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3 protocols using tetrahydrofuran

1

Eucalyptus Biomass Compositional Analysis

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Eucalyptus (hardwood) chips were obtained from Nine Dragons Paper. A cutting mill was utilized to mill wood chips into powder with grains around 0.712 mm in diameter. Sodium hydroxide (NaOH), sulfuric acid (H2SO4), hydrochloric acid (HCl) and tetrahydrofuran (THF) were purchased from Nanjing Chemical Reagent Co., Ltd., Nanjing, China.
The composition analysis of raw biomass was performed according to the NREL [29 (link)] protocol. Results are as shown in Table 1:
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2

Synthesis of Functional Polymeric Materials

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Castor oil, caustic potash (KOH), anhydrous methanol, tetrabutyl titanate, tetrahydrofuran, 1,3,5-Tris (2-hydroxyethyl) cyanuric acid (THEIC), diethyl chlorophosphate, concentrated sulfuric acid, chloroform, dioctyl phthalate (DOP), propargyl bromide solution, potassium carbonate, sodium azide, N,N-dimethylformamide (DMF), acetone, cuprous bromide, 5,5-dimethyl-2,2-dipyridyl were bought from Nanjing Chemical Reagent Co., Ltd. PVC was bought from Hanwha.
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3

Cardanol-based Polymeric Materials

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Cardanol (99%, acid value 5.5–6.6. Iodine value 210–250) was provided by Jining Hengtai Chemical Co., Ltd. (Jining, China) Propargyl bromide solution, tetrahydrofuran (THF), potassium carbonate, sodium azide, methanol, acetone, cuprous bromide, 5,5-dimethyl-2,2-dipyridyl, N,N-dimethylformamide (DMF) and dioctyl phthalate (DOP) were kindly provided by Nanjing Chemical Reagent Co., Ltd. (Nanjing, China) Polyvinyl chloride (PVC) was supplied by Hanwha (KM-31, Seoul, Korea).
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