Eucalyptus globulus was used as feedstock and was provided by CIFOR-INIA (“Centro de Investigación Forestal-Instituto Nacional de Investigación y Tecnología Agraria y Alimentaria”, in Spain). The ionic liquid 1-methylimidazolium chloride ([Mim][Cl], 98% purity) was supplied by Iolitec GmbH. Ethanol was used as antisolvent and supplied by Panreac (96% purity). N,N-Dimethylformamide (DMF, ≥99.9%, Panreac) and ReadyCal Kit PMMA standards (Polymer Standards Service GmbH) were used in GPC analysis.
1 methylimidazolium chloride
Manufactured by IoLiTec
1-methylimidazolium chloride is a chemical compound with the formula C4H7N2+Cl-. It is a white crystalline solid that is soluble in water and other polar solvents. The compound is commonly used as a building block in the synthesis of other chemicals and materials.
Automatically generated - may contain errors
2 protocols using 1 methylimidazolium chloride
1
Eucalyptus Depolymerization Using Ionic Liquid
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Eucalyptus globulus was used as feedstock and was provided by CIFOR-INIA (“Centro de Investigación Forestal-Instituto Nacional de Investigación y Tecnología Agraria y Alimentaria”, in Spain). The ionic liquid 1-methylimidazolium chloride ([Mim][Cl], 98% purity) was supplied by Iolitec GmbH. Ethanol was used as antisolvent and supplied by Panreac (96% purity). N,N-Dimethylformamide (DMF, ≥99.9%, Panreac) and ReadyCal Kit PMMA standards (Polymer Standards Service GmbH) were used in GPC analysis.
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Eucalyptus globulus was used as feedstock and was provided by CIFOR-INIA (“Centro de Investigación Forestal-Instituto Nacional de Investigación y Tecnología Agraria y Alimentaria”, in Spain). The ionic liquid 1-methylimidazolium chloride ([Mim][Cl], 98% purity) was supplied by Iolitec GmbH. Ethanol was used as antisolvent and supplied by Panreac (96% purity). N,N-Dimethylformamide (DMF, ≥99.9%, Panreac) and ReadyCal Kit PMMA standards (Polymer Standards Service GmbH) were used in GPC analysis.
2
Synthesis and Characterization of Ionic Liquids
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1-Butyl-3-Methyl Imidazolium Chloride (BMIM Cl) (99%), 1-Hexyl-3-Methyl Imidazolium Chloride (HMIM Cl) (>98 %), 1-Methyl Imidazolium Chloride (MIM Cl) (98 %), and 1-Butyl-3-Methyl trifluoromethanesulfonate (BMIM OTf) (98 %) were purchased from Iolitec®. Silver trifluoromethanesulfonate (Ag OTf) was purchased from ACROS®.
1-Butyl-3-Methyl Imidazolium Bromide (BMIM Br) was prepared according to the procedure described by Wu et al. 29 . 1-Butyl-3-MethylImidazolium bis(trifluoromethyl)sulfonyl imide (BMIM TFSI) was also prepared according to Wu et al. procedure 29 , slightly modified. Briefly, 1.1 eq LiTFSI and 1 eq BMIM Br were mixed in ultra pure water during 16 h at room temperature. The solid obtained was then washed 4 times with ultra pure water and dried by evaporation under vacuum during 24 h at 80 °C.
Density and viscosity of ionic liquids were determined using respectively a DMA 4100 densimeter and a Lovis 2000 viscosimeter, both from Anton Paar®.
1-Butyl-3-Methyl Imidazolium Bromide (BMIM Br) was prepared according to the procedure described by Wu et al. 29 . 1-Butyl-3-MethylImidazolium bis(trifluoromethyl)sulfonyl imide (BMIM TFSI) was also prepared according to Wu et al. procedure 29 , slightly modified. Briefly, 1.1 eq LiTFSI and 1 eq BMIM Br were mixed in ultra pure water during 16 h at room temperature. The solid obtained was then washed 4 times with ultra pure water and dried by evaporation under vacuum during 24 h at 80 °C.
Density and viscosity of ionic liquids were determined using respectively a DMA 4100 densimeter and a Lovis 2000 viscosimeter, both from Anton Paar®.
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