The solvents dimethylsulfoxide (DMSO), dimethyl acetamide, chloroform (CHCl3), methanol (CH3OH), acetone, 1,4-dioxane, tetrahydrofuran (THF) and toluene were dried and distilled by well known standard procedures39 and kept in a glovebox for further use. Fluorene (1), 4,7-dibromobenzo[c]-1,2,5-thiadiazole (7), 9-(heptadecan-9-yl)-2,7-bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-9H-carbazole (M3) and perylene-3,4,9,10-tetracarboxylic dianhydride were purchased from Sigma-Aldrich (USA) and was used directly without purification. 2-Bromo-9,9-dioctylfluorene (2), 2-bromo-7-nitro-9,9-dioctylfluorene (3), 2-amino-7-bromo-9,9-dioctylfluorene (4), 2,7-dibromo-9,9-dioctyl-9H-fluorene (5) and 4,4,5,5-tetramethyl-2-(4-octylthiophene-2-yl)-1,3,2-dioxaborolane (6) were synthesized by reported literature procedures.40–42 (link) 2,2′-(9,9-Dioctyl-9H-fluoren-2,7-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) (M2) and 4,7-bis(4-octylthiophen-2-yl)benzo[c]-1,2,5-thiadiazole (M4) were synthesized by reported methods with modified reaction conditions and improved yields43,44 (link) (details were given in ESI† ).
Perylene 3 4 9 10 tetracarboxylic dianhydride
Manufactured by Merck Group
Sourced in United States
Perylene-3,4,9,10-tetracarboxylic dianhydride is a chemical compound used in laboratory settings. It functions as a precursor for the synthesis of various organic molecules.
Automatically generated - may contain errors
Lab products found in correlation
Chloroplatinic acid hexahydrate, by Merck Group (1 mentions)
Hplc grade methanol, by SD Fine Chemicals (1 mentions)
Titanium 4 isopropoxide ti och ch3 2 4, by Merck Group (1 mentions)
Ammonium persulfate aps nh4 2s2o8, by Merck Group (1 mentions)
Milli q water, by Merck Group (1 mentions)
Aniline, by Merck Group (1 mentions)
Silica nanoparticles, by Merck Group (1 mentions)
Octamethylcyclotetrasiloxane d4, by Merck Group (1 mentions)
Trifluoromethanesulfonic acid triflic acid, by Merck Group (1 mentions)
3 protocols using perylene 3 4 9 10 tetracarboxylic dianhydride
1
Synthetic Procedures for Organic Semiconductors
2
Synthesis of Doped Perylene Dianhydride Nanocomposites
Check if the same lab product or an alternative is used in the 5 most similar protocols
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Aniline, chloroplatinic
acid hexahydrate (H2PtCl6, 6H2O,
≥37.50% Pt basis), perylene-3,4,9,10-tetracarboxylic dianhydride,
ammonium persulfate [(NH4)2S2O8] (APS), and titanium(IV) isopropoxide [Ti{OCH(CH3)2}4] were bought from Sigma-Aldrich and were
used as supplied, except Aniline which was distilled before use. Methanol
(HPLC Grade) was supplied by S D Fine-Chem Limited. Deionized water
(18 MU cm, Millipore Milli-Q water) was used to prepare solutions
where necessary.
acid hexahydrate (H2PtCl6, 6H2O,
≥37.50% Pt basis), perylene-3,4,9,10-tetracarboxylic dianhydride,
ammonium persulfate [(NH4)2S2O8] (APS), and titanium(IV) isopropoxide [Ti{OCH(CH3)2}4] were bought from Sigma-Aldrich and were
used as supplied, except Aniline which was distilled before use. Methanol
(HPLC Grade) was supplied by S D Fine-Chem Limited. Deionized water
(18 MU cm, Millipore Milli-Q water) was used to prepare solutions
where necessary.
3
Synthesis of Siloxane-based Functional Materials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Octamethylcyclotetrasiloxane (D4, 98%, Sigma-Aldrich), trifluoromethanesulfonic acid (triflic acid, 99%, Sigma-Aldrich), heptamethylcyclotetrasiloxane (tech-95, Gelest), trivinylmethylsilane (95%, Gelest), platinum(0)-1,3-divinyl-1,1,3,3-tertramethyldisiloxane in xylene (Pt catalyst, 2% of Pt, Sigma-Aldrich), perylene-3,4,9,10-tetracarboxylic dianhydride (97%, Sigma-Aldrich), and solvents were used as purchased. CB pearls 2000 (BP-2000) were offered by Cabot Corporation, silica nanoparticles (20 nm) were purchased from Sigma-Aldrich, and PTFE nanoparticles (MPD170, 20-50 nm) were purchased from DuPont. All the chemicals were used directly without further treatment.
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