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2 boc amino ethanethiol

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Sourced in Denmark

2-(boc amino) ethanethiol is a chemical compound used in laboratory settings. It is a thiol-containing molecule with a tert-butyloxycarbonyl (Boc) protective group on the amino functionality. This product is commonly utilized in organic synthesis and biochemical applications that require the use of thiol-reactive reagents or the introduction of protected amino groups.

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Lab products found in correlation

Maldi plate, by Bruker (1 mentions) α cyano 4 hydroxycinnamic acid hcca, by Bruker (1 mentions) L ascorbic acid, by Avantor (1 mentions) Pierce c18 tip, by Thermo Fisher Scientific (1 mentions) Synergy 185, by Merck Group (1 mentions) Methanol, by Merck Group (1 mentions) Lucirin tpo l, by BASF (1 mentions) Lithium hydroxide, by Merck Group (1 mentions) Sodium azide, by Thermo Fisher Scientific (1 mentions) N n dimethylethanolamine, by Merck Group (1 mentions) 1 4 dioxane, by Merck Group (1 mentions) Trifluoroacetic acid, by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Azobisisobutyronitrile, by Merck Group (1 mentions) Glycidyl methacrylate, by Merck Group (1 mentions) Ethylene glycol dimethacrylate, by Merck Group (1 mentions)

Close spelling variants of this product

Ethanethiol

2 protocols using 2 boc amino ethanethiol

1

Immunoglobulin G Extraction and Proteomic Analysis

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Pentaerythritol-tetrakis(3-mercaptopropionate) (“tetrathiol”), triallyl-1,3,5-triazine-2,4,6-(1H,3H,5H)-trione (“triallyl”), 2-(boc amino) ethanethiol, and methanol (99.8%) were obtained from Sigma-Aldrich (Brøndby, Denmark). Lucirin TPO-L was obtained from BASF (Ludvigshafen, Germany). Acetonitrile (ACN), trifluoroacetic acid (TFA), DL-dithiothreitol (D9779, DTT), iodoacetamide (I670-9, IAA), immunoglobulin G (56,834-25MG, IgG, from human serum), trypsin (T1426, from bovine pancreas), and salts were purchased from Sigma-Aldrich (Stockholm, Sweden). L( +)-Ascorbic acid (99.0–100.5%) was from VWR chemicals (Stockholm, Sweden). Water (MQ H2O) was purified in a Millipore Synergy® 185 (Bedford, MA, USA) to a resistivity of 18.2 MΩ·cm at 25 °C. DEAE Affi-Gel® Blue Gel (DEAE) used for IgG extraction was obtained from Bio-RAD, Hercules, USA. Pierce® C18 Tips, 100 µL bed size, were from Thermo Fisher Scientific (Rockford, USA). Kinesis Tubing PEEK (TM) natural 1/32 inch × 0.015 inch connecting syringe and microchip was purchased from Fisher Scientific (Stockholm, Sweden). MALDI matrices 2,5-dihydroxybenzoic acid (DHB) and α-cyano-4-hydroxycinnamic acid (HCCA) and MALDI plate were obtained from Bruker Daltonics (Bremen, Germany).
Zhou Y., Jönsson A., Sticker D., Zhou G., Yuan Z., Kutter J.P, & Emmer Å. (2023). Thiol-ene-based microfluidic chips for glycopeptide enrichment and online digestion of inflammation-related proteins osteopontin and immunoglobulin G. Analytical and Bioanalytical Chemistry, 415(6), 1173-1185.
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2

Synthesis of Functionalized Polymers

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Glycidyl methacrylate (GMA, 97%) and ethylene glycol dimethacrylate (EGDMA, 98%) were purchased from Sigma-Aldrich and passed through a column of neutral Al2O3 prior to use. N,N-dimethylformamide (DMF, anhydrous, 99.8%), trifluoroacetic acid (TFA, HPLC grade, >99.0%), N,N-dimethylethanolamine (redistilled, 99.5%), 1,4-dioxane (HPLC grade, >99.5%), azobisisobutyronitrile (AIBN, 98%), 2-(Boc-amino)ethanethiol (97%), lithium hydroxide (LiOH, reagent grade, 98%), tris((1-benzyl-4-triazolyl)methyl)amine (TBTA, 97%) and tetrakis(acetonitrile)copper(i) hexafluorophosphate (Cu(CH3CN)4PF6, 97%) were purchased from Sigma-Aldrich and used without further purification. Sodium azide (NaN3, 99%) was purchased from Acros Organics and used as supplied.‡

Safety note: Large scale reactions of azide are prone to dangerous exothermic reactions. The use of chlorinated solvents in the presence of sodium azide must be avoided, as the byproducts may be highly explosive.81

4-methyl-7-(prop-2-yn-1-yloxy)-2H-chromen-2-one was purchased from MolPort as used without any further purifications. Dichloromethane (DCM, 99.7%) and methanol (MeOH) were obtained from Ossum Chemicals. Demi-water was used unless stated otherwise. The RAFT agent 2-[[(butylthio)thioxomethyl] thio] propanoic acid was synthesized following a literature procedure.79
Kusmus D.N., van Veldhuisen T.W., Khan A., Cornelissen J.J, & Paulusse J.M. (2022). Uniquely sized nanogels via crosslinking polymerization. RSC Advances, 12(45), 29423-29432.
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