All the chemicals required were obtained from Sigma-Aldrich, Alfa Aesar, Spectrochem, and TCI and used without further purification. FT-IR spectra were recorded on a Bruker Alpha II system (ν max in cm−1) on KBr disks. 1H NMR and 13C NMR (400 MHz and 100 MHz respectively) spectra were recorded using a Bruker Avance II-400 spectrometer using CDCl3 as the solvent (chemical shifts in δ with TMS as internal standard). Powder XRD analyses were carried out using a Bruker D8 Advance and Rigaku Ultima IV XRD instrument. Transmission Electron Microscopy (TEM) analysis was carried out using a JEOL JSM 100CX system. Scanning electron microscopy (SEM) and Energy Dispersive X-ray (EDX) analysis were carried out using a JSM-6360 (JEOL) system. X-Ray Photoelectron Spectroscopy (XPS) was performed using a PHI 5000 VersaProbe III system. Thermogravimetric analysis (TGA) was carried out using a Perkin Elmer Precisely STA 6000 simultaneous thermal analyzer. Inductively coupled plasma optical emission spectroscopy (ICP-OES) was carried out using Thermo Scientific™ iCAP™ 7600 instrument. TLC Silica gel 60 F254 (Merck) was used for TLC analysis. Hexane refers to the fraction boiling between 60 and 80 °C.
Precisely sta 6000
Manufactured by PerkinElmer
The Precisely STA 6000 is a simultaneous thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) system. It provides thermal analysis of various materials by measuring changes in a sample's mass and heat flow as a function of temperature or time.
Automatically generated - may contain errors
Lab products found in correlation
Jsm 6360, by JEOL (3 mentions)
Avance 2 400 spectrometer, by Bruker (2 mentions)
Jsm 100cx system, by JEOL (2 mentions)
Silica gel g, by Merck Group (2 mentions)
Icap 7600, by Thermo Fisher Scientific (1 mentions)
D8 advance, by Rigaku (1 mentions)
Tlc silica gel 60 f254, by Merck Group (1 mentions)
Xevo g2 xs qtof mass spectrometer, by Waters Corporation (1 mentions)
Alpha 2, by Bruker (1 mentions)
Jnm ecs400, by JEOL (1 mentions)
Phi 5000 versa prob 2, by Thermo Fisher Scientific (1 mentions)
Spectrum bx ft ir system, by PerkinElmer (1 mentions)
Labram hr system, by Horiba (1 mentions)
3 protocols using precisely sta 6000
1
Characterization of Inorganic Compounds
2
Detailed Physicochemical and Structural Characterization
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Melting points were determined
in open capillaries and are uncorrected. Infrared (FT-IR) spectra
were recorded on a Bruker Alpha II system (υmax in cm–1) on KBr disks. 1H NMR and 13C NMR (400, 500
MHz and 100, 125 MHz, respectively) spectra were recorded on Bruker
Avance II-400 and JEOL JNM ECS400 spectrometers in DMSO-d6 and CDCl3 (chemical shifts in δ with
TMS as the internal standard). High-resolution mass spectrometry (HRMS)
spectra were recorded on a Waters Xevo-G2-XS QT of Mass spectrometer.
Transmission electron microscopy (TEM) images were recorded on a JEOL
JSM 100CX. Scanning electron microscopy (SEM) and energy-dispersive
X-ray (EDX) were recorded on a JSM-6360 (JEOL). Thermogravimetric
analysis (TGA) was recorded on a Perkin Elmer Precisely STA 6000 simultaneous
thermal analyzer. Powder XRD was recorded on a 9 kW powder X-ray diffraction
system (make: Rigaku Technologies, JAPAN, model: Smartlab). Silica
gel G (E-Merck, India) was used for TLC. Hexane refers to the fraction
boiling between 60 and 80 °C.
in open capillaries and are uncorrected. Infrared (FT-IR) spectra
were recorded on a Bruker Alpha II system (υmax in cm–1) on KBr disks. 1H NMR and 13C NMR (400, 500
MHz and 100, 125 MHz, respectively) spectra were recorded on Bruker
Avance II-400 and JEOL JNM ECS400 spectrometers in DMSO-d6 and CDCl3 (chemical shifts in δ with
TMS as the internal standard). High-resolution mass spectrometry (HRMS)
spectra were recorded on a Waters Xevo-G2-XS QT of Mass spectrometer.
Transmission electron microscopy (TEM) images were recorded on a JEOL
JSM 100CX. Scanning electron microscopy (SEM) and energy-dispersive
X-ray (EDX) were recorded on a JSM-6360 (JEOL). Thermogravimetric
analysis (TGA) was recorded on a Perkin Elmer Precisely STA 6000 simultaneous
thermal analyzer. Powder XRD was recorded on a 9 kW powder X-ray diffraction
system (make: Rigaku Technologies, JAPAN, model: Smartlab). Silica
gel G (E-Merck, India) was used for TLC. Hexane refers to the fraction
boiling between 60 and 80 °C.
3
Characterization of Novel Compounds
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Melting points were determined
in open capillaries and are uncorrected.
IR spectra were recorded on a Spectrum BX FT-IR system, PerkinElmer
(νmax in cm–1) on KBr disks. 1H NMR and 13C NMR (400 and 100 MHz, respectively)
spectra were recorded using a Bruker Avance II-400 spectrometer, using
CDCl3 as the solvent (chemical shifts in δ with TMS
as internal standard). Mass spectra were recorded on a Waters ZQ-4000
system. Transmission electron microscopy analysis was carried out
using a JEOL JSM 100CX system. Scanning electron microscopy and energy-dispersive
X-ray analysis were carried out using a JSM-6360 (JEOL) system. Thermogravimetric
analysis was carried out using a PerkinElmer Precisely STA 6000 simultaneous
thermal analyzer. CHN analysis was carried out using a CHN-OS analyzer
(PerkinElmer 2400, Series II). Powder XRD analysis was carried out
using a Bruker D8 Advance XRD instrument SWAX. Raman analysis was
carried out on a Horiba Jobin Vyon, model Lab Ram HR system. X-ray
photoelectron spectroscopy was performed using a PHI 5000 Versa Prob
II, FEI Inc. system. Inductively coupled plasma atomic emission spectroscopy
analysis was carried out on an Arcos simultaneous ICP spectrometer.
Silica gel G (E-Merck, India) was used for TLC analysis. Hexane refers
to the fraction boiling between 60 and 80 °C.
in open capillaries and are uncorrected.
IR spectra were recorded on a Spectrum BX FT-IR system, PerkinElmer
(νmax in cm–1) on KBr disks. 1H NMR and 13C NMR (400 and 100 MHz, respectively)
spectra were recorded using a Bruker Avance II-400 spectrometer, using
CDCl3 as the solvent (chemical shifts in δ with TMS
as internal standard). Mass spectra were recorded on a Waters ZQ-4000
system. Transmission electron microscopy analysis was carried out
using a JEOL JSM 100CX system. Scanning electron microscopy and energy-dispersive
X-ray analysis were carried out using a JSM-6360 (JEOL) system. Thermogravimetric
analysis was carried out using a PerkinElmer Precisely STA 6000 simultaneous
thermal analyzer. CHN analysis was carried out using a CHN-OS analyzer
(PerkinElmer 2400, Series II). Powder XRD analysis was carried out
using a Bruker D8 Advance XRD instrument SWAX. Raman analysis was
carried out on a Horiba Jobin Vyon, model Lab Ram HR system. X-ray
photoelectron spectroscopy was performed using a PHI 5000 Versa Prob
II, FEI Inc. system. Inductively coupled plasma atomic emission spectroscopy
analysis was carried out on an Arcos simultaneous ICP spectrometer.
Silica gel G (E-Merck, India) was used for TLC analysis. Hexane refers
to the fraction boiling between 60 and 80 °C.
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