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Tch600

Manufactured by Leco
Sourced in United States

The TCH600 is a laboratory equipment designed for testing and analyzing materials. It is a compact and versatile instrument that can be used for a variety of applications. The core function of the TCH600 is to provide accurate and reliable measurements of various properties of materials.

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7 protocols using tch600

1

Characterization of Ti6Al4V Powder for SLM

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In this study, Ti6Al4V gas atomized powder (SLM Solutions Group AG, Lübeck, Germany) was used. The chemical composition of virgin powder delivered by the manufacturer is in Table 1. The powder shape was checked by scanning electron microscopy (SEM) LEO 1450VP (Carl Zeiss AG, Oberkochen, Germany). Figure 1a shows that the powder particles have a spherical shape with a low amount of satellites. The particles size distribution was analysed by laser diffraction analyser LA-960 (Horiba, Kioto, Japan). Measured particle mean size was 43 µm and median size 40.9 µm. The particles up to 29.97 µm represented 10% of particle distribution while particles up to 58.61 µm represented 90% (Figure 1b).
The chemical composition of used powder was evaluated by the following methods. The aluminium content was checked by the inductively coupled plasma atomic emission spectroscopy. Oxygen and nitrogen contents were evaluated by hot extraction in helium by LECO TCH 600 (LECO Corporation, Saint Joseph, MO, USA). The hydrogen concentration was verified by the inert gas fusion thermal conductivity method JUWE H-Mat 2500 (JUWE Laborgeraete GmbH, Viersen, Germany). The accuracy of all methods is Al ±0.327 wt %, O ±0.008 wt % and N ±0.0025 wt %.
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2

Comprehensive Elemental Analysis of Chars

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Element analyses for C, N and H were performed on a Vario EL cube (Elementar Analysensysteme GmbH, Langenselbold, Germany). All chars were dried at 106 °C until constant weight. Oxygen was determined with a LECO TCH600 (LECO, St. Joseph, MI, USA). The ash content was determined in a muffle furnace at 815 ± 15 °C. Three samples of each char were also analysed for 23 other elements by Inductive Coupled Plasma Optical Emission Spectroscopy (ICP-OES). To do so, 50 mg of sample were mixed with 0.25 g of LiBO3 and heated within 3 h to 1000 °C in a muffle furnace. The decomposition was performed for 30 min at this temperature. After cooling, the melt was dissolved in 30 ml HCl (5%). The solution was diluted to 50 ml. Duplicate samples were diluted 1/10 and analysed with an iCAP 7600 (Thermo Fisher Scientific, Waltham, Massachusetts, USA).
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3

Additive Manufacturing of Titanium Alloy

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Titanium alloy wire AWS A5.16 ER Ti5 (EN ISO 24034) was used with a commercially available diameter of 1.2 mm. The deposition was carried out with two different substrates: Commercial pure Titanium Grade 2 for the parameter studies and the single bead experiments; and Titanium Grade 5 (Ti-6Al-4V) for the subsequent multilayer-experiments, and mechanical as well as metallographic characterization.
The chemical compositions of the applied titanium alloy wire and the AM structures made out of it were determined as follows: the proportion of the elements aluminum (Al), vanadium (V), and iron (Fe) are determined by atomic absorption spectroscopy. The interstitial elements carbon (C) via solid-state infrared absorption detection method with LECO CS230 (LECO Corporation, St. Joseph, MI, USA); nitrogen (N) via thermal conductivity detection method with LECO ON 736 (LECO Corporation, St. Joseph, MI, USA); and oxygen (O) via non-dispersive infrared absorption detection method with LECO TCH600 (LECO Corporation, St. Joseph, MI, USA). Table 1 shows the chemical composition of the applied wire in this work.
For the titanium alloy wire, the proportion of all elements with the exception of vanadium is according to the specification. Only the proportion of vanadium is slightly below the permissible lower limit of the specification.
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4

Comprehensive Elemental Analysis of NT-Ni Specimens

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The contents of light elements—H, C, N, O, and S—in the as-deposited NT-Ni specimens were analyzed using a combination of simultaneous carbon/sulfur determinator (CS600, LECO) and oxygen/nitrogen/hydrogen analyzer (TCH-600, LECO). The contents of other elements were also quantified using inductively coupled plasma optical emission spectroscopy (ICP-OES; OPTIMA 8300DV). The carbon and sulfur in our specimens (table S1) originate from the additives in the plating bath, i.e., 2-butyne-1,4-diol and sodium saccharin, and their contents in NT-Ni specimens are consistent with those reported previously in (49 ). Energy-dispersive x-ray spectroscopy (EDS) equipped in an FEI Talos F200X TEM was used as a supplemental method to characterize the elemental distribution at GBs in the as-deposited NT-2.9 specimen. EDS line scans showed that carbon and sulfur were uniformly distributed in the sample with no obvious segregation at the GBs (fig. S13).
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5

Characterizing Metal Powder Properties

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Example 3

Particle flow can be measured according to a standardized protocol, such as by using a Hall flow meter according ASTM International Standard B213.

Molecular content of the metal powders produced by the methods described herein can be determined using LECO testers. For example, nitrogen and oxygen content can be tested with LECO Model TC436DR. Carbon and sulfur content can be tested with LECO Model CS444LS. Nitrogen, oxygen, and hydrogen content can be tested with LECO Model TCH600.

Purity can be assess by glow discharge mass spectrometry or inductively coupled plasma mass spectrometry.

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6

Standardized Characterization of Metal Powders

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Example 3

Particle flow can be measured according to a standardized protocol, such as by using a Hall flow meter according ASTM International Standard B213.

Molecular content of the metal powders produced by the methods described herein can be determined using LECO testers. For example, nitrogen and oxygen content can be tested with LECO Model TC436DR. Carbon and sulfur content can be tested with LECO Model CS444LS. Nitrogen, oxygen, and hydrogen content can be tested with LECO Model TCH600.

Purity can be assess by glow discharge mass spectrometry or inductively coupled plasma mass spectrometry.

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7

Characterizing Metal Powder Properties

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Example 3

Particle flow can be measured according to a standardized protocol, such as by using a Hall flow meter according ASTM International Standard B213.

Molecular content of the metal powders produced by the methods described herein can be determined using LECO testers. For example, nitrogen and oxygen content can be tested with LECO Model TC436DR. Carbon and sulfur content can be tested with LECO Model CS444LS. Nitrogen, oxygen, and hydrogen content can be tested with LECO Model TCH600.

Purity can be assess by glow discharge mass spectrometry or inductively coupled plasma mass spectrometry.

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