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2 protocols using potassium carbonate

1

Synthesis and Characterization of Phenolphthalin

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Potassium 2,5-dihydroxybenzenesulfonate (SHQ), 2,6-difluorobenzonitrile (DFBN), deuterated dimethyl sulfoxide (DMSO-d6) and N,N-dimethyl formamide (DMF) were obtained from Sigma Aldrich (Shanghai, China). Bisphenol A (BPA), phenolphthalein (PP), zinc (Zn), sodium hydroxide (NaOH), potassium carbonate (K2CO3), N-methyl pyrrolidone (NMP), toluene, ethanol, tetrahydrofuran (THF), N,N-dimethylformamide (DMF), dichloromethane (CH2Cl2) and sodium dodecyl sulfate (SDS) were received from Chengdu Kelong Chemical Co. (Chengdu, China). Methylene blue (MB) and methyl orange (MO) were purchased from Sinopharm chemical reagent (Shanghai, China). Phenolphthalin (PPL) was synthesized from phenolphthalein (PP), Zn and NaOH.
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2

Synthesis of Undecanedioic Acid and AUA

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Undecanedioic acid (98%) and 11-aminoundecanoic acid (AUA, 98%) were supported by Hunan Huateng Scientific Co. Ltd. Hexamethylenediamine (99%, AR), potassium carbonate (K2CO3, AR) and deionized water were purchasedfrom Kelong Chemical Reagent Corp (Chengdu, China). All reagents and solvents in the syntheses were used without further purification.
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