Apexiv suite2022

X-ray diffraction experiments
were performed at the analytical facility of the University of Paderborn
or at the University of Innsbruck. Data collection was performed using
the ApexIII and ApexIV software package on a Bruker D8 Venture (Paderborn)
or on a Bruker D8 Quest instrument (Innsbruck). Data refinement and
reduction were performed using the Bruker ApexIII 2019 or ApexIV suite
2022. Using the OLEX2 software package,^{120 (link)} all structures were solved with SHELXT^{121 (link)} and refined with SHELXL.^{122 (link)} Strongly
disordered solvent molecules have been removed using the SQUEEZE operation.^{123 (link)} All nonhydrogen atoms were refined anisotropically,
and hydrogen atoms were included at the geometrically calculated positions
and refined using a riding model. For further crystallographic details,
see Tables S1 and S2 in the Supporting
Information.

X-ray diffraction experiments
were performed at the analytical facility of the University of Innsbruck.
Data collection was performed using the ApexIV software package on
a Bruker D8 Quest instrument. Data refinement and reduction were performed
using the Bruker ApexIV suite 2022. Using the OLEX2 software package,^{165 (link)} all structures were solved with SHELXT^{166 (link)} and refined with SHELXL.^{167 (link)} Strongly disordered solvent molecules have been removed
using the SQUEEZE operation.^{168 (link)} All non-hydrogen
atoms were refined anisotropically, and hydrogen atoms were included
at the geometrically calculated positions and refined using a riding
model. For further crystallographic details, see Tables S1 and S2 in the Supporting Information.