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Sta 449 f1 jupiter instrument

Manufactured by Netzsch
Sourced in Germany

The STA 449 F1 Jupiter is a simultaneous thermal analysis (STA) instrument manufactured by Netzsch. It is designed to perform thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC) measurements on a wide range of materials. The instrument provides accurate and reliable data on mass changes and heat flow effects experienced by samples during controlled temperature programs.

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7 protocols using sta 449 f1 jupiter instrument

1

Thermogravimetric Analysis of Samples

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A small amount
of the sample (2–3 mg) was taken in a standard
alumina pan with an alumina lid with a pin hole at the middle. An
empty crucible was used as the reference. Thermogravimetric Analysis
(TGA)-DSC analyses were carried out by using a NETZSCH STA 449 F1
Jupiter instrument. The samples were heated from room temperature
to 300 °C at a heating rate of 5 °C min–1 under nitrogen atmosphere with a flow rate of 60 mL min–1 protective and 40 mL min–1 purge gases.
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2

Thermogravimetric Analysis of Solid Samples

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Thermogravimetric measurements were taken with a STA 449F1 JUPITER instrument, manufactured by Netzsch GmbH in Selb, Germany. Calibrations of temperature and sensitivity were conducted with indium over a temperature range of 30–700 °C. After the weighing of the solid samples, which ranged from around 5.0 to 11 mg, the samples were placed in alumina pans to be subjected to TG measurements. The temperature range employed was between 30 and 700 °C, and the heating rate was 10 °C/min. This was performed in an environment of dry nitrogen with a flow rate of 50 mL/min. The NETZSCH PROTEUS 4.2 software (Netzsch, GmbH, Selb, Germany) was used to perform the analysis of the data.
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3

Thermogravimetric Analysis of Samples

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The thermogravimetry study was carried out on a NETZSCH TG 209 F1 thermal analyzer (NETZSCH STA 449 F1 Jupiter instrument, Netzsch, Selb, Germany) and the data obtained were analyzed. The thermal decomposition of the samples was analyzed in nitrogen in the temperature range from 25 to 700 °C. The protective and blowout gas flow rates were 20 mL/min. The samples were heated in cylindrical corundum crucibles in a dynamic temperature regime (10 °C/min). A TG 209 F1 analyzer was calibrated using the instructions and reference manifestations that appear with the instrument and weighing the samples on an XFR-125E laboratory balance. The measurement data were processed in the NETZSCH Proteus Thermal Analysis 4.8.4 software supplied with the instrument.
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4

Cellulose Thermal Analysis by TGA

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The thermogravimetric analysis (TGA) was carried out on a synchronous thermal analyzer (NETZSCH STA 449 F1 Jupiter instrument, Netzsch, Selb, Germany). The cellulose samples were analyzed in the argon atmosphere upon heating from 30 to 900 °C at a rate of 10 °C/min−1. The measured data were processed in the NETZSCH. Proteus Thermal Analysis. 5.1.0 software.
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5

Thermogravimetric Analysis of Solid Samples

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Thermogravimetric measurements were taken with a STA 449F1 JUPITER instrument, manufactured by Netzsch GmbH in Selb, Germany. Calibrations of temperature and sensitivity were conducted with indium over a temperature range of 30–700 °C. After the weighing of the solid samples, which ranged from around 5.0 to 11 mg, the samples were placed in alumina pans to be subjected to TG measurements. The temperature range employed was between 30 and 700 °C, and the heating rate was 10 °C/min. This was performed in an environment of dry nitrogen with a flow rate of 50 mL/min. The NETZSCH PROTEUS 4.2 software (Netzsch, GmbH, Selb, Germany) was used to perform the analysis of the data.
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6

Thermogravimetric Analysis of Lignin

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The thermogravimetry analysis was carried out using a Netzsch STA 449 F1 Jupiter instrument (Waldkraiburg, Germany). The thermal degradation of the lignin samples was studied in argon in the temperature range from 298 to 1173 K. The samples were heated in the dynamic mode at a heating rate of 10 °C/min in corundum crucibles. The measured data were processed using the Netzsch Proteus Thermal Analysis.5.1.0 software package supplied with the instrument.
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7

Thermal Analysis of Lead Xanthates

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The samples
of lead xanthates for TGA were precipitated from the 1 mM colloidal
solutions by centrifugation at 10g for 10 min, washed
with water by decantation, and dried on a filter paper in air at room
temperature. TGA and DTA were performed in the range from the ambient
temperature to 900 °C using a STA449 F1 Jupiter instrument (Netzsch)
at the heating rate of 10 °C/min in argon at a gas flow rate
of 50 mL/min; some experiments were also conducted in air.
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