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2 protocols using 1 chlorotetradecane

1

Synthesis of Lead Perovskite Nanocrystals

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All chemicals were used as received: Lead(II) acetate tri-hydrate (Aldrich, 99.999%), oleic acid (OA, Aldrich, 90%), nonanoic acid (Alfa Aesar, 97%), trioctylphosphine (TOP; ABCR, 97%), 1,2-diiodoethane (DIE; Aldrich, 99%), methylammonium bromide (MAB; Aldrich, 98%), methylammonium chloride (MAC; Aldrich, 98%), methylammonium iodide (MAI; Aldrich, 98%), diphenyl ether (DPE; Aldrich, 99%), toluene (VWR, 99,5%), dimethylformamide (DMF; Aldrich, 99,8%), 1bromotetradecane (BTD; Aldrich, 97%), 1-chlorotetradecane (CTD; Aldrich, 98%), octadecylamine (ODA; Aldrich, 97%), tetradecylamine (TDA; Aldrich, 95%), hexadecylamine (HDA; Aldrich, 90%), dodecylamine (DDA; Merck, 98%), oleylamine (ACROS, 80-90%).
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2

Synthesis of Lead Sulfide Nanoparticles

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All chemicals have been used as received. The chemicals used were: lead(II) acetate trihydrate (Aldrich, 99.999 %), thioacetamide (Sigma-Aldrich, >= 99.0 %), thiourea (Aldrich, >= 99.0 %), diphenyl ether (Aldrich, 99 %+), dimethyl formamide (Sigma-Aldrich, 99.8% anhydrous), oleic acid (Aldrich, 90 %), 1-chlorotetradecane (Aldrich, 98 %), 1-chloroheptane (Aldrich, 99 %), 1-fluorotetradecane (Lancaster, 98 %), 1-fluoroheptane (Aldrich, 98 %), 1-bromotetradecane (Aldrich, 97 %), 1-bromoheptan (Aldrich, 99 %), 1iododecane (Aldrich, 98 %), tetradecylamine (Aldrich, 95 %) and heptylamine (Aldrich,
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