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Heptane

Manufactured by Sinopharm
Sourced in China

Heptane is an organic compound with the chemical formula C7H16. It is a colorless, flammable liquid that is commonly used as a solvent in various industrial and laboratory applications. Heptane has a high boiling point and is often used in applications where a stable, non-polar solvent is required, such as in the synthesis of organic compounds, in the extraction of certain chemicals, and in the preparation of samples for analytical procedures.

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3 protocols using heptane

1

Quantification of Illicit and Pharmaceutical Drugs

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Amphetamine (AMP), methamphetamine (MAMP), 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymethamphetamine (MDMA), ketamine, methadone, pethidine, secobarbital, lidocaine, clenbuterol, benzhexol, carbamazepine, diazepam, chlorpromazine, olanzapine, flurazepam, clozapine, alprazolam, triazolam and diphenoxylate were purchased from the National Institute for Control of Pharmaceutical and Biological Products (Beijing, PR China). HPLC grade chlorobutane was obtained from Sigma–Aldrich Co., Ltd. (St. Louis, USA). Analytical grade ethyl acetate, hexane, cyclohexane, heptane, isooctane, sodium hydroxide (NaOH) and HPLC grade methanol were purchased from Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China).
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2

Facile Synthesis of Monolithic MSQ Aerogels

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The MSQ aerogel monolith was synthesized by a sol-gel process followed by ambient drying in an oven at 40 °C for 12 h. For hydrolysis and polymerization, Methyltrimethoxysilane (MTMS, Aladdin, Shanghai, China, 98%) was added into a mix of hexadecyltrimethylammonium chloride (CTAC, Aladdin, 97%), methanol, and HCl solution, with vigorous stirring and an ice-bath for 30 min. Propylene oxide (PO, Sinopharm Chemical Reagent Co., Ltd., Shanghai, China, ≥99.5%) was then added as a gelation agent into the mixed solution and stirred for 2 min. The fabricated mix solution was closed and placed into an oven at 40 °C for the gelation process for about 40 min and a further aging process for 40 min. The gel was further solvent-exchanged with 2-propanol, hexamethyldisilane/n-heptane, and heptane (Sinopharm Chemical Reagent Co., Ltd., Shanghai, China, ≥99.5%) to eliminate CTAC and water. Finally, the solvent-exchanged gels were dried at 40 °C for 24 h to prepare the monolith of MSQ aerogel.
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3

Phytic Acid Membrane Fabrication Protocol

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Phytic acid (PhA, 70 wt%) was provided by Shanghai Dibo Chemicals Technology Co. Ltd. (China). Magnesium sulphate (MgSO4, 99%), sodium sulphate (Na2SO4, 99%), magnesium chloride (MgCl2, 95%), sodium chloride (NaCl, 99%), camphorsulfonic acid (C10H16O4S, 99%), triethylamine (C6H15N, 99%), Isopar G (CH3(CH2)4CH3, 99%), and trimesoyl chloride (C9H3Cl3O3, 99%) were supplied by XiLong Chemical Reagents Co. Ltd. (China). Piperazine (C4H10N2, 99%) and heptane (C7H16, 99%) were obtained from Sinopharm Chemical Reagents Co. Ltd. (China). A polysulfone (PSU) ultrafiltration membrane, and VNF1, DNF2 and VNFK commercial membranes were supplied by Suntar Membrane Technology (Xiamen). The reagents mentioned above are of analytical grade.
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