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2 protocols using nickel 2 acetate

1

Synthesis and Characterization of HP-β-CD Complexes

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HP-β-CD
with a molar substitution between 0.6 and 0.9 was kindly received
as a gift from Wacker Chemie AG (Germany). Sodium hypophosphite hydrate
(SHP, Sigma-Aldrich), BTCA (Sigma-Aldrich, 99%), PAHs [acenaphthene
(Ace, 99%), fluorene (Flu, 98%), fluoranthene (FluA, 98%), phenanthrene
(Phe, 98%), and pyrene (Pyr, 98%)], and heavy metals (zinc(II) acetate,
manganese(II) acetate, lead(IV) acetate, cadmium(II) acetate, copper(II)
acetate, and nickel(II) acetate) were all obtained from Sigma-Aldrich.
High-purity water was produced from a Millipore Milli-Q system (resistivity ≥
18 MΩ cm).
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2

Synthesis of Tungsten Disulfide Nanocomposites

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Bulk tungsten(iv) disulfide (WS2, powder 99.9%), Nickel(ii) acetate (Ni(CH3COO)2·4H2O, powder <99%), Iron(ii) acetate (Fe(CH3COO)2, powder 96%) polyethylene (d = 0.92 g mL−1, powder) were obtained from Sigma-Aldrich and cetyltrimethylammonium bromide (CTAB) was purchased from AppliChem.
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