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Advance 3 400 instrument

Manufactured by Bruker
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The ADVANCE III 400 is a high-performance nuclear magnetic resonance (NMR) spectrometer designed for analytical and research applications. It operates at a proton frequency of 400 MHz and provides reliable data collection and analysis capabilities.

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Advance III (58 citations) Advance 400 (46 citations) Advance III 400 (12 citations)

2 protocols using advance 3 400 instrument

1

NMR Spectroscopy of Organic Compounds

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1H NMR spectra were recorded at 400 MHz on a Bruker ADVANCE III 400 instrument. Chemical shifts (δH) are given in parts per million (ppm) as referenced to the appropriate residual solvent peak.
Tseng C.C., Baillie G., Donvito G., Mustafa M.A., Juola S.E., Zanato C., Massarenti C., Dall’Angelo S., Harrison W.T., Lichtman A.H., Ross R.A., Zanda M, & Greig I.R. (2019). The Trifluoromethyl Group as a Bioisosteric Replacement of the Aliphatic Nitro Group in CB1 Receptor Positive Allosteric Modulators. Journal of medicinal chemistry, 62(10), 5049-5062.
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2

Fluorine NMR Spectroscopy Protocol

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19F NMR spectra were recorded at 376 MHz on a Bruker ADVANCE III 400 instrument without 1H decoupling. Chemical shifts (δC) are given in parts per million (ppm) as referenced to CFCl3 as 0 ppm. All NMR spectra were recorded at 298 K unless otherwise stated. Chemical shifts (δC) are given in parts per million (ppm) as referenced to CHCl3. The following abbreviations were used to explain the multiplicities: s = singlet, d = doublet, t = triplet, q = quartet, quint = quintet, m = multiplet, br = broad.
Tseng C.C., Baillie G., Donvito G., Mustafa M.A., Juola S.E., Zanato C., Massarenti C., Dall’Angelo S., Harrison W.T., Lichtman A.H., Ross R.A., Zanda M, & Greig I.R. (2019). The Trifluoromethyl Group as a Bioisosteric Replacement of the Aliphatic Nitro Group in CB1 Receptor Positive Allosteric Modulators. Journal of medicinal chemistry, 62(10), 5049-5062.
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