Natural graphite flakes were purchased from Nacional de Grafite Ltda company (Minas Gerais, Brazil). Phosphoric acid (H3PO4, >99%), sulfuric acid (H2SO4, 95–98%), dimethylformamide (DMF), p-phenylenediamine (>99%), dibenzylamine (97%), diisopropylamine (99%) and piperidine (99%) were all purchased from Sigma-Aldrich; potassium permanganate (KMnO4, 99%) was acquired from Neon Commercial.
Dibenzylamine
Manufactured by Merck Group
Sourced in United States
Dibenzylamine is a chemical compound commonly used in various laboratory applications. It is a secondary amine with the molecular formula C₁₄H₁₅N. Dibenzylamine serves as a precursor and intermediate in organic synthesis, often utilized in the production of other chemical compounds. Its core function is to provide a nitrogen-containing building block for more complex molecular structures.
Automatically generated - may contain errors
Lab products found in correlation
Milli q direct 8 system, by Merck Group (2 mentions)
Hydrochloric acid (hcl), by Honeywell (2 mentions)
Methacrylic acid, by Merck Group (2 mentions)
Propranolol hydrochloride, by Merck Group (2 mentions)
Sulfuric acid, by Merck Group (1 mentions)
Phosphoric acid, by Merck Group (1 mentions)
Dimethylformamide, by Merck Group (1 mentions)
H3po4, by Merck Group (1 mentions)
Piperidine, by Merck Group (1 mentions)
Diisopropylamine, by Merck Group (1 mentions)
P phenylenediamine, by Merck Group (1 mentions)
Methanol, by Merck Group (1 mentions)
Acetonitrile, by Merck Group (1 mentions)
Metoprolol tartrate, by Merck Group (1 mentions)
Ephedrine, by Merck Group (1 mentions)
Inhibitor remover, by Merck Group (1 mentions)
Methyl tert butyl ether (mtbe), by Merck Group (1 mentions)
Toluene, by Merck Group (1 mentions)
Ethylene glycol dimethacrylate, by Merck Group (1 mentions)
Strata x cw, by Phenomenex (1 mentions)
4 protocols using dibenzylamine
1
Graphite Flake Preparation Protocol
2
Synthesis and Characterization of Chiral Ionic Imprints
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Methacrylic acid (MAA), ethylene glycol dimethacrylate (EDMA), propranolol hydrochloride, dibenzylamine (DBA), (R)-(−)-2-benzylamino-1-phenylethanol (RBz), N-Benzyl-2-phenethylamine (NBz), metoprolol tartrate, ephedrine, acetic acid (AcOH) were purchased from Sigma (St. Louis, MO, USA), N-benzylmethylamine from Alfa Aesar (Haverhill, MA, USA), azobisisobutyronitrile (AIBN) from Fluka (Buchs, Switzerland), HCl from Riedel-De Haën (Seelze, Germany), acetonitrile and methanol from Merck (Darmstadt, Germany) Water was purified with a Milli Q Direct 8 system (Millipore, Burlington, MA, USA).
Prior to use, propranolol hydrochloride and metoprolol tartrate were transformed to their free base form, by means of neutralization with 0.2 M NaOH solution followed by extraction with methyl tert-butyl ether.
Prior to use, propranolol hydrochloride and metoprolol tartrate were transformed to their free base form, by means of neutralization with 0.2 M NaOH solution followed by extraction with methyl tert-butyl ether.
3
Polymeric Ion-Exchange Sorbent Synthesis
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Propranolol hydrochloride, methacrylic acid, dibenzylamine (DBA), ethylene glycol dimethacrylate (EDMA), tetrabutylammonium hydroxide solution (40% in water) and inhibitor remover (Aldrich 306312) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Sodium hydroxide (NaOH), sodium dihydrogen phosphate monohydrate (NaH2PO4·H2O), tetrabutylammonium bromide (TBABr) and azobisisobutyronitrile (AIBN) were obtained from Fluka (Buchs, Switzerland). Acetonitrile (HPLC grade), methanol, toluene and methyl tert-butyl ether were ordered from Merck (Darmstadt, Germany). Water was purified with a Milli Q Direct 8 system (Millipore, Burlington, MA, USA). HCl was purchased from Riedel-De Haën (Seelze, Germany). The weak cation exchanger, Strata-X-CW, was obtained as a free sample from Phenomenex (Macclesfield, UK). Its binding capacity was 0.76 mol/kg according to the manufacturer.
The structure of the used compounds can be found in theSupplementary Materials (Figure S1) .
The structure of the used compounds can be found in the
4
Synthesis of Fluorescent Conjugates
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Bromoethanol, p-nitrophenyl
chloroformate, 3-toluenesulfonyl chloride, triethylamine, 2,4-quinolinediol,
phenylphosphonyl dichloride, p-xylylendiamine, valeroyl
chloride, calcium oxide, di-tert-butyl decarbonate,
deuterated solvents, ethyl acetate, dimethyl sulfoxide (DMSO), sodium
hydroxide (NaOH), hydrochloric acid (HCl), 2,4-dimethoxybenzyl amine,
trifluoroacetic acid (TFA), platinum on carbon (10% Pt/C), benzylamine,
benzyl alcohol, dibenzylamine, 4-dimethylaminopyridine (DMAP), 2,2′-azobis(2-methylpropionitrile)
(AIBN), n-butylamine, N,N-dimethylacrylamide (DMA), sodium bicarbonate (NaHCO3), cholesterol, acryloxyethyl thiocarbamoyl rhodamine B, 2-mercaptoethanol,
2,2′-dipyridyl disulfide, and N,N′-dicyclohexylcarbodiimide (DCC) were obtained from Sigma-Aldrich.
Potassium sulfite, sulfur, tris(2-carboxyethyl)phosphin (TCEP), and
sodium sulfate were purchased from Acros Organics, Alfa Aesar, TCI
Chemicals, and Carl Roth GmbH+ Co. KG, respectively. N,N-Dimethylformamide (DMF), chloroform, dichloromethane
(DCM), tetrahydrofuran (THF), succinimidyl 4-(N-maleimidomethyl)cyclohexane-1-carboxylate
(SMCC), and Gibco Dulbecco’s phosphate-buffered saline (DPBS)
were obtained from Thermo Fisher Scientific Inc., and methanol (MeOH),
acetone, and ethanol were obtained from Honeywell International.
chloroformate, 3-toluenesulfonyl chloride, triethylamine, 2,4-quinolinediol,
phenylphosphonyl dichloride, p-xylylendiamine, valeroyl
chloride, calcium oxide, di-tert-butyl decarbonate,
deuterated solvents, ethyl acetate, dimethyl sulfoxide (DMSO), sodium
hydroxide (NaOH), hydrochloric acid (HCl), 2,4-dimethoxybenzyl amine,
trifluoroacetic acid (TFA), platinum on carbon (10% Pt/C), benzylamine,
benzyl alcohol, dibenzylamine, 4-dimethylaminopyridine (DMAP), 2,2′-azobis(2-methylpropionitrile)
(AIBN), n-butylamine, N,N-dimethylacrylamide (DMA), sodium bicarbonate (NaHCO3), cholesterol, acryloxyethyl thiocarbamoyl rhodamine B, 2-mercaptoethanol,
2,2′-dipyridyl disulfide, and N,N′-dicyclohexylcarbodiimide (DCC) were obtained from Sigma-Aldrich.
Potassium sulfite, sulfur, tris(2-carboxyethyl)phosphin (TCEP), and
sodium sulfate were purchased from Acros Organics, Alfa Aesar, TCI
Chemicals, and Carl Roth GmbH+ Co. KG, respectively. N,N-Dimethylformamide (DMF), chloroform, dichloromethane
(DCM), tetrahydrofuran (THF), succinimidyl 4-(N-maleimidomethyl)cyclohexane-1-carboxylate
(SMCC), and Gibco Dulbecco’s phosphate-buffered saline (DPBS)
were obtained from Thermo Fisher Scientific Inc., and methanol (MeOH),
acetone, and ethanol were obtained from Honeywell International.
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