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3 protocols using n n dimethylformamide dmf ar

1

Synthesis of Bismuth-based Nanomaterials

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Poly(ethylene oxide) (PEO, Mn = 100 000), sodium carbonate (Na2CO3), hexadecyl trimethyl ammonium bromide (CTAB) and bismuth nitrate pentahydrate (Bi(NO3)3·5H2O) were purchased from Anpel Laboratory Technologies (Shanghai, China). Pentaerythrotol triacrylate (PETA) was purchased from Yuanye Biological Inc (Shanghai, China). Dichloromethane (DCM, HPLC), methanol (AR) and N,N-dimethylformamide (DMF, AR) were purchased from Sinopharm Chemical Reagent Co., Ltd (Shanghai, China). The above-mentioned reagents were used as provided by the manufacturer without further purification. Ultrapure water produced from a Milli-Q device (18.2 MΩ cm−1) was used throughout the experiments. L-929 fibroblast cells, Dulbecco's modified Eagle medium (DMEM), fetal bovine serum (FBS) and cell Counting Kit-8 (CCK8) were purchased from Shanghai Fanmeng Biotechnology Co., Ltd (Shanghai, China).
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2

Synthesis of Antimony Nanoparticles

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Oleylamine (80–90.0%) and N-Methyl-2-pyrrolidone (NMP, AR, 99.0%) were purchased from Aladdin. Oleic acid (90.0%) was purchased from Alfa Aesar. Sodium borohydride (99.0%) was purchased from Fluka. All other chemical reagents including antimony (5N), dodecanethiol (CP), ethanol (AR), methanol (AR), n-butanol (AR), ethylene glycol (AR), isopropanol (AR), glycerol (AR), cyclohexane (AR), acetone (AR), polyvinylpyrrolidone (PVP, K-30), N,N-dimethylformamide (DMF, AR) and antimony trichloride (AR) were purchased from Sinopharm Chemical Reagent Co. Ltd. All the reagents were used without further purification.
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3

Synthesis and Characterization of Metal-Organic Frameworks

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The chemicals of nickel(ii) nitrate hexahydrate (Ni(NO3)2·6H2O, AR), phosphomolybdic acid (H3PMo12O40·nH2O, HPMo, AR), tungstophosphoric acid (H3PW12O40·nH2O, HPW, AR), silicotungstic acid (HSiW, H4SiW12O40·nH2O, HSiW, AR), and terephthalic acid (H2-BDC, AR) are purchased from Shanghai Aladdin Biochemical Technology Co., Ltd, Shanghai, China. Absolute ethanol (AR), oleic acid (C18:1, AR), anhydrous methanol (AR), and N,N-dimethylformamide (DMF, AR) are purchased from Sinopharm Chemical Reagent Co., Ltd, Shanghai, China. These chemicals are directly used without further purification.
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