Xrd 6000 x ray powder diffractometer

Manufactured by Shimadzu

Sourced in Japan

The XRD-6000 is a versatile X-ray powder diffractometer manufactured by Shimadzu. It is designed to analyze the crystallographic structure of solid materials by recording the diffraction pattern produced when a sample is exposed to X-rays. The instrument features a goniometer that precisely controls the relative positions of the sample, X-ray source, and detector, allowing for accurate measurement of the diffraction angles.

Automatically generated - may contain errors

Lab products found in correlation

M510 pump, by Waters Corporation (1 mentions) Dcs r 100, by Shimadzu (1 mentions)

Spelling variants of this product

XRD-6000 (381 citations) XRD-6000 diffractometer (81 citations) XRD-6000 X-ray diffractometer (41 citations) X-ray diffractometer (19 citations) XRD-6000 powder diffractometer (6 citations) X-ray powder diffractometer (6 citations) X-ray 6000 (5 citations) X-ray diffractometer 6000 (3 citations) XRD-6000 powder (2 citations) 6000 powder diffractometer (2 citations)

5 protocols using xrd 6000 x ray powder diffractometer

Characterization of Synthesized ZnO Nanoparticles

Check if the same lab product or an alternative is used in the 5 most similar protocols

We used different techniques to characterize the synthesized ZnO NPs. The crystal structure and primary crystal size were characterized using an XRD-6000 powder X-ray diffractometer (Shimadzu scientific instruments, Kyoto, Japan) at the National Center for Radiation Research and Technology (NCRRT)—Egyptian Atomic Energy Authority, Cairo, Egypt. X-ray tube target (copper), voltage (40 kV), current (30 mA), and scanning drive axis (Theta-2Theta) with a continuous scan mode at a scan speed of 8 (deg./min) and the scan range from 4–90 (deg.) were the used parameters. The particle size (D) of the sample was calculated by Scherrer’s relationship [43 (link)]:

D = \frac{0.94 λ}{β c o s θ}

where λ is the X-ray wavelength, β is the broadening of the diffraction line measured at half of its maximum intensity in radians, and θ is the Braggs diffraction angle.

Elzahaby D.A., Farrag H.A., Haikal R.R., Alkordi M.H., Abdeltawab N.F, & Ramadan M.A. (2023). Inhibition of Adherence and Biofilm Formation of Pseudomonas aeruginosa by Immobilized ZnO Nanoparticles on Silicone Urinary Catheter Grafted by Gamma Irradiation. Microorganisms, 11(4), 913.

+ Open protocol

+ Expand

Analytical Techniques for Material Characterization

Check if the same lab product or an alternative is used in the 5 most similar protocols

The following equipment and instruments were
used in this study:
a Waters 244-type high-performance liquid chromatograph (American
Waters Company) equipped with a chromatographic column (Diamonsil
C18; 250 × 4.6 mm), a Waters 486 differential detector, an M510
pump, a six-way valve sample injector, a Zhejiang University 2000
chromatographic work station, and a mobile phone: experimental parameters—0.05
mol/L H₂SO₄ (v/v)); temperature, 55 °C;
and flow velocity, 0.01 mL/min; solvents—redistilled water
filtered through a 0.45 μm filtration membrane was used, acetonitrile
employed was chromatographically pure, methyl alcohol filtered through
a 0.51 μm filtration membrane was a guaranteed reagent, and
phosphoric acid used was a guaranteed reagent; an IR-Prestige-21-type
FTIR spectrometer (Shimadzu Corporation); an XRD6000-powder-X-ray
diffractometer (Shimadzu Corporation); a probe-type thermometer (accuracy:
0.1 °C; Shenzhen Youkong Electric Limited Company); artificial
board single-layer hot press (Y33-50; Pingxiang Jiuzhou Precise Press
Limited Company); an all-purpose mechanical tester (DCS-R-100; Shimadzu
Corporation); and an MIRA3LMH-type scanning electron microscope (TESCAN
China, Ltd.): experimental parameters—test pressure, 0.8 MPa
and test voltage, 15 KV.

Yin C., Yang Y, & Li X. (2021). Research on the Compatibility of Bamboo and Portland Cement. ACS Omega, 6(36), 23636-23642.

+ Open protocol

+ Expand

X-ray Diffraction Analysis of Drug Crystallinity

Check if the same lab product or an alternative is used in the 5 most similar protocols

Samples were subject to X-ray diffraction (XRD) analysis on XRD-6000 X-ray powder diffractometer (Shimadzu, Japan) coupled with a standard Cu sealed X-ray tube with 40 kV voltage and 40 mA current. Data collection was performed at 2-theta of 5–60° in steps of 0.04 and scanning speed of 0.4 degrees per step. XRD charts were recorded and investigated for any change in the drug crystalline pattern.

, & Khames A. (2017). Investigation of the effect of solubility increase at the main absorption site on bioavailability of BCS class II drug (risperidone) using liquisolid technique. Drug Delivery, 24(1), 328-338.

+ Open protocol

+ Expand

Apatite Mineral Fraction Preparation

Check if the same lab product or an alternative is used in the 5 most similar protocols

The
object of the study
is a monomineral fraction of apatite, separated from the apatite-nepheline
ore of Khibiny deposits and subjected to preliminary preparation.
The surface of the samples under study was cleaned from organic inclusions
(collector fragments) by calcination of the sample in a muffle furnace
at 600 °C for 4 h. The phase composition was established by X-ray
diffraction (XRD) on a XRD-6000 X-ray powder diffractometer manufactured
by Shimadzu (Japan). The XRD spectrum of the ore surface is shown
in Figure 2.
The only defined crystalline phase is calcium phosphate. The chemical
composition of the sample was established by X-ray fluorescent analysis
with an XRF-1800 device of Shimadzu company. The sample consists of
50.024% CaO; 42.30% P₂O₅; 3.00% SrO; and 2.0405%
F, the remaining is impurities.
Oleic acid (technical degree
of purity) with a main component concentration
of at least 97.4% was chosen as a model fatty acid collector. Saponification
of oleic acid with sodium hydroxide was carried out at 60 °C
for 2 h per saponification number. Phospholan PE65 was provided by
Akzo Nobel Chemistry AB (Stenungsund, Sweden) and was saponified under
the same conditions before the flotation experiments. 0.10 mol/L HCl
and 0.10 mol/L NaOH with analytical purity were used to adjust the
pH of the flotation pulp. Preparation of solutions and flotation experiments
were carried out using distilled water.

Sergeev V.V., Cheremisina O.V., Fedorov A.T., Gorbacheva A.A, & Balandinsky D.A. (2022). Interaction Features of Sodium Oleate and Oxyethylated Phosphoric Acid Esters with the Apatite Surface. ACS Omega, 7(3), 3016-3023.

+ Open protocol

+ Expand

Characterizing Amorphous Drug Formulations

Check if the same lab product or an alternative is used in the 5 most similar protocols

Samples of clozapine powder, CAPs as well as solid dispersion formulations were subject to X-ray diff raction analysis. A Shimadzu XRD-6000 X-ray powder diff ractometer (Shimadzu, Japan) coupled with a standard Cu sealed X-ray tube with voltage, and current (40 kV and 40 mA), was used to characterize the amorphous or crystalline state of formulations (22) (link). Data collection was performed at 2-theta of 5-60° in steps of 0.04 and scanning speed of 0.4 per step. Any change in the crystalline pa ern of the prepared co-amorphous dispersions compared to those of the parent crystalline components was recorded and evaluated.

Ali A.M., Ali A.A, & Maghrabi I.A. (2015). Clozapine-carboxylic acid plasticized co-amorphous dispersions: Preparation, characterization and solution stability evaluation. Acta pharmaceutica (Zagreb, Croatia), 65(2).

+ Open protocol

+ Expand

About PubCompare

Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.

We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.

However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.

Ready to get started?

Revolutionizing how scientists
search and build protocols!