The thermal properties of the nanofibers were analyzed using a Perkin Elmer Jade differential scanning calorimeter (DSC). Samples were weighed and placed in alumina pans. The heating was performed from room temperature to 300 °C with a heating rate of 10 °C/min under dynamic argon atmosphere (20 mL/min).
Jade differential scanning calorimeter
Manufactured by PerkinElmer
Sourced in United States
The Jade differential scanning calorimeter is a laboratory instrument designed to measure the thermal properties of materials. It operates by precisely controlling the temperature of a sample and a reference material, and measures the difference in heat flow between the two. This data can be used to analyze phase transitions, heat capacity, and other thermal characteristics of the material under investigation.
Automatically generated - may contain errors
6 protocols using jade differential scanning calorimeter
1
Thermal Analysis of Nanofibers
2
Differential Scanning Calorimetry of Paint Films
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
A PerkinElmer Jade
differential scanning calorimeter was used for this study. The temperature
program cycled twice between 10 and −60 °C with a rate
of 5 °C/min. Paint films (90 μm thickness) were taken out
of the water, patted dry with paper tissue before being cut into small
pieces, and then placed into sealed aluminum DSC pans. The pans were
weighed when empty and after adding the sample to a Sartorius M2P
microbalance. To minimize water evaporating from potentially leaking
pans, the nitrogen flow in the DSC instrument was turned off during
measurements. The aluminum pans were weighed again after the measurement
run to check for water evaporation. This data can be found in Section
E of theSupporting Information .
differential scanning calorimeter was used for this study. The temperature
program cycled twice between 10 and −60 °C with a rate
of 5 °C/min. Paint films (90 μm thickness) were taken out
of the water, patted dry with paper tissue before being cut into small
pieces, and then placed into sealed aluminum DSC pans. The pans were
weighed when empty and after adding the sample to a Sartorius M2P
microbalance. To minimize water evaporating from potentially leaking
pans, the nitrogen flow in the DSC instrument was turned off during
measurements. The aluminum pans were weighed again after the measurement
run to check for water evaporation. This data can be found in Section
E of the
3
Characterization of Polymeric Materials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All of the solvents and liquid
substrates were degasified and dried over activated molecular sieves
(4 Å) prior to use. Deuterated solvents were purchased from Cambridge
Isotope Laboratory. All 1H and 13C NMR spectra
were recorded on a Bruker AVANCE-500 NMR spectrometer and referenced
to the residue solvents in CDCl3 or CD3CN. GPC
analysis was performed on a Varian Prostar system, using the PLgel
5 μm Mixed-D column, a Prostar 355 RI detector, and THF as the
eluent at a flow rate of 1 mL/min (20 °C). Polystyrene standards
were used for calibration. Infrared spectroscopy results were obtained
on a Thermo Scientific Nicolet iS5 FT-IR instrument and analyzed with
OMNIC 8.2 software. The samples for IR analysis were directly loaded
using an iD5 ATR accessory as a thin film without any support. DSC
measurements were performed on a Perkin Elmer Jade differential scanning
calorimeter, and the instrument was calibrated using zinc and indium
standards. Glass-transition temperatures (Tg) of polymer samples were determined from the second heating cycles
with a heating/cooling rate of 20 °C/min under nitrogen atmosphere
(20 mL/min). DSC data were analyzed using Pyris V9.0.2 software.
substrates were degasified and dried over activated molecular sieves
(4 Å) prior to use. Deuterated solvents were purchased from Cambridge
Isotope Laboratory. All 1H and 13C NMR spectra
were recorded on a Bruker AVANCE-500 NMR spectrometer and referenced
to the residue solvents in CDCl3 or CD3CN. GPC
analysis was performed on a Varian Prostar system, using the PLgel
5 μm Mixed-D column, a Prostar 355 RI detector, and THF as the
eluent at a flow rate of 1 mL/min (20 °C). Polystyrene standards
were used for calibration. Infrared spectroscopy results were obtained
on a Thermo Scientific Nicolet iS5 FT-IR instrument and analyzed with
OMNIC 8.2 software. The samples for IR analysis were directly loaded
using an iD5 ATR accessory as a thin film without any support. DSC
measurements were performed on a Perkin Elmer Jade differential scanning
calorimeter, and the instrument was calibrated using zinc and indium
standards. Glass-transition temperatures (Tg) of polymer samples were determined from the second heating cycles
with a heating/cooling rate of 20 °C/min under nitrogen atmosphere
(20 mL/min). DSC data were analyzed using Pyris V9.0.2 software.
4
Thermal Analysis of Polymeric Coatings
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The thermal properties of polymeric coating were analysed using Differential Scanning Calorimetry (DSC) and Thermogravimetric Analysis (TGA). DSC analysis was carried out using a Jade differential scanning calorimeter (Perkin Elmer, US). The temperature scale of the DSC instrument was calibrated using indium as a standard; which has a known melting point of 156.6°C. Sealed pans containing 2-4mg of sample were heated under a flow of nitrogen gas at a rate of 20°C/min from 20 to 300°C. TGA analysis was carried out using Pyris 1 TGA thermogravimetric analyser (Perkin Elmer, US). Under the flow of nitrogen gas and air, sealed pans containing 8-10mg of sample were heated at a rate of 20°C/min from 20 to 700°C.
5
Differential Scanning Calorimetry of Coating Samples
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Differential Scanning Calorimetry (DSC) studies were carried out using a Jade Differential Scanning Calorimeter, (PerkinElmer, US). Indium, with a known melting point, Tm, of 156.6°C was used as a standard to calibrate the temperature scale of the calorimeter. Coating samples (2-4mg) were sealed in aluminium pans and heated at a rate of 20°C/min under a flow of nitrogen gas.
6
Thermal Analysis of Atomized Coatings
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The thermal properties and stability of the atomised coatings using two thermal analytical techniques; differential scanning calorimetry (DSC) and thermogravimetric analysis (DSC).
DSC studies were carried out using a Jade differential scanning calorimeter (Perkin Elmer, US); 2-4mg of sample were hermetically sealed in aluminium pans were heated at a rate of 20°C/min from 20° to 200°C, under purge and flow of nitrogen gas.
DSC studies were carried out using a Jade differential scanning calorimeter (Perkin Elmer, US); 2-4mg of sample were hermetically sealed in aluminium pans were heated at a rate of 20°C/min from 20° to 200°C, under purge and flow of nitrogen gas.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!