Fourier transform infrared spectroscopy (ATR-FTIR) analysis was carried out for the composites using a Nicolet iN10 FTIR microscope (Thermo-Scientific, Winsford, UK) with a Germanium micro tip accessory, and the scanning range was between 400 and 4000 cm− 1 wavelengths.
Nicolet in10 ftir microscope
Manufactured by Thermo Fisher Scientific
Sourced in United Kingdom
The Nicolet iN10 FTIR microscope is a compact and versatile instrument designed for infrared microscopy analysis. It utilizes Fourier Transform Infrared (FTIR) spectroscopy to provide high-quality images and spectra of small samples. The core function of the Nicolet iN10 FTIR microscope is to perform non-destructive, chemical analysis of microscopic samples.
Automatically generated - may contain errors
Lab products found in correlation
Atr ftir, by Thermo Fisher Scientific (1 mentions)
Cary 60 spectrophotometer, by Agilent Technologies (1 mentions)
Dpx 200, by Bruker (1 mentions)
Nicolet is50 ftir spectrometer, by Thermo Fisher Scientific (1 mentions)
Drx 400 spectrometer, by Bruker (1 mentions)
S 3400n 2, by Hitachi (1 mentions)
Xrd 6000, by Shimadzu (1 mentions)
Dtg 60, by Shimadzu (1 mentions)
12 protocols using nicolet in10 ftir microscope
1
Analyzing Composite Materials via ATR-FTIR
2
FT-IR Spectral Analysis of Samples
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FT-IR spectra of the samples were obtained using a Thermo Scientific Nicolet iN 10 FT-IR microscope with an FT-IR spectrometer from 4000 to 650 cm−1 at a resolution of 4 cm−1 and 128 scans per sample.
3
Transesterification Analysis of PBT-PET Blend
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To examine whether the blend of PBT and PET underwent transesterification, Fourier transform infrared spectroscopy (ATR-FTIR) analysis was conducted on the 60/40 PBT–PET blend and PBT–PET–Al composites bars. The analysis was conducted using a Nicolet iN10 FTIR microscope (Thermo Scientific, Winsford, UK) equipped with a germanium micro tip accessory. The wave number scanning range was set between 400 and 4000 cm−1.
4
ATR-FTIR Surface Functional Analysis
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Fourier transform infrared spectroscopy (ATR-FTIR, Thermo Scientific, Winsford, UK) analysis was performed using a Nicolet iN10 FTIR microscope with a germanium microtip. The analysis was performed in the wavenumber range of 650–4000 at a resolution of 4 cm−1 with 64 scans. Three spectral measurements were performed on each sample in various locations to analyze the functional groups on the surface of the composites.
5
Adsorption Kinetics of Pharmaceutical Powders
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Five kinds of pharmaceutical powders were weighed to 25 g, respectively. These powder and 4 g activated carbon were put into the closed vessel, respectively. It was left in closed vessel for 20 min, 40 min, 60 min, 80 min, 100 min and 120 min, respectively. Each activated carbon was removed, dried, weighed, respectively.
FT-IR spectra: FT-IR spectra of the above samples were obtained using a Thermo Scientific Nicolet iN10 FT-IR microscope as previously mentioned (Lin et al., 2015; Peng et al., 2014b (link), Peng et al., 2015 , Sun et al., 2014 , Wang et al., 2009 ).
FT-IR spectra: FT-IR spectra of the above samples were obtained using a Thermo Scientific Nicolet iN10 FT-IR microscope as previously mentioned (Lin et al., 2015; Peng et al., 2014b (link), Peng et al., 2015 , Sun et al., 2014 , Wang et al., 2009 ).
6
ATR-FTIR Analysis of Functional Groups
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Attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR) analysis was carried out using a Nicolet iN10 FTIR microscope (Thermo Scientific, Winsford, UK) with a Germanium microtip to determine the functional groups.
7
Bamboo Charcoal Adsorption Kinetics
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Five kinds of pharmaceutical powder were weighed in amounts of 25 g. These powders and 4 g bamboo charcoal were put into the closed vessel. It was blasted in a closed vessel for 20 min, 40 min, 60 min, 80 min, 100 min and 120 min. Each bamboo charcoal was removed, dried, and weighed.
FT-IR spectra. FT-IR spectra of the above samples were obtained using a Thermo Scientific Nicolet iN10 FT-IR microscope as previously (Lin et al., 2015 , Peng et al., 2014a (link), Peng et al., 2014b (link), Peng et al., 2014c (link), Sun et al., 2014 ).
FT-IR spectra. FT-IR spectra of the above samples were obtained using a Thermo Scientific Nicolet iN10 FT-IR microscope as previously (Lin et al., 2015 , Peng et al., 2014a (link), Peng et al., 2014b (link), Peng et al., 2014c (link), Sun et al., 2014 ).
8
Characterization of Organic Thin Films
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All 1H-NMR spectra were recorded with a DPX200 or a DRX400 spectrometer from Bruker with a 1H resonance frequency of 200.13 and 400.13 MHz, respectively. The residual solvent peak was used as internal standard for calibration of chemical shifts. Ultraviolet–visible (UV–vis) measurements were performed with a Cary 60 spectrophotometer from Agilent Technologies in quartz cuvettes with an optical path length of 1 cm. Reflection Fourier transform infrared (FTIR) spectroscopy measurements were conducted on a Nicolet iS50 FTIR spectrometer or a Nicolet iN10 FTIR microscope from Thermo Fisher Scientific. Samples were prepared as thin films on corresponding substrates by a drop cast process from organic solvents (ethanol or acetone).
9
Micro-FTIR Characterization of Material Samples
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Two micro-samples were prepared for the cross-sectional analysis carried out by optical microscopy (OM) and SEM-EDS. Additionally, a small part of the sample referred to as n.M1 was employed for micro-FTIR analyses.
Fourier Transform Infrared Spectroscopy (FTIR) FTIR spectroscopy analyses were performed using a Thermo Scientific Nicolet iN10 FT IR microscope instrument in transmission mode. A small fragment of the sample of n.M1 was mechanically separated and placed directly on a diamond cell. The sample was flattened on the diamond cell using a roller blade knife tool. The spectra were acquired in the 4,000-650 cm -1 spectral range using a liquid nitrogen-cooled MCT detector.
Fourier Transform Infrared Spectroscopy (FTIR) FTIR spectroscopy analyses were performed using a Thermo Scientific Nicolet iN10 FT IR microscope instrument in transmission mode. A small fragment of the sample of n.M1 was mechanically separated and placed directly on a diamond cell. The sample was flattened on the diamond cell using a roller blade knife tool. The spectra were acquired in the 4,000-650 cm -1 spectral range using a liquid nitrogen-cooled MCT detector.
10
FT-IR Analysis of Sample Films
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FT-IR spectra of the films were measured on a Thermo Scientific Nicolet In 10 FT-IR Microscope (Thermo Nicolet Corporation, Madison, WI) equipped with a liquid nitrogen cooled MCT detector. Dried samples were recorded with BaF2 disks in the range from 4000 to 650 cm−1 at a resolution of 4 cm−1 and 128 scans per sample.
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