1,3PDT (>99%), (3-aminopropyl)triethoxysilane (99%), butylhydroxytoluene (BHT; analytical standard), 1,8-diazabicyclo[5.4.0]undec-7-ene (98%), dichloromethane (DCM; anhydrous, ≥ 99.8%), N,N-dimethyl-n-octadecyl-3-aminopropyltrimethoxtsilyl chloride (42 wt% in methanol), 2,2-dimethoxy-2-phenylacetophenone (DMPA; 99%), poly(vinyl alcohol) (cold water soluble, molecular weight of 31,000 to 50,000, 98 to 99% hydrolyzed) were purchased from Sigma-Aldrich. Hydrochloric acid (HCl; certified ACS Plus, 36.5 to 38.0%), magnesium sulfate (anhydrous powder) (MgSO4), and tetrahydrofuran (high-performance liquid chromatography grade) were purchased from Thermo Fisher Scientific. RM82 and RM257 were purchased from Wilshire Technologies. 5CB were purchased from Tokyo Chemical Industry. NOA63 was purchased from Noland Optical Adhesive. SilcPigTM was purchased from Smooth-On. Photoinitiator, Irgacure 369, was purchased from Ciba. All chemicals were used as received. PTFE tubing for templating LCE fiber was purchased from Cole-Parmer.
Irgacure 369
Manufactured by Novartis
Irgacure 369 is a photoinitiator used in the curing of various photopolymerizable systems. It is a highly efficient type I photoinitiator that absorbs in the UV-A and visible light regions. Irgacure 369 is commonly used in applications such as coatings, inks, and adhesives.
Automatically generated - may contain errors
Lab products found in correlation
Tetrahydrofuran, by Thermo Fisher Scientific (1 mentions)
1 8 diazabicyclo 5.4.0 undec 7 ene, by Merck Group (1 mentions)
Silc pigtm, by Smooth-On (1 mentions)
Dichloromethane, by Merck Group (1 mentions)
Polyvinyl alcohol (pva), by Merck Group (1 mentions)
2 2 dimethoxy 2 phenylacetophenone, by Merck Group (1 mentions)
Dimethyl methylphosphonate, by Merck Group (1 mentions)
Acetone, by Merck Group (1 mentions)
Tetrahydrofuran, by Biosolve (1 mentions)
Toluene, by Biosolve (1 mentions)
3 protocols using irgacure 369
1
Fabrication of Liquid Crystal Elastomer Fibers
2
Preparing Liquid Crystal Polymer Films with Enhanced UV Stability
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
RM82 (Mw = 120,000, Sigma Aldrich) and Irgacure369 (provided
by Ciba, Basel, Switzerland) were used as the nematic reactive mesogen
and photoinitiator, respectively. Also, silane-coated rutile TiO2
nanoparticles (SSNANO Co., Ltd.) with an average size of 20 nm were
selected as an inorganic UV-light absorber. Meanwhile, to carry out
the studies as accurately as possible, the TiO2 nanoparticles were
mixed with Tinuvin460 (BASF) as an organic UV-light absorber, which
has already been studied25 (link) in specific
weight percentages as listed inTable. 1 . These materials cause a low glass transition temperature
(Tg) in the respective LCN polymer films.23 (link),24 (link) It is also noteworthy that, further, polyimide X610-33C (JNC Corporation,
Tokyo, Japan) and polyimide SE-5662 (Nissan) were employed to create
surface alignment layers with planar and homeotropic molecular orientations,
respectively, to achieve a splay molecular orientation in the LCN
polymer matrix.
by Ciba, Basel, Switzerland) were used as the nematic reactive mesogen
and photoinitiator, respectively. Also, silane-coated rutile TiO2
nanoparticles (SSNANO Co., Ltd.) with an average size of 20 nm were
selected as an inorganic UV-light absorber. Meanwhile, to carry out
the studies as accurately as possible, the TiO2 nanoparticles were
mixed with Tinuvin460 (BASF) as an organic UV-light absorber, which
has already been studied25 (link) in specific
weight percentages as listed in
(Tg) in the respective LCN polymer films.23 (link),24 (link) It is also noteworthy that, further, polyimide X610-33C (JNC Corporation,
Tokyo, Japan) and polyimide SE-5662 (Nissan) were employed to create
surface alignment layers with planar and homeotropic molecular orientations,
respectively, to achieve a splay molecular orientation in the LCN
polymer matrix.
3
Synthesis of Acryloyl-Based Compounds
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
2-Methyl-1,4-phenylene bis(4-(3-(acryloyloxy)propoxy)benzoate)
[RM 257] (1 ) and 4-methoxyphenyl 4-((6-(acryloyloxy)hexyl)oxy)benzoate
[RM 105] (2 ) were obtained from Merck. 4-((6-(Acryloyloxy)hexyl)oxy)benzoic
acid (3 ) and 4-((6-(acryloyloxy)hexyl)oxy)-2-methylbenzoic
acid (4 ) were purchased from Synthon. Irgacure 369 (6 ) was purchased from CIBA. Chiral dopant (R)-(+)-3-methyladipic acid (5 ) and dimethylmethylphosphonate
(7 ) were from Sigma-Aldrich, as well as trimethylamine
and diisopropylamine. Solvents tetrahydrofuran and toluene were purchased
from Biosolve, and acetone was purchased from Sigma-Aldrich.
[RM 257] (
[RM 105] (
acid (
acid (
(
and diisopropylamine. Solvents tetrahydrofuran and toluene were purchased
from Biosolve, and acetone was purchased from Sigma-Aldrich.
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!