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3 4 ethylenedioxythiophene edot monomer

Manufactured by Merck Group

3,4-ethylenedioxythiophene (EDOT) monomer is a colorless liquid organic compound used in the production of conductive polymers. It is a key building block for the synthesis of poly(3,4-ethylenedioxythiophene) (PEDOT), a widely used conductive polymer material.

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2 protocols using 3 4 ethylenedioxythiophene edot monomer

1

Synthesis of MWCNT Sheets for Energy Applications

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Multi-walled carbon nanotube (MWCNT) sheets were drawn from ~400 μm high MWCNT forests27 (link) that were grown by chemical vapor deposition on iron catalyst-coated silicon wafers using acetylene (C2H2) gas as the carbon precursor36 (link). Iron(III)p-toluene sulfonate hexahydrate (Fe(III)PTS; Mw, 677.52), pyridine (anhydrous, 99.8%), 1-butanol (≥99%), and 3,4-ethylenedioxythiophene (EDOT) monomer (97%) were purchased from Sigma-Aldrich. Sulfuric acid solutions (2N; 1 M H2SO4) were purchased from Daejung Chemicals.
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2

Fabrication of Porous PCL Scaffolds

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3D printed macroporous medical grade PCL scaffolds with porosity of 70% were purchased from Osteopore TM . Circular samples (12 mm diameter) were cut out of the 5 x 5 cm sheet using a metallic hole-puncher. PCL films (to be used for FTIR and contact angle measurements) were thermally pressed into a thickness of approximately 120 µm. Briefly, a known mass of PCL was placed between two stainless steel sheets on a Carver bench press (Carver Inc, USA). Temperature was elevated to 100 °C and pressure exerted for 30 min. The pressed film was then allowed to cool to room temperature via normal convection cooling.
Clevios™ CB 40 V2 (40% wt/wt Fe(III) p-toluenesulfonate (Tosylate) in butanol) was purchased from Heraeus (Germany). 3,4-Ethylenedioxythiophene (EDOT) monomer (142.18 g/mol), pyridine (79.10 g/mol), and the triblock copolymer poly(ethylene glycol)-block-poly(propylene glycol)-blockpoly(ethylene glycol) (PEG-PPG-PEG, 5800 g/mol) were purchased from Sigma-Aldrich. All chemicals were used as received without further purification.
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