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2 protocols using benzo j fluoranthene

1

Comprehensive PAH Standard Solution Analysis

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A composite standard solution of 18 PAHs including acenaphthene(ANA), acenaphthylene (ANY), benzo(b)fluoranthene (BbF), benzo(k)fluoranthene (BkF), benzo(g,h,i)perylene (BPE), chrysene (CHR), fluoranthene (FLT), fluorene (FLU), naphthalene (NAP), phenanthrene (PHE), anthracene (ANT), benzo(a)- anthracene (BEA), benzo(j)fluoranthene (BjF), benzo(a)pyrene (BaP), benzo(e)pyrene (BeP), bibenzo(a,h)anthracene (BaA), indeno(1,2,3-cd)pyrene (IPY) and pyrene (PYR) was purchased from Sigma-Aldrich (USA), each at a concentration of 1000 μg·mL−1. N-hexane and acetonitrile were obtained from Chongqing Xinyu Chemical Reagent Co., Ltd. (China), both with an analytical grade.
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2

PAH Detection in Environmental Samples

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Analytical grade (99.9% pure) acetone and hexane are purchased from Merck Millipore (Massachusetts, USA). 18 PAH standard mixture solution (Acenaphthene (AcP), Acenaphthylene (AcPy), Anthracene (Ant), Benzo[a]Anthracene (BaA), Benzo[a]pyrene (BaP), Benzo[e]pyrene (BeP), Benzo[b]fluoranthene (BbFL), Benzo[g,h,i]perylene (BghiP), Benzo[j]fluoranthene (BjFL), Benzo[k]fluoranthene (BkFL), Chrysene (Chr), Dibenzo[a,h]Anthracene (DBA), Fluoranthene (FL), Fluorene (Flu), Indeno [1,2,3-cd]pyrene (InP), Naphthalene (NaP), Phenanthrene (Phe) and Pyrene (Pyr)) are obtained from Sigma–Aldrich (Missouri, USA). Powdered Benzo[e]pyrene-d12 (BeP-d12) perdeuterated internal standard is purchased from Sigma–Aldrich (Missouri, USA). 16 PAH internal standard mixture solution (1000 μg/mL in toluene) (AcP-d10, Acpy-d8, Ant-d10, BaA-d12, Bap-d12, BbFL-d12, BghiP-d12, BkFL-d12, Chr-d12, DBA-d14, Flu-d10, FL-d10, InP-d12, NaP-d8, Phe-d10, Pyr-d10) are from Chiron (Trondheim, Norway). Disposable Nylone filters (0.22 μm) are provided by Merck Millipore (Massachusetts, USA).
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