Example 9
X-ray Powder Diffraction (XRPD):
X-Ray Powder Diffraction traces were obtained using a D8 Advance, Bruker apparatus; using one of two Methods:
Scan 5-45° 2-theta, 0.02° step size, 1 sec per step; or
Scan 3-40° 2-theta, 0.037° step size, 1.5 sec per step
Fourier Transform Infrared Spectroscopy (FTIR):
FTIR traces were obtained using a Nicolet iS10 FTIR apparatus from ThermoFisher Scientific
Method: Analyzed by attenuated total reflectance with 32 scans and a resolution of 4 over a wavenumber range of 525-4000 cm−1 with a background obtained before each measurement