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3d feg microscope

Manufactured by Thermo Fisher Scientific

The 3D FEG microscope is a high-performance electron microscope that uses a field emission gun (FEG) as the electron source. It provides high-resolution imaging and analytical capabilities for a wide range of samples. The microscope is designed to deliver exceptional image quality and analytical data, making it a valuable tool for materials science, nanotechnology, and other advanced research applications.

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2 protocols using 3d feg microscope

1

Electrochemical Characterization of Nanocomposite

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All electrochemical experiments
were performed by using a Biologics SP-150 potentiostat, which is
a three-electrode system consisting of auxiliary, counter, and working
electrodes. In this system, Ag/AgCl is used as an auxiliary, platinum
as a counter, and gold wire as a working electrode. The synthesized
nanocomposite was characterized by FESEM to evaluate the surface morphology
using a FEI Quanta 3D FEG microscope. The crystallinity was analyzed
with X-ray diffraction (XRD) using a Rigaku Smart Lab (2θ range:
5 to 40°) diffractometer. FTIR spectra were recorded from a Bruker
Tensor 37 instrument in the range of 500–4000 cm–1. Double-distilled water was used throughout the experiment.
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2

Characterization of nanomaterials

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SEM images were recorded by a FEI Quanta 3D FEG microscope, using a 5-kV electron beam and a secondary electron detector. XRD patterns were obtained by a Bruker 2D phaser (Cu Kα radiation, λ = 1.5405 Å). UV-vis-NIR absorption measurements were performed by PerkinElmer Lambda 900 UV-vis-NIR spectrophotometer. Steady-state photoluminescence spectra were measured by Edinburgh Instruments FLSP920 double-monochromator luminescence spectrometer, with a near-infrared photomultiplier (Hamamatsu).
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