Daejung Company. All materials were purchased from local store in Iran. Biological samples were gotten from Blood Transfusion Organization (Babol, Iran) and stored frozen until the analysis. Tablets of PAR (500 mg) were obtained from resident drug store. Also, deionized water (DW) was applied in the all parts.
+ Open protocol
+ Expand
2

Synthesis of Graphene-Based Electrocatalyst

Check if the same lab product or an alternative is used in the 5 most similar protocols
All chemicals and reagents used for experiments were of analytical quality. Potassium permanganate (KMnO4, extra pure 99–100%) manganese chloride monohydrate (MnCl2·H2O, ≥97% pure) and terephthalic acid (C8H6O4, ≥98%) were purchased from Sigma-Aldrich. Graphite powder (chemical pure) and hydrogen peroxide (H2O2, 30%) were provided by Daejung, Korea. Sulfuric acid (H2SO4, ≥98%) and hydrochloric acid (HCl, 35.4%) were supplied by BDH AnalaR® England. Orthophosphoric acid (H3PO4, 85%) and methanol (CH4O, ≥99.7%) were supplied by Honeywell, Germany. Absolute ethanol by AnalaR® NORMAPUR, VWR and N,N-dimethylformamide (C3H7NO, 99%) by Merck. Deionized water at 2.0 MΩ cm−1 resistivity was used during synthesis process. Liquid ionic binder Nafion (C23H20N2O2S) solution (5 wt% in methanol) was purchased from Ion Power, Inc. Commercial carbon-supported Pt NPs catalyst (10% Pt/C) was supplied by Alfa Aesar, USA.
+ Open protocol
+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required

Sign up now

Revolutionizing how scientists
search and build protocols!