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Tg 209 f3 tarsus instrument

Manufactured by Netzsch
Sourced in Germany, United States

The TG 209 F3 Tarsus is a thermogravimetric analysis (TGA) instrument designed for thermal analysis. The instrument measures the change in a sample's mass as a function of temperature or time in a controlled atmosphere. It provides quantitative data on processes such as evaporation, sublimation, absorption, adsorption, and decomposition.

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5 protocols using tg 209 f3 tarsus instrument

1

Thermal Characterization of Materials

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Thermogravimetric analysis was performed using a TG 209 F3 Tarsus instrument (NETZSCH, Selb, Germany). The open corundum crucible was used for measurements. The analyzed samples were heated at 5 °C/min from 25 to 900 °C under a nitrogen atmosphere (flow rate, 30 mL/min).
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2

Characterization of Cu-BTC Metal-Organic Frameworks

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The PXRD patterns of the Cu-BTCs were recorded using a Rigaku MiniFlex diffractometer (Rigaku Corp., Neu-Isenburg, Germany). FTIR spectra were measured on a Nicolet iS10 FTIR spectrometer with KBr pellets (Thermo Fisher Scientific, Waltham, MA, USA). TGA was performed using a TG 209 F3 Tarsus® instrument (NETZSCH, Burlington, MA, USA). The surface morphology and elemental composition of Cu-BTC were characterized using SEM-EDS (FE-SEM, JEOL JSM-5800F, Peabody, MA, USA). N2 adsorption isotherms were obtained by using a BELSORP-mini II instrument (BEL Japan, Inc., Tokyo, Japan). High-purity (99.999%) gases were used throughout the adsorption experiments. All samples were activated by rinsing them thoroughly, followed by drying under vacuum for 24 h prior to the gas sorption measurements.
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3

Comprehensive Materials Characterization of Cu-MOF Scaffolds

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PXRD patterns of Cu-MOF, PS, and PS@Cu-MOF were recorded using a Rigaku MiniFlex diffractometer (Rigaku Corp, Neu-Isenburg, Germany). The FT-IR spectrum was measured on a Bio-Rad FTS 135 spectrometer (Hercules, CA, USA). DSC runs were carried out using a DSC 214 Polyma (NETZSCH, Burlington, MA, USA). TGA was performed using a TG 209 F3 Tarsus® instrument (NETZSCH, Burlington, MA, USA). The surface morphology and elemental composition of PS and the PS@Cu-MOF scaffolds were characterized using SEM-EDS (FE-SEM, JEOL JSM-5800F, Peabody, MA, USA). The mechanical properties of PS and PS@Cu-MOF were evaluated using a TA rheometer (Discovery HR 10, New Castle, DE, USA). The degradation of PS@Cu-MOF was carried out by ICP-MS (Agilent Marker 7700, RF Generator Power 1550 W, Tokyo, Japan). The colorimetric absorbance was determined using a microplate reader (Synergy H1, BioTek, Winooski, VT, USA), and the live/dead double-stained cells were imaged by fluorescence microscopy (IX83, Olympus, Center Valley, PA, USA).
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4

Comprehensive Characterization of Composite Materials

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Transmission electron microscopy (TEM, JEM-2100) and field emission scanning electron microscopy (SEM, Zeiss Supra 55) were employed to obtain images of composite morphology. The product was analyzed using a Fourier transform infrared (FTIR) spectrometer (Cary 610/670 micro IR spectrometer). Thermogravimetric analysis (TGA) was conducted using a TG209F3 Tarsus instrument (NETZSCH, Germany) at a heating rate of 10 °C min−1, with the ambient temperature raised to 900 °C under a nitrogen atmosphere. X-Ray photoelectron spectroscopy (XPS) measurements were carried out to analyze the element composition of composite materials. Electrochemical tests were conducted on an electrochemical workstation (CH Instruments, 760E). Electrochemical tests in both three-electrode and two-electrode systems are presented in the ESI.
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5

Thermogravimetric Analysis of Samples

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Thermogravimetric analysis was performed using a TG 209 F3 Tarsus instrument (NETZSCH, Selb, Germany). The open corundum crucible was used for measurements. The analyzed samples were heated at a 5 K/min rate under a nitrogen atmosphere (30 mL/min).
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