Mdma d5

Manufactured by Lipomed

Sourced in Switzerland

MDMA-d5 is a deuterated analog of 3,4-methylenedioxymethamphetamine (MDMA). It is used as an internal standard and reference material in analytical methods for the detection and quantification of MDMA in various matrices.

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Lab products found in correlation

Ammonium acetate, by Avantor (1 mentions) Isoamyl alcohol, by Merck Group (1 mentions) Heptafluorobutyric acid hfba, by Merck Group (1 mentions) β glucuronidase, by Merck Group (1 mentions) Ammonium formate, by Thermo Fisher Scientific (1 mentions) Acetonitrile, by Thermo Fisher Scientific (1 mentions) Methanol, by Thermo Fisher Scientific (1 mentions) 2 propanol, by Thermo Fisher Scientific (1 mentions) Amphetamine d5, by Lipomed (1 mentions) Formic acid, by Merck Group (1 mentions) Diazepam d5, by Lipomed (1 mentions) Cotinine d3, by LGC (1 mentions) Oasis hlb cartridge, by Waters Corporation (1 mentions) Thc cooh, by Lipomed (1 mentions) Cotinine, by LGC (1 mentions) 3 4 methylenedioxymethamphetamine mdma, by Lipomed (1 mentions) Trifluoroacetic acid tfa, by Merck Group (1 mentions)

4 protocols using mdma d5

Certified 3-MeO-PCP Quantification Protocol

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Certified solution of 3-MeO-PCP, at 1 mg/mL in methanol, used to prepare the working solutions for the calibration curve was purchased from Sigma Aldrich (Saint-Quentin-Fallavier, France). MDMA-d5, used as internal standard, was obtained from Lipomed (Arlersheim, Switzerland) and diluted to appropriate concentrations. Ammonium formate, >99%, di-sodium tetraborate decahydrate and ammonium acetate were provided by VWR Chemicals (Leuven, Belgium). Formic acid for LC-MS was obtained from Carlo Erba (Chaussée du Vexin). HPLC-grade acetonitrile, methanol, dichloromethane, n-hexane, ethyl acetate and diethyl ether, acetic acid and 36% hydrochloric acid were obtained from VWR Prolabo (Fontenay-sous-Bois, France). Isoamyl alcohol, β-glucuronidase and heptafluorobutyric acid (HFBA) were purchased from Sigma Aldrich.

Arbouche N., Kintz P., Zagdoun C., Gheddar L., Raul J.S, & Ameline A. (2021). Determination of 3-MeO-PCP in human blood and urine in a fatal intoxication case, with a specific focus on metabolites identification. Forensic Sciences Research, 6(3), 208-214.

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Quantitative Analysis of Drugs in Biological Samples

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Reference standards including the internal standards diazepam-d₅, morphine-d₆, methadone‐d₃, mianserin-d₃ and amphetamine-d₅ or MDMA-d₅ were purchased from Lipomed GmbH (Arlesheim, Switzerland), Cerilliant (Round Rock, TX, USA) or Toronto Research Chemicals (Toronto, ON, Canada). All reference standards were of ≥98% purity, as stated in the certificates. Acetonitrile (≥99.9%), methanol (≥99.9%), purified water, 2-propanol (≥99.5%) and ammonium formate (≥99.9%) were obtained from Fisher Scientific (Loughborough, UK) and were all LC–MS grade. Formic acid (98–100%) was purchased from Merck (Damstadt, Germany). Leucine enkephalin acetate was purchased from Sigma-Aldrich (St. Louis, MO, USA).

Hansen S.L., Dalsgaard P.W., Linnet K, & Rasmussen B.S. (2022). Comparison of Comprehensive Screening Results in Postmortem Blood and Brain Tissue by UHPLC–QTOF-MS. Journal of Analytical Toxicology, 46(9), 1053-1058.

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Comprehensive Quantification of Illicit Drugs

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BE, AMPH, METH, MDMA, MOR, THC-COOH, and their deuterated analogues used as internal standards (BE-d₃, MOR-d₃, THC-COOH-d₃, MDMA-d₅) were purchased from Lipomed (Arlesheim, Switzerland). EtS and EtS-d₅ were obtained from Restek (Bellefonte, PA, USA). Cotinine and Cotinine-d₃ were purchased from Toronto Research Chemicals (TRC) (Ontario, Canada). Oasis HLB cartridges (6 mL/500 mg) were obtained from Waters Corporation (Milford, MA, USA). Glass-fiber filters (Whatman® glass microfiber filters, Grade GF/F, 0.7 μm) were purchased from Merck, (Darmstadt, Germany) as well as ammonium acetate, liquid chromatography grade methanol, ultrapure water, acetonitrile, and acetic acid (98 % purity).

, & Guzel E.Y. (2022). Monitoring of changes in illicit drugs, alcohol, and nicotine consumption during Ramadan via wastewater analysis. Environmental Science and Pollution Research International, 29(59), 89245-89254.

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Quantitative Bioanalysis of MDMA, MDA, and MPh

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3,4-Methylenedioxymethamphetamine (MDMA); 3,4-methylenedioxyamphetamine (MDA); MDMA-D5; MDA-D5 and methylphenidate (MPh) were obtained from Lipomed (Arlesheim, Switzerland). Water was purified with a Purelab Ultra (Labtec, Villmergen, Switzerland) filtration unit. Alpha-cyano-4-hydroxycinnamic acid (CHCA), acetonitrile (ACN), methanol (MeOH), sodium carbonate (Na 2 CO 3 ), ethyl acetate (EtOAc), butyl acetate (ButOAc) and trifluoroacetic acid (TFA) were purchased from Sigma Aldrich (Buchs, Switzerland). All other chemicals used were purchased from Merck (Zug, Switzerland) and of the highest grade available.

Poetzsch M., Steuer A.E., Hysek C.M., Liechti M.E, & Kraemer T. (2016). Development of a high-speed MALDI-triple quadrupole mass spectrometric method for the determination of 3,4-methylenedioxymethamphetamine (MDMA) in oral fluid. Drug testing and analysis, 8(2).

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