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3 butyn 1 ol

Manufactured by Merck Group
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3-butyn-1-ol is a chemical compound that serves as a versatile building block in organic synthesis. It consists of a linear four-carbon chain with a terminal alkyne group and a hydroxyl group. This compound is commonly used in the preparation of various pharmaceuticals, fine chemicals, and other industrial products.

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Lab products found in correlation

1 5 7 triazabicyclo 4.4.0 dec 5 ene, by Merck Group (1 mentions) Tetrahydrofuran thf, by Thermo Fisher Scientific (1 mentions) Anhydrous ch2cl2, by Merck Group (1 mentions) Hydrofluoric acid, by Merck Group (1 mentions) Cyclopropylamine, by Merck Group (1 mentions) Hydrogen peroxide, by Merck Group (1 mentions) Sulfuric acid, by Merck Group (1 mentions) Mesitylene, by Merck Group (1 mentions) Terephthalic acid, by Merck Group (1 mentions) 1 octanol, by Merck Group (1 mentions) 4 chlorophenol 4 cp, by Merck Group (1 mentions) Hydrazine n2h4, by Merck Group (1 mentions) Chloroform, by Merck Group (1 mentions) Acetone, by Merck Group (1 mentions) Ascorbic acid, by Merck Group (1 mentions) Titanium 4 isopropoxide, by Merck Group (1 mentions) Se1700, by Dow (1 mentions)

4 protocols using 3 butyn 1 ol

1

Synthesis and Characterization of COP

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2-Chloro-2-oxo-1,3,2-dioxaphospholane (COP) was synthesized, distilled under vacuum and stored at −20 °C.23 (link) Tetrahydrofuran (THF) purchased from Alfa Aesar in Shanghai was used after distillation. After purification by phthalic anhydride, sodium hydroxide and calcium hydride, triethylamine (TEA, Aladdin) was distilled for subsequent studies. Monomethoxy poly(ethylene glycol) (mPEG, Mn = 5000 g mol−1) was acquired from Sigma-Aldrich and was dried by azeotropic distillation with toluene subsequently. 1,5,7-Triazabicyclo[4.4.0]dec-5-ene (TBD), anhydrous CH2Cl2, 3-butyn-1-ol, DOX and Ce6 were purchased from Sigma-Aldrich. All other undeclared reagents and solvents were of analytical grade and used as received.
Zhou J., Sun C, & Yu C. (2020). Highly-controllable drug release from core cross-linked singlet oxygen-responsive nanoparticles for cancer therapy. RSC Advances, 10(34), 19997-20008.
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2

Silicon (111) Surface Functionalization

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In this experiment, P-type silicon (111) (0.001–0.005 Ω cm) was ordered from Semiconductor Wafer, Inc. (Hsinchu, Taiwan). Cyclopropylamine (98%), 3-Butyn-1-ol (97%), Mesitylene (98%), Hydrogen peroxide (30%), Hydrofluoric acid (ACS reagent, 48%) as well as sulfuric acid (99.99%) were acquired from Sigma-Aldrich (St Louis, MO, USA), except where noted, and used with no further purification.
Zida S.I., Lin Y.D, & Khung Y.L. (2021). Sonochemical Reaction of Bifunctional Molecules on Silicon (111) Hydride Surface. Molecules, 26(20), 6166.
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3

Synthesis of Hybrid Nanomaterials

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All chemical reagents used in the experiments were obtained from commercial sources as guaranteed grade reagents. Titanium (IV) isopropoxide 97% (TTIP: Ti[OCH(CH3)2]4), 3-butyn-1-ol 97% (HC≡CCH2CH2OH or C4H6O), 1-octanol 98% (CH3(CH2)7OH), chloroform 99% (CHCl3), acetone ACS reagent ≥ 99.5% (CH3COCH3), ethanol absolute (CH3CH2OH), 4-chlorophenol (4-CP), Cu(CH3COO)2, ascorbic acid (C6H8O6), hydrazine (N2H4), hexadecylamine (HDA), vanadium triisopropoxide (VOTPP), cadmium chloride (CdCl2), sodium sulfide (Na2S), and terephthalic acid (TA) were purchased from Sigma-Aldrich (St. Louis, MO, USA). All reagents were of analytical grade and were used without further purification.
Lozano H., Devis S., Aliaga J., Alegría M., Guzmán H., Villarroel R., Benavente E, & González G. (2022). Two-Dimensional Titanium Dioxide–Surfactant Photoactive Supramolecular Networks: Synthesis, Properties, and Applications for the Conversion of Light Energy. International Journal of Molecular Sciences, 23(7), 4006.
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4

Fabrication of Superhydrophobic PDMS Surface

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A polydimethylsiloxane adhesive (SE1700) with a curing agent was purchased from Dow Corning, United States 3-Butyn-1-ol (97%) and 1H,1H,2H,2H-perfluorooctyl-trichlorosilane (CF3(CF2)5CH2CH2SiCl3; PFTS, 97%) were purchased from Sigma-Aldrich. Toluene and absolute ethanol were purchased from the Chengdu Kelong Chemical Company, China.
He Z., Wang N., Mu L., Wang Z., Su J., Chen Y., Luo M., Wu Y., Lan X, & Mao J. (2023). Porous polydimethylsiloxane films with specific surface wettability but distinct regular physical structures fabricated by 3D printing. Frontiers in Bioengineering and Biotechnology, 11, 1272565.
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